(3,4-Dimethoxyphenyl)acetonitrile

Product Name: (3,4-Dimethoxyphenyl)acetonitrile
CAS No.: 93-17-4
Chemical Name: (3,4-Dimethoxyphenyl)acetonitrile
Synonyms: Homoveratronitrile;3,4-dimethoxybenzyl;3,4-Dimethoxybenzyl cyanide;NSC 6324;Veratryl cyanide;HOMOVERATONITRILE;WLN: NC1R CO1 DO1;Homoveratronitrite;TIMTEC-BB SBB005899;(3,4-Dimethoxyphenyl
CBNumber: CB3254471
Molecular Formula: C10H11NO2
Formula Weight: 177.2
MOL File: 93-17-4.mol

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(3,4-Dimethoxyphenyl)acetonitrile Property

Melting point:: 54-57 °C(lit.)
Boiling point:: 171-178 °C10 mm Hg(lit.)
Density: 1.1607 (rough estimate)
refractive index: 1.5168 (estimate)
Flash point:: >230 °F
storage temp.: Sealed in dry,Room Temperature
solubility: methanol: 0.1 g/mL, clear
form: Crystals or Crystalline Needles
color: yellow
Water Solubility: insoluble
BRN: 1956100
Exposure limits: NIOSH: IDLH 25 mg/m3
InChIKey: ASLSUMISAQDOOB-UHFFFAOYSA-N
LogP: 0.915
CAS DataBase Reference: 93-17-4(CAS DataBase Reference)
NIST Chemistry Reference: Benzeneacetonitrile, 3,4-dimethoxy-(93-17-4)

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Safety

Hazard Codes: Xn,T
Risk Statements: 22-23/24/25-36/37/38-20/21/22
Safety Statements: 36/37-45-22-36-26
RIDADR: 3276
WGK Germany: 3
RTECS: AL9325000
HazardClass: IRRITANT
HS Code: 29269090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word: Warning
Hazard statements: H302Harmful if swallowed

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: PHR2619
Product name: 3,4-Dimethoxyphenylacetonitrile
Purity: Pharmaceutical Secondary Standard; Certified Reference Material
Packaging: 100MG
Price: $400
Updated: 2024/03/01

Sigma-Aldrich

Product number: 126349
Product name: (3,4-Dimethoxyphenyl)acetonitrile
Purity: 98%
Packaging: 100g
Price: $74.4
Updated: 2024/03/01

Sigma-Aldrich

Product number: 126349
Product name: (3,4-Dimethoxyphenyl)acetonitrile
Purity: 98%
Packaging: 500g
Price: $419
Updated: 2022/05/15

TCI Chemical

Product number: D1887
Product name: 3,4-Dimethoxybenzyl Cyanide
Purity: >98.0%(GC)
Packaging: 25g
Price: $25
Updated: 2024/03/01

TCI Chemical

Product number: D1887
Product name: 3,4-Dimethoxybenzyl Cyanide
Purity: >98.0%(GC)
Packaging: 500g
Price: $191
Updated: 2024/03/01

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(3,4-Dimethoxyphenyl)acetonitrile Chemical Properties,Usage,Production

Chemical Properties

white to almost white crystals or cryst. needles

Uses

(3,4-Dimethoxyphenyl)acetonitrile has been used in the synthesis of (Z)-3-(benzo[b]thiophen-2-yl)-2-(3,4-dimethoxyphenyl)acrylonitrile. It has also been used in the preparation of modified diterpene (±) nimbidiol which relies on a sulfenium ion promoted polyene cyclization.

Uses

An Impurity of Verapamil (V125000). An intermediate in the preparation of the muscle relaxant Papverine (P190500).

Synthesis Reference(s)

Journal of the American Chemical Society, 57, p. 1126, 1935 DOI: 10.1021/ja01309a053
Tetrahedron Letters, 24, p. 4533, 1983 DOI: 10.1016/S0040-4039(00)85947-X

Purification Methods

Its solubility is 10% in MeOH, and it has been recrystallised from EtOH or MeOH. Purify it also by distillation followed by recrystallisation. [Price & Rogers Org Synth Coll Vol III 174 1955, Niederl & Ziering J Am Chem Soc 64 885 1952, Julian & Sturgis J Am Chem Soc 57 1126 1935, Beilstein 10 I 198.]

