ChemicalBook > CAS DataBase List > METHYL-2-BROMO-4-BROMOMETHYLBENZOATE

METHYL-2-BROMO-4-BROMOMETHYLBENZOATE

Product Name: METHYL-2-BROMO-4-BROMOMETHYLBENZOATE
CAS No.: 128577-48-0
Chemical Name: METHYL-2-BROMO-4-BROMOMETHYLBENZOATE
Synonyms: CAS:128577-48-0;Methyl 2-bromo-4-(bromomethyl);METHYL-2-BROMO-4-BROMOMETHYLBENZOATE;Benzoic acid, 2-bromo-4-(bromomethyl)-, methyl ester
CBNumber: CB3491995
Molecular Formula: C9H8Br2O2
Formula Weight: 307.97
MOL File: 128577-48-0.mol

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METHYL-2-BROMO-4-BROMOMETHYLBENZOATE Property

Melting point:: 53 - 56°C
Boiling point:: 340.3±32.0 °C(Predicted)
Density: 1.780±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
solubility: Chloroform (Slightly), Ethyl Acetate (Soluble)
form: Solid
color: White to Off-White
Stability:: Hygroscopic, Moisture Sensitive
InChI: InChI=1S/C9H8Br2O2/c1-13-9(12)7-3-2-6(5-10)4-8(7)11/h2-4H,5H2,1H3
InChIKey: ZTDXOVAPGGNGSD-UHFFFAOYSA-N
SMILES: C(OC)(=O)C1=CC=C(CBr)C=C1Br

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Safety

HS Code: 2916399090

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: M296273
Product name: Methyl-2-bromo-4-bromomethylbenzoate
Packaging: 100mg
Price: $45
Updated: 2021/12/16

TRC

Product number: M296273
Product name: Methyl-2-bromo-4-bromomethylbenzoate
Packaging: 500mg
Price: $65
Updated: 2021/12/16

TRC

Product number: M296273
Product name: Methyl-2-bromo-4-bromomethylbenzoate
Packaging: 1g
Price: $75
Updated: 2021/12/16

Usbiological

Product number: 456025
Product name: Methyl-2-bromo-4-bromomethylbenzoate
Packaging: 100mg
Price: $305
Updated: 2021/12/16

Matrix Scientific

Product number: 119646
Product name: Methyl 2-bromo-4-(bromomethyl)benzoate
Purity: 95+%
Packaging: 5g
Price: $390
Updated: 2021/12/16

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METHYL-2-BROMO-4-BROMOMETHYLBENZOATE Chemical Properties,Usage,Production

Synthesis

87808-49-9

128577-48-0

General procedure for the synthesis of methyl 2-bromo-4-bromomethylbenzoate from methyl 2-bromo-4-methylbenzoate: the reaction mixture was placed in a controlled microwave synthesizer of the model Biotage Initiator + SP Wave (power range 0-200 W, frequency 2.45 GHz, 60 W capped at steady state) and heated to 120 °C at 1 bar pressure for for several minutes. Upon completion of the reaction, the target product was isolated and purified by column chromatography using ethyl acetate-hexane gradient elution.

References

[1] Synlett, 2014, vol. 25, # 17, p. 2485 - 2487
[2] Patent: WO2016/89062, 2016, A2. Location in patent: Page/Page column 38; 39
[3] Patent: US2005/70584, 2005, A1. Location in patent: Page/Page column 24
[4] Patent: WO2008/124575, 2008, A1. Location in patent: Page/Page column 144
[5] Patent: WO2017/156165, 2017, A1. Location in patent: Paragraph 00504; 00505

METHYL-2-BROMO-4-BROMOMETHYLBENZOATE Preparation Products And Raw materials

Raw materials

Preparation Products

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METHYL-2-BROMO-4-BROMOMETHYLBENZOATE Suppliers

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128577-48-0, METHYL-2-BROMO-4-BROMOMETHYLBENZOATERelated Search:

4-(BROMOMETHYL)BENZALDEHYDE 3-BROMO-4-METHYL BENZALDEHYDE METHYL-2-BROMO-4-BROMOMETHYLBENZOATE 2-Bromo-4-methylbenzoic acid 4-Bromomethylbenzoic acid Methyl 4-(bromomethyl)benzoate METHYL 2-BROMO-4-METHYLBENZOATE

Methyl 2-bromo-4-(bromomethyl)

METHYL-2-BROMO-4-BROMOMETHYLBENZOATE

Benzoic acid, 2-bromo-4-(bromomethyl)-, methyl ester

CAS:128577-48-0

128577-48-0