N-Boc-N-methylethylenediamine

Uses

Product Name: N-Boc-N-methylethylenediamine
CAS No.: 121492-06-6
Chemical Name: N-Boc-N-methylethylenediamine
Synonyms: N-Boc-(2-Aminoethyl)-N-methylamine;tert-butyl 2-aminoethyl(methyl)carbamate;BOC,ME-EDA;CAS:121492-06-6;BUTTPARK 90\06-19;BOC-N-METHYLETHYLENEDIAMINE;N-(2-AMinoethyl)-N-Methylca;N-BOC-N-METHYLETHYLENEDIAMINE;1-BOC-1-METHYL-ETHYLENEDIAMINE;N-Boc-N-methyl-1,2-diaminoethane
CBNumber: CB3424935
Molecular Formula: C8H18N2O2
Formula Weight: 174.24
MOL File: 121492-06-6.mol

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N-Boc-N-methylethylenediamine Property

Melting point:: 248-251 °C (decomp)
Boiling point:: 79°C/0.4mmHg(lit.)
Density: 0.975 g/mL at 20 °C (lit.)
refractive index: n20/D 1.447
Flash point:: >100 °C
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
solubility: Chloroform (Slightly), Methanol (Slightly)
pka: 9.44±0.10(Predicted)
form: Liquid
color: Clear colorless to pale yellow
BRN: 3588326
InChI: InChI=1S/C8H18N2O2/c1-8(2,3)12-7(11)10(4)6-5-9/h5-6,9H2,1-4H3
InChIKey: QYJVBVKFXDHFPQ-UHFFFAOYSA-N
SMILES: C(OC(C)(C)C)(=O)N(CCN)C
CAS DataBase Reference: 121492-06-6(CAS DataBase Reference)

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Safety

Hazard Codes: C
Risk Statements: 34
Safety Statements: 26-36/37/39-45
RIDADR: 2734
WGK Germany: 3
HazardClass: 8
PackingGroup: Ⅲ
HS Code: 2924190090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H314Causes severe skin burns and eye damage

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P363Wash contaminated clothing before reuse.

P405Store locked up.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 15567
Product name: N-Boc-N-methylethylenediamine
Purity: ≥97.0% (GC)
Packaging: 1ml
Price: $130
Updated: 2023/06/20

Sigma-Aldrich

Product number: 15567
Product name: N-Boc-N-methylethylenediamine
Purity: ≥97.0% (GC)
Packaging: 5ml
Price: $181
Updated: 2022/05/15

TCI Chemical

Product number: B4277
Product name: N-(tert-Butoxycarbonyl)-N-methyl-1,2-ethylenediamine
Purity: >95.0%(GC)(T)
Packaging: 1mL
Price: $44
Updated: 2025/07/31

TCI Chemical

Product number: B4277
Product name: N-(tert-Butoxycarbonyl)-N-methyl-1,2-ethylenediamine
Purity: >95.0%(GC)(T)
Packaging: 5mL
Price: $132
Updated: 2025/07/31

Usbiological

Product number: 265320
Product name: Boc-N-methylethylenediamine
Packaging: 1g
Price: $350
Updated: 2021/12/16

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N-Boc-N-methylethylenediamine Chemical Properties,Usage,Production

Uses

N-Boc-N-methylethylenediamine is a compound useful in organic synthesis and other chemical processes.

Chemical Properties

Liquid

Uses

Mono-protected building block.

reaction suitability

reagent type: cross-linking reagent

Synthesis

24424-99-5

109-81-9

121492-06-6

Step 1: N-methylethylenediamine (11.8 mL, 134.9 mmol) was dissolved in acetonitrile (300 mL) and cooled to -30 °C. Subsequently, triethylamine (TEA, 7.46 mL, 53.9 mmol) was added to this solution, followed by dropwise addition of di-tert-butyl dicarbonate (Boc2O, 9.81 g, 45 mmol) in acetonitrile solution. The reaction mixture was stirred at room temperature for 2 hours. After completion of the reaction, the insoluble material was removed by Celite filtration. The filtrate was purified by silica gel column chromatography (elution gradient: 1:50→1:20→1:10 ethyl acetate/hexane) to afford tert-butyl N-(2-aminoethyl)-N-methylcarbamate (CXVIII) as a yellow oil (5.2 g, 29.9 mmol, 66% yield). The product was confirmed by electrospray ionization mass spectrometry (ESIMS) with molecular formula C8H18N2O2, m/z 175 (M + H).

References

[1] Patent: US2008/318957, 2008, A1. Location in patent: Page/Page column 72; 73
[2] Journal of Medicinal Chemistry, 2000, vol. 43, # 16, p. 3093 - 3102

N-Boc-N-methylethylenediamine Preparation Products And Raw materials

Raw materials

Preparation Products

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N-Boc-N-methylethylenediamine Suppliers

Americas 1 Canada 2 China 176 Europe 1 Germany 5 India 7 Japan 1 Switzerland 3 United Kingdom 14 United States 40 Global 250

Senn Chemicals AG.