(3,4-Dimethoxyphenyl)acetonitrile Preparation Products And Raw materials

Raw materials

1,2-Dimethoxybenzene

Preparation Products

5-chloro-2-(3,4-dimethoxyphenyl)-2-isopropylvaleronitrile 3,4-Dimethoxyphenethylamine

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(3,4-Dimethoxyphenyl)acetonitrile Suppliers

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View Lastest Price from (3,4-Dimethoxyphenyl)acetonitrile manufacturers

HEBEI SHENGSUAN CHEMICAL INDUSTRY CO.,LTD

Product: (3,4-Dimethoxyphenyl)acetonitrile 93-17-4
Price: US $100.00-75.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 5000
Release date: 2024-08-21

WUHAN FORTUNA CHEMICAL CO., LTD

Product: (3,4-Dimethoxyphenyl)acetonitrile 93-17-4
Price: US $0.00/g
Min. Order: 10g
Purity: 98%
Supply Ability: 10kgs/month
Release date: 2021-10-28

Jinan Finer Chemical Co., Ltd

Product: (3,4-Dimethoxyphenyl)acetonitrile 93-17-4
Price: US $0.00/Kg/Drum
Min. Order: 1ASSAYS
Purity: 99%
Supply Ability: 200mt/year
Release date: 2021-07-08

93-17-4, (3,4-Dimethoxyphenyl)acetonitrileRelated Search:

Dimethyldimethoxysilane Dimethoxymethane 4-Methoxybenzyl cyanide Methoxyacetonitrile 2,6-Dimethoxybenzaldehyde 1,1-Dimethoxyethane Diphenyldimethoxysilane Acetonitrile (3-Methoxyphenyl)acetonitrile (3,4-Dimethoxyphenyl)acetic acid 2-(3,4-Dimethoxyphenyl)ethanol 3,4-Dimethoxyphenylacetone 3,4-Dimethoxyacetophenone Veratraldehyde acetonitrile POTASSIUM CYANIDE HYDROGEN CYANIDE 4-BENZYLOXY-3-METHOXYPHENYLACETONITRILE

3,4-Dimethoxylphenylacetonitrile

(3,4-Dimethoxyphenyl)acetonitrile, 3,4-Dimethoxybenzylcyanide, Homoveratronitrile

(3,4-Dimethoxyphenyl)acetonitrile, 3,4-Dimethoxybenzylcyanide

3,4-dimethoxy-benzeneacetonitril

3,4-dimethoxybenzeneacetonitrile

3,4-dimethoxybenzyl

3,4-dimethoxyphenyl-acetonitril

Acetonitrile, (3,4-dimethoxyphenyl)-

HOMOVERATONITRILE

3,5-DIMETHOXY-BENZENEACETONITRILE

4-Dimethoxybenzyl Cyanide

Homoveratronitrite

(3,4-Dimethoxyphenyl)acetonitrile in stock Factory

1-Cyanomethyl-3,4-dimethoxybenzene

(3,4-Dimethoxyphenyl

4-DiMethyloxy phenylacetonotrile

NSC 6324

(3,4-DiMethoxyphenyl) acetoniotrile

(3,4-DiMethoxyphenyl)acetonitrile, 99+% 25GR

Acetonitrile, (3,4-diMethoxyphenyl)- (6CI,7CI,8CI)

2-(3,4-dimethoxyphenyl)ethanenitrile

Benzeneacetonitrile, 3,4-dimethoxy- (9CI)

WLN: NC1R CO1 DO1

3,4-Dimethylbenzyl cyanide

3,4-Dimethoxyphenyl)acetoni

TIMTEC-BB SBB005899

3,5-DIMETHOXYPHENYLACETONITRILE

3,4-Dimethoxybenzyl Acetonitrile

Homoveratronitrile98%

(3,4-Dimethoxyphenyl)acetonitrile, 99+%

3,4-DIMETHOXYPHENYLACETONITRILE / HOMOVERATRONITRILE

Homoveratronitrile

Veratryl cyanide

BENZENEACETONITRILE,3,4-DIMETHOXY

3,4-Dimethoxybenzylacetontrile

(3,4-Dimethoxyphenyl)acetonitrile

3,4-Dimethoxybenzyl cyanide

3,4-dimethoxylphenethylacetonitrile

3,4-DimethoxybenzylCyanide&gt

Homo veratronitrile (HVN) (3,4-Dimethoxyphenyl) Acetonitrile

3,4-Dimethoxyphenyl acetonitrile (Homoveratryl nitrile)

Homo Veratonitrile(HVN)

Dobutamine Impurity 27

Verapamil Impurity 18

93-17-4

Nitrogen Compounds

Organic Building Blocks

pH Sensitive Probes and Indicators

Alphabetical

ARYL ISOCYANATE

C10 to C27

BioChemical

Biochemicals and Reagents

Building Blocks

Fluorescent Probes, Labels, Particles and Stains

Fluorescent Indicators and Probes

Cyanides/Nitriles

Detection