4-Bromobenzenesulfonamide
- Product Name
- 4-Bromobenzenesulfonamide
- CAS No.
- 701-34-8
- Chemical Name
- 4-Bromobenzenesulfonamide
- Synonyms
- AKOS 206-12;p-bromo-benzenesulfonamid;P-BROMOBENZENESULFONAMIDE;4-BROMOBENZENESULFONAMIDE;Bromo Benzene Sulphonamide;4-BROMOBENZENESULPHONAMIDE;Benzenesulfonamide, p-bromo-;Benzenesulfonamide, 4-bromo-;4-Bromobenzenesulphonamide 98%;4-Bromobenzenesulphonamide-98%
- CBNumber
- CB3379855
- Molecular Formula
- C6H6BrNO2S
- Formula Weight
- 236.09
- MOL File
- 701-34-8.mol
4-Bromobenzenesulfonamide Property
- Melting point:
- 163-167 °C
- Boiling point:
- 360.7°C (rough estimate)
- Density
- 1.8000 (estimate)
- refractive index
- 1.6140 (estimate)
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- solubility
- DMSO (Slightly), Methanol (Slightly)
- form
- Solid
- pka
- 9.89±0.10(Predicted)
- color
- White to Off-White
- Water Solubility
- 991.6mg/L(15 ºC)
- BRN
- 2691657
- InChIKey
- STYQHICBPYRHQK-UHFFFAOYSA-N
- CAS DataBase Reference
- 701-34-8(CAS DataBase Reference)
- NIST Chemistry Reference
- 4-Bromobenzenesulfonamide(701-34-8)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H301Toxic if swalloed
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- 16374
- Product name
- 4-Bromobenzenesulfonamide
- Purity
- ≥99.0% (T)
- Packaging
- 5g
- Price
- $51.66
- Updated
- 2024/03/01
- Product number
- 16374
- Product name
- 4-Bromobenzenesulfonamide
- Purity
- ≥99.0% (T)
- Packaging
- 100g
- Price
- $128
- Updated
- 2022/05/15
- Product number
- B682628
- Product name
- 4-Bromobenzenesulfonamide
- Packaging
- 500mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- 8669-9-X9
- Product name
- 4-Bromobenzenesulfonamide
- Purity
- 98.0%
- Packaging
- 25g
- Price
- $47
- Updated
- 2021/12/16
- Product number
- 023739
- Product name
- 4-Bromobenzenesulfonamide
- Purity
- 98%
- Packaging
- 100g
- Price
- $104
- Updated
- 2021/12/16
4-Bromobenzenesulfonamide Chemical Properties,Usage,Production
Uses
4-Bromobenzenesulfonamide was used as reagent in preparation of cobalt(III) complexes of N,R-sulfonyldithiocarbimate anion. It was also used in the synthesis of 2-, 3- and 4-(substituted-phenylethynyl)benzenesulfonamides.
General Description
4-Bromobenzenesulfonamide is a metabolite of ebrotidine, a new H2-receptor antagonist.
Synthesis
98-58-8
701-34-8
Preparation of 4-bromobenzenesulfonamide: 4-bromobenzenesulfonyl chloride (1.0 g, 3.9 mmol) was dissolved in methanol (5 mL), methanol/ammonia solution (5 mL, excess) was added, and the mixture was mixed in a 25 mL single-neck flask. The reaction mixture was stirred overnight at room temperature under nitrogen protection. On the next day, the reaction solution was concentrated under reduced pressure to give p-bromobenzenesulfonamide (1.13 g, 100% yield) as a white solid. The product was confirmed by ion spray mass spectrometry (m/z 235.9 [M*]) and could be used for subsequent reactions without further purification.
References
[1] Bioorganic and Medicinal Chemistry Letters, 2007, vol. 17, # 14, p. 3880 - 3885
[2] Patent: US2004/63680, 2004, A1
[3] Patent: US7034045, 2006, B1. Location in patent: Page/Page column 83
[4] Journal of Medicinal Chemistry, 2018, vol. 61, # 11, p. 4860 - 4882
[5] RSC Advances, 2014, vol. 4, # 24, p. 12119 - 12126
4-Bromobenzenesulfonamide Preparation Products And Raw materials
Raw materials
Preparation Products
4-Bromobenzenesulfonamide Suppliers
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View Lastest Price from 4-Bromobenzenesulfonamide manufacturers
- Product
- 4-Bromobenzenesulfonamide 701-34-8
- Price
- US $1.00-4.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 200000KG
- Release date
- 2025-09-04
- Product
- 4-Bromobenzenesulfonamide 701-34-8
- Price
- US $0.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 1000kg
- Release date
- 2025-05-08
- Product
- 4-Bromobenzenesulfonamide 701-34-8
- Price
- US $10.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 10 mt
- Release date
- 2025-03-13