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Email: sales@sennchem.com
Country: Switzerland
ProdList: 204
Advantage: 58

SIGMA-RBI

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Country: Switzerland
ProdList: 6896
Advantage: 91

Senn Chemicals AG

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Email: swiss@sennchem.com
Country: Switzerland
ProdList: 3143
Advantage: 71

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View Lastest Price from N-Boc-N-methylethylenediamine manufacturers

Hebei Chuanghai Biotechnology Co., Ltd

Product: N-Boc-N-methylethylenediamine 121492-06-6
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 20 mt
Release date: 2024-11-13

Career Henan Chemical Co

Product: N-Boc-N-methylethylenediamine 121492-06-6
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 1000KG
Release date: 2018-08-09

121492-06-6, N-Boc-N-methylethylenediamineRelated Search:

2-Butoxyethanol tert-Butyl peroxybenzoate Urethane Diethylene glycol monobutyl ether Diisobutyl phthalate N-METHYLETHYLENEDIAMINE tert-Butyl carbazate tert-Butyl acetate 4-Aminobenzoic acid N,N-Dimethylethylenediamine Methyl anthranilate 2-(2-Aminoethylamino)ethanol tert-Butyl 4-aminobenzoate N,N,N',N'-Tetramethylethylenediamine N-(1-Naphthyl)ethylenediamine dihydrochloride Butyl acrylate Thiophanate-methyl tert-Butanol

TERT-BUTYL N-(2-AMINOETHYL)-N-METHYLCARBAMATE

N-T-BUTYLOXYCARBONYL-N-METHYL-ETHYLENEDIAMINE

N-TERT-BUTYLOXYCARBONYL-N-METHYL-ETHYLENEDIAMINE

N-BOC-N-METHYLETHYLENEDIAMINE

N-(2-AMINOETHYL)-N-METHYL CARBAMIC ACID TERT-BUTYL ESTER

N-(2-AMINOETHYL)-N-BOC-METHYLAMINE

BOC,ME-EDA

BOC-N-METHYLETHYLENEDIAMINE

BUTTPARK 90\06-19

(2-AMINO-ETHYL)-METHYL-CARBAMIC ACID TERT-BUTYL ESTER

1-BOC-1-METHYL-ETHYLENEDIAMINE

N-(2-Aminoethyl)-N-methyl carbamic acid tert-butyl

N-Boc-(2-Aminoethyl)-N-methylamine

Carbamic acid, N-(2-aminoethyl)-N-methyl-, 1,1-dimethylethyl ester

N-Boc-N-methylethylenediamine ,98%

tert-butyl 2-aminoethyl(methyl)carbamate

tert-butyl (2-aminoethyl)methylcarbamate(SALTDATA: FREE)

2-(N-Boc-N-methylamino)ethylamine

1-BOC-1-methyl-ethylenediamine-HCl

2-Methylpropan-2-yl N-(2-AMinoethyl)-N-MethylcarbaMate

N-(2-AMinoethyl)-N-Methylca

N-(2-AMinoethyl)-N-Methyl-carbaMic Acid 1,1-DiMethylethyl Ester

N-(2-AMinoethyl)-N-Methyl-N-(tert-butoxycarbonyl)aMine

N-(tert-Butoxycarbonyl)-N-methylethane-1,2-diamine, tert-Butyl (2-aminoethyl)methylcarbamate

N-Methylethane-1,2-diamine, N-BOC protected

N-(tert-Butoxycarbonyl)-N-methyl-1,2-ethylenediamine

N1-BOC-N1-METHYL-1,2-ETHYLENEDIAMINE

Boc-N-methylethylenediamine≥ 98% (GC)

N-(tert-Butoxycarbonyl)-N-methyl-1,2-ethylenediamine &gt

N-(tert-Butoxycarbonyl)-N-methyl-1,2-diaminoethane

N-Boc-N-methyl-1,2-diaminoethane

N-Boc-N-methyl-1,2-ethylenediamine

N-Boc-N-methylethylenediamine USP/EP/BP

N-Boc-N-methylethylenediamine 121492-06-6

2-Methyl-2-propanyl (2-aminoethyl)methylcarbamate

CAS:121492-06-6

<i>N</i>-Boc-<i>N</i>-methylethylenediamine

121492-06-6

Building Blocks

Nitrogen Compounds

Organic Building Blocks

Protected Amines

Bifunctional Linkers

Building Blocks

Chemical Biology

Chemical Synthesis

Linkers and Crosslinkers

Nitrogen Compounds

Organic Building Blocks

Protected Amines

Small molecule