ChemicalBook > CAS DataBase List > 2-Bromo-3-nitroanisole

2-Bromo-3-nitroanisole

Uses

Product Name: 2-Bromo-3-nitroanisole
CAS No.: 67853-37-6
Chemical Name: 2-Bromo-3-nitroanisole
Synonyms: TIMTEC-BB SBB008642;2-BROMO-3-NITROANISOLE;2-Bromo-3-nitroanisole 99%;2-Bromo-3-methoxynitrobenzene;2-BROMO-1-METHOXY-3-NITROBENZENE;Benzene, 2-bromo-1-methoxy-3-nitro-;2-Bromo-3-nitroanisole ISO 9001：2015 REACH;2-Bromo-3-methoxynitrobenzene, 2-Bromo-1-methoxy-3-nitrobenzene, 2-Bromo-3-nitrophenyl methyl ether
CBNumber: CB4109787
Molecular Formula: C7H6BrNO3
Formula Weight: 232.03
MOL File: 67853-37-6.mol

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2-Bromo-3-nitroanisole Property

Boiling point:: 273.3±20.0 °C(Predicted)
Density: 1.640±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
form: powder
color: Yellow
InChI: InChI=1S/C7H6BrNO3/c1-12-6-4-2-3-5(7(6)8)9(10)11/h2-4H,1H3
InChIKey: KCFDURKFXBLIAY-UHFFFAOYSA-N
SMILES: C1(OC)=CC=CC([N+]([O-])=O)=C1Br
CAS DataBase Reference: 67853-37-6(CAS DataBase Reference)

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Safety

Hazard Codes: Xi,Xn
Risk Statements: 20/21/22-22
Safety Statements: 26-36/37/39
Hazard Note: Irritant
HS Code: 2909309090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: TMT00303
Product name: 2-Bromo-1-methoxy-3-nitrobenzene
Packaging: 1g
Price: $550
Updated: 2025/07/31

TRC

Product number: B688108
Product name: 2-Bromo-3-nitroanisole
Packaging: 100mg
Price: $45
Updated: 2021/12/16

TRC

Product number: B688108
Product name: 2-Bromo-3-nitroanisole
Packaging: 250mg
Price: $55
Updated: 2021/12/16

TRC

Product number: B688108
Product name: 2-Bromo-3-nitroanisole
Packaging: 500mg
Price: $65
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB139753
Product name: 2-Bromo-1-methoxy-3-nitrobenzene
Packaging: 5G
Price: $60
Updated: 2021/12/16

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2-Bromo-3-nitroanisole Chemical Properties,Usage,Production

Uses

2-Bromo-3-nitroanisole belongs to the class of bromoanisoles and can be used to synthesize rhodopsin coupling promoters and new drugs.

Synthesis

101935-40-4

74-88-4

67853-37-6

General procedure for the synthesis of 2-bromo-3-nitroanisole from 2-bromo-3-nitrophenol (3.1 g, 14.2 mmol) and iodomethane (2.6 mL, 42.5 mmol): 2-bromo-3-nitrophenol was dissolved in N,N-dimethylformamide (DMF, 20 mL), to which was added ground cesium carbonate (5.58 g, 17.1 mmol), followed by the addition of iodomethane. The reaction mixture was stirred at room temperature overnight. After completion of the reaction, DMF was removed by rotary evaporator and the residue was dissolved in ether (200 mL) and washed sequentially with water (200 mL) and saturated sodium chloride solution (4 x 100 mL). The organic phase was dried with anhydrous magnesium sulfate, filtered and concentrated to give the crude product 2-bromo-3-nitroanisole (94% yield, 3.1 g) as an orange solid. Mass spectrometry (MS) analysis showed m/z 234 ([M+2H]+). High performance liquid chromatography (HPLC, TFA system, 220 nm detection) showed a product purity of 98%.

References

[1] Patent: WO2004/103996, 2004, A1. Location in patent: Page 40-41
[2] Patent: WO2006/7700, 2006, A1. Location in patent: Page/Page column 62
[3] Patent: US2006/19905, 2006, A1. Location in patent: Page/Page column 24
[4] Patent: WO2006/85, 2006, A1. Location in patent: Page/Page column 75-76
[5] Patent: WO2007/9227, 2007, A1. Location in patent: Page/Page column 35

2-Bromo-3-nitroanisole Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-Bromo-3-nitroanisole manufacturers

Henan Fengda Chemical Co., Ltd

Product: 2-Bromo-3-nitroanisole 67853-37-6
Price: US $100.00-1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: g-kg-tons, free sample is available
Release date: 2023-12-26

Shaanxi Dideu Medichem Co. Ltd

Product: 2-Bromo-3-nitroanisole 67853-37-6
Price: US $0.00-0.00/Kg
Min. Order: 1KG
Purity: 99.0%
Supply Ability: 100 tons
Release date: 2020-01-10

Career Henan Chemical Co

Product: 2-Bromo-3-nitroanisole 67853-37-6
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: Customized
Release date: 2019-05-23

67853-37-6, 2-Bromo-3-nitroanisoleRelated Search:

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2-BROMO-1-METHOXY-3-NITROBENZENE

2-BROMO-3-NITROANISOLE

TIMTEC-BB SBB008642

2-Bromo-3-nitroanisole 99%

2-Bromo-3-methoxynitrobenzene, 2-Bromo-1-methoxy-3-nitrobenzene, 2-Bromo-3-nitrophenyl methyl ether

2-Bromo-3-methoxynitrobenzene

Benzene, 2-bromo-1-methoxy-3-nitro-

2-Bromo-3-nitroanisole ISO 9001：2015 REACH

67853-37-6

C7H6NO3Br

Anisoles, Alkyloxy Compounds & Phenylacetates

Bromine Compounds

Nitro Compounds

Anisole