ChemicalBook > CAS DataBase List > 2,4,6-Trichloro-5-methylpyrimidine

2,4,6-Trichloro-5-methylpyrimidine

Product Name
2,4,6-Trichloro-5-methylpyrimidine
CAS No.
1780-36-5
Chemical Name
2,4,6-Trichloro-5-methylpyrimidine
Synonyms
2,4,6-Trichoro-5-MethylpyriMidine;2,4,6-TRICHLORO-5-METHYLPYRIMIDINE;5-Methyl-2,4,6-trichloropyrimidine;Pyrimidine, 2,4,6-trichloro-5-methyl-;5-Methyl-2,4,6-trichloropyrimidine 98%;2,4,6-TRICHLORO-5-METHYLPYRIMIDINE, 98+%;2,4,6-Trichloro-5-MethylpyriMidine;2,4,6-Trichloro-5-methylpyrimidine ISO 9001:2015 REACH
CBNumber
CB3496309
Molecular Formula
C5H3Cl3N2
Formula Weight
197.45
MOL File
1780-36-5.mol
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2,4,6-Trichloro-5-methylpyrimidine Property

Melting point:
65-69 °C
Boiling point:
132-136 °C(Press: 23-25 Torr)
Density 
1.542±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Sealed in dry,Room Temperature
form 
solid
pka
-6.75±0.39(Predicted)
color 
Off-white
CAS DataBase Reference
1780-36-5(CAS DataBase Reference)
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Safety

Hazard Codes 
C
Risk Statements 
22-34
Safety Statements 
26-36/37/39-45
RIDADR 
UN 3261
WGK Germany 
3
HazardClass 
8
PackingGroup 
HS Code 
29335990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H302Harmful if swallowed

H314Causes severe skin burns and eye damage

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P270Do not eat, drink or smoke when using this product.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
679054
Product name
2,4,6-Trichloro-5-methylpyrimidine
Purity
97%
Packaging
1g
Price
$112
Updated
2023/06/20
TRC
Product number
T774393
Product name
2,4,6-Trichloro-5-methylpyrimidine
Packaging
1g
Price
$65
Updated
2021/12/16
Matrix Scientific
Product number
073214
Product name
2,4,6-Trichloro-5-methylpyrimidine
Purity
95+%
Packaging
1g
Price
$35
Updated
2021/12/16
Frontier Specialty Chemicals
Product number
JK901784
Product name
2,4,6-Trichloro-5-methylpyrimidine
Purity
98%
Packaging
250mg
Price
$40
Updated
2021/12/16
Biosynth Carbosynth
Product number
NT67801
Product name
2,4,6-Trichloro-5-methylpyrimidine
Packaging
10g
Price
$72.5
Updated
2021/12/16
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2,4,6-Trichloro-5-methylpyrimidine Chemical Properties,Usage,Production

Synthesis

2565-47-1

1780-36-5

1. 450 mL (2.94 mol) of phosphorus trichloride was added to a 2-liter flask and 49.3 mL (0.39 mol) of N,N-dimethylaniline was added slowly while cooling and stirring. 2. 142 g (1 mol) of 1-methylpyrimidine-2,4,6(1H,3H,5H)-trione was added in a batch over 20 min and the reaction was exothermic. 3. the reaction mixture was heated to reflux and held for 5 hours until gas escape ceased. 4. the reaction suspension is slowly poured into water at a controlled temperature of 25°C to 30°C 5. Filter the aqueous suspension by suction and dissolve the filtrate in 250 mL of dichloromethane. 6. Filter the solution until clear and extract twice with 250 mL of ice water. 7. The organic phase was dried and concentrated by evaporation to give a crystalline residue. 8. the residue was dried under vacuum to give 126.7 g of 5-methyl-2,4,6-trichloropyrimidine crystals with a melting point of 67°C-68°C and a yield of 64.2% of the theoretical value.

References

[1] Patent: US4741760, 1988, A

2,4,6-Trichloro-5-methylpyrimidine Preparation Products And Raw materials

Raw materials

Preparation Products

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2,4,6-Trichloro-5-methylpyrimidine Suppliers

J & K SCIENTIFIC LTD.
Tel
18210857532; 18210857532
Fax
86-10-82849933
Email
jkinfo@jkchemical.com
Country
China
ProdList
96815
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76
Alfa Aesar
Tel
400-6106006
Fax
021-67582001/03/05
Email
saleschina@alfa-asia.com
Country
China
ProdList
30123
Advantage
84
Energy Chemical
Tel
021-021-58432009 400-005-6266
Fax
021-58436166
Email
sales8178@energy-chemical.com
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China
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44801
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Wuhan Chemwish Technology Co., Ltd
Tel
86-027-67849912
Fax
86-027-87531808
Email
sales@chemwish.com
Country
China
ProdList
35896
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Capot Chemical Co., Ltd
Tel
+86 (0) 571 85 58 67 18
Fax
0086-571-85864795
Country
China
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JinYan Chemicals(ShangHai) Co.,Ltd.
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13817811078
Fax
86-021-50426522,50426273
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sales@jingyan-chemical.com
Country
China
ProdList
9976
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Nanjing Habo Medical Technology Co., Ltd.
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025-85760892 13376080562
Fax
025-85766769
Email
sales@habotech.com
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China
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Pure Chemistry Scientific Inc.
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001-857-928-2050 or 1-888-588-9418
Fax
001-617-206-9595
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sales@chemreagents.com
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United States
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Accela ChemBio Co.,Ltd.
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021-50795510 4000665055
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021-50795055
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sales@accelachem.com
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China
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Shanghai Longsheng chemical Co.,Ltd.
Tel
021-58099652-8005 13585536065
Fax
021-58099609
Email
bin.wu@shlschem.com
Country
China
ProdList
9883
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View Lastest Price from 2,4,6-Trichloro-5-methylpyrimidine manufacturers

Hebei Zhuanglai Chemical Trading Co Ltd
Product
2,4,6-Trichloro-5-methylpyrimidine 1780-36-5
Price
US $100.00-50.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
20 tons
Release date
2024-11-12
Hebei Chuanghai Biotechnology Co., Ltd
Product
2,4,6-Trichloro-5-methylpyrimidine 1780-36-5
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
500000kg
Release date
2024-10-28
Dideu Industries Group Limited
Product
2,4,6-Trichloro-5-methylpyrimidine 1780-36-5
Price
US $1.10/g
Min. Order
1g
Purity
99.00%
Supply Ability
100 Tons Min
Release date
2021-12-06

1780-36-5, 2,4,6-Trichloro-5-methylpyrimidineRelated Search:


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