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(3,4-Dimethoxyphenyl)acetonitrile

Product Name
(3,4-Dimethoxyphenyl)acetonitrile
CAS No.
93-17-4
Chemical Name
(3,4-Dimethoxyphenyl)acetonitrile
Synonyms
Homoveratronitrile;3,4-dimethoxybenzyl;3,4-Dimethoxybenzyl cyanide;NSC 6324;Veratryl cyanide;HOMOVERATONITRILE;WLN: NC1R CO1 DO1;Homoveratronitrite;TIMTEC-BB SBB005899;(3,4-Dimethoxyphenyl
CBNumber
CB3254471
Molecular Formula
C10H11NO2
Formula Weight
177.2
MOL File
93-17-4.mol
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(3,4-Dimethoxyphenyl)acetonitrile Property

Melting point:
54-57 °C(lit.)
Boiling point:
171-178 °C10 mm Hg(lit.)
Density 
1.1607 (rough estimate)
refractive index 
1.5168 (estimate)
Flash point:
>230 °F
storage temp. 
Sealed in dry,Room Temperature
solubility 
methanol: 0.1 g/mL, clear
form 
Crystals or Crystalline Needles
color 
yellow
Water Solubility 
insoluble
BRN 
1956100
Exposure limits
NIOSH: IDLH 25 mg/m3
InChIKey
ASLSUMISAQDOOB-UHFFFAOYSA-N
LogP
0.915
CAS DataBase Reference
93-17-4(CAS DataBase Reference)
NIST Chemistry Reference
Benzeneacetonitrile, 3,4-dimethoxy-(93-17-4)
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Safety

Hazard Codes 
Xn,T
Risk Statements 
22-23/24/25-36/37/38-20/21/22
Safety Statements 
36/37-45-22-36-26
RIDADR 
3276
WGK Germany 
3
RTECS 
AL9325000
HazardClass 
IRRITANT
HS Code 
29269090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
PHR2619
Product name
3,4-Dimethoxyphenylacetonitrile
Purity
Pharmaceutical Secondary Standard; Certified Reference Material
Packaging
100MG
Price
$400
Updated
2024/03/01
Sigma-Aldrich
Product number
126349
Product name
(3,4-Dimethoxyphenyl)acetonitrile
Purity
98%
Packaging
100g
Price
$74.4
Updated
2024/03/01
Sigma-Aldrich
Product number
126349
Product name
(3,4-Dimethoxyphenyl)acetonitrile
Purity
98%
Packaging
500g
Price
$419
Updated
2022/05/15
TCI Chemical
Product number
D1887
Product name
3,4-Dimethoxybenzyl Cyanide
Purity
>98.0%(GC)
Packaging
25g
Price
$25
Updated
2024/03/01
TCI Chemical
Product number
D1887
Product name
3,4-Dimethoxybenzyl Cyanide
Purity
>98.0%(GC)
Packaging
500g
Price
$191
Updated
2024/03/01
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(3,4-Dimethoxyphenyl)acetonitrile Chemical Properties,Usage,Production

Chemical Properties

white to almost white crystals or cryst. needles

Uses

(3,4-Dimethoxyphenyl)acetonitrile has been used in the synthesis of (Z)-3-(benzo[b]thiophen-2-yl)-2-(3,4-dimethoxyphenyl)acrylonitrile. It has also been used in the preparation of modified diterpene (±) nimbidiol which relies on a sulfenium ion promoted polyene cyclization.

Uses

An Impurity of Verapamil (V125000). An intermediate in the preparation of the muscle relaxant Papverine (P190500).

Synthesis Reference(s)

Journal of the American Chemical Society, 57, p. 1126, 1935 DOI: 10.1021/ja01309a053
Tetrahedron Letters, 24, p. 4533, 1983 DOI: 10.1016/S0040-4039(00)85947-X

Purification Methods

Its solubility is 10% in MeOH, and it has been recrystallised from EtOH or MeOH. Purify it also by distillation followed by recrystallisation. [Price & Rogers Org Synth Coll Vol III 174 1955, Niederl & Ziering J Am Chem Soc 64 885 1952, Julian & Sturgis J Am Chem Soc 57 1126 1935, Beilstein 10 I 198.]

(3,4-Dimethoxyphenyl)acetonitrile Preparation Products And Raw materials

Raw materials

1,2-Dimethoxybenzene

Preparation Products

5-chloro-2-(3,4-dimethoxyphenyl)-2-isopropylvaleronitrile 3,4-Dimethoxyphenethylamine
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(3,4-Dimethoxyphenyl)acetonitrile Suppliers

Americas 1 Belgium 2 Canada 3 China 382 Europe 3 France 2 Germany 4 India 42 Italy 1 Japan 4 Poland 1 Russia 1 Slovakia 1 South Korea 1 Switzerland 2 The Netherlands 1 Ukraine 1 United Kingdom 12 United States 43 Global 507
Toronto Research Chemicals
Tel
--
Fax
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Email
info@trc-canada.com
Country
Canada
ProdList
6038
Advantage
71
Kessler Chemical, Inc.
Tel
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Fax
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Email
gkessler@epix.net
Country
Canada
ProdList
558
Advantage
51
A Unisource India
Tel
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Fax
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Country
Canada
ProdList
619
Advantage
58
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View Lastest Price from (3,4-Dimethoxyphenyl)acetonitrile manufacturers

HEBEI SHENGSUAN CHEMICAL INDUSTRY CO.,LTD
Product
(3,4-Dimethoxyphenyl)acetonitrile 93-17-4
Price
US $100.00-75.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
5000
Release date
2024-08-21
WUHAN FORTUNA CHEMICAL CO., LTD
Product
(3,4-Dimethoxyphenyl)acetonitrile 93-17-4
Price
US $0.00/g
Min. Order
10g
Purity
98%
Supply Ability
10kgs/month
Release date
2021-10-28
Jinan Finer Chemical Co., Ltd
Product
(3,4-Dimethoxyphenyl)acetonitrile 93-17-4
Price
US $0.00/Kg/Drum
Min. Order
1ASSAYS
Purity
99%
Supply Ability
200mt/year
Release date
2021-07-08

93-17-4, (3,4-Dimethoxyphenyl)acetonitrileRelated Search:

Dimethyldimethoxysilane Dimethoxymethane 4-Methoxybenzyl cyanide Methoxyacetonitrile 2,6-Dimethoxybenzaldehyde 1,1-Dimethoxyethane Diphenyldimethoxysilane Acetonitrile (3-Methoxyphenyl)acetonitrile (3,4-Dimethoxyphenyl)acetic acid 2-(3,4-Dimethoxyphenyl)ethanol 3,4-Dimethoxyphenylacetone 3,4-Dimethoxyacetophenone Veratraldehyde acetonitrile POTASSIUM CYANIDE HYDROGEN CYANIDE 4-BENZYLOXY-3-METHOXYPHENYLACETONITRILE

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  • WLN: NC1R CO1 DO1
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  • BENZENEACETONITRILE,3,4-DIMETHOXY
  • 3,4-Dimethoxybenzylacetontrile
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  • Dobutamine Impurity 27
  • Verapamil Impurity 18
  • 93-17-4
  • Nitrogen Compounds
  • Organic Building Blocks
  • pH Sensitive Probes and Indicators
  • Alphabetical
  • ARYL ISOCYANATE
  • C10 to C27
  • BioChemical
  • Biochemicals and Reagents
  • Building Blocks
  • Fluorescent Probes, Labels, Particles and Stains
  • Fluorescent Indicators and Probes
  • Cyanides/Nitriles
  • Detection