ChemicalBook > CAS DataBase List > 7-Methoxy-1,2,3,4-tetrahydroquinoline

7-Methoxy-1,2,3,4-tetrahydroquinoline

Product Name: 7-Methoxy-1,2,3,4-tetrahydroquinoline
CAS No.: 19500-61-9
Chemical Name: 7-Methoxy-1,2,3,4-tetrahydroquinoline
Synonyms: 1,2,3,4-tetrahydro-7-methoxyQuinoline;Quinoline, 1,2,3,4-tetrahydro-7-methoxy-
CBNumber: CB32651926
Molecular Formula: C10H13NO
Formula Weight: 163.22
MOL File: 19500-61-9.mol

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7-Methoxy-1,2,3,4-tetrahydroquinoline Property

storage temp.: Keep in dark place,Inert atmosphere,Room temperature
Appearance: Colorless to light yellow Liquid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: M845270
Product name: 7-Methoxy-1,2,3,4-tetrahydroquinoline
Packaging: 5mg
Price: $45
Updated: 2021/12/16

TRC

Product number: M845270
Product name: 7-Methoxy-1,2,3,4-tetrahydroquinoline
Packaging: 10mg
Price: $65
Updated: 2021/12/16

TRC

Product number: M845270
Product name: 7-Methoxy-1,2,3,4-tetrahydroquinoline
Packaging: 50mg
Price: $285
Updated: 2021/12/16

AK Scientific

Product number: J96342
Product name: 7-Methoxy-1,2,3,4-tetrahydroquinoline
Packaging: 5g
Price: $2743
Updated: 2021/12/16

Medical Isotopes, Inc.

Product number: 35398
Product name: 7-Methoxy-1,2,3,4-tetrahydroquinoline
Purity: 95+%
Packaging: 1000mg
Price: $1280
Updated: 2021/12/16

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7-Methoxy-1,2,3,4-tetrahydroquinoline Chemical Properties,Usage,Production

Synthesis

4964-76-5

19500-61-9

General procedure for the synthesis of 7-methoxy-1,2,3,4-tetrahydroquinoline from 7-methoxyquinoline: platinum oxide (PtO2, 180 mg, 0.79 mmol) was added to a methanol (60 mL) solution of 7-methoxyquinoline (2.0 g, 12.56 mmol). Hydrogen (H2) was passed into the above solution at room temperature and the reaction mixture was stirred overnight. Upon completion of the reaction, the solid catalyst was removed by filtration. The filtrate was concentrated under reduced pressure to give the crude product. The crude product was purified by silica gel column chromatography using a petroleum ether solution of 3% ethyl acetate as eluent to afford 7-methoxy-1,2,3,4-tetrahydroquinoline as a light yellow oil (1.5 g). Mass spectrum (M + H)+ m/z: 164.0. 1H-NMR (300 MHz, CD3OD) δ: 6.76 (d, J = 8.4 Hz, 1H), 6.09-6.17 (m, 2H), 3.69 (s, 3H), 3.19-3.23 (m, 2H), 2.64-2.69 (t, J = 6.6 Hz, 2H), 1.85 -1.93 (m, 2H).

References

[1] Patent: WO2012/58125, 2012, A1. Location in patent: Page/Page column 115; 116
[2] Patent: WO2012/94462, 2012, A2. Location in patent: Page/Page column 83
[3] Patent: WO2016/86200, 2016, A1. Location in patent: Page/Page column 278
[4] Farmaco, Edizione Scientifica, 1954, vol. 9, p. 205,209
[5] Bioorganic and Medicinal Chemistry Letters, 2006, vol. 16, # 13, p. 3415 - 3418

7-Methoxy-1,2,3,4-tetrahydroquinoline Preparation Products And Raw materials

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View Lastest Price from 7-Methoxy-1,2,3,4-tetrahydroquinoline manufacturers

Career Henan Chemical Co

Product: 7-Methoxy-1,2,3,4-tetrahydroquinoline 19500-61-9
Price: US $1.00/g
Min. Order: 1g
Purity: 99%
Supply Ability: g/kg/T
Release date: 2019-12-18

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19500-61-9