1-(1-Methyl-2-piperidinyl)acetone

ChemicalBook > CAS DataBase List > 1-(1-Methyl-2-piperidinyl)acetone

1-(1-Methyl-2-piperidinyl)acetone

Product Name: 1-(1-Methyl-2-piperidinyl)acetone
CAS No.: 18747-42-7
Chemical Name: 1-(1-Methyl-2-piperidinyl)acetone
Synonyms: Methylisopunicine;Methylisopelletierine;N-Methylisopelletierine;(+/-)-1-Methylpelletierine;1-(1-Methyl-2-piperidinyl)acetone;1-(1-methylpiperidin-2-yl)propan-2-one;1-(1-Methyl-2-piperidinyl)-2-propanone;2-Propanone, 1-(1-methyl-2-piperidinyl)-
CBNumber: CB41237281
Molecular Formula: C9H17NO
Formula Weight: 155.24
MOL File: 18747-42-7.mol

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1-(1-Methyl-2-piperidinyl)acetone Property

Boiling point:: 217℃
Density: 0.920
refractive index: 1.4674
Flash point:: 67℃
storage temp.: Refrigerator
solubility: Chloroform (Slightly), DMSO (Slightly), Ethanol (Slightly)
form: Oil
pka: 9.53±0.10(Predicted)
color: Orange to Very Dark Orange

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: M223080
Product name: Methylisopelletierine
Packaging: 50mg
Price: $175
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: PXT0005157
Product name: METHYLISOPELLETIERINE
Purity: 95.00%
Packaging: 5MG
Price: $498.04
Updated: 2021/12/16

Crysdot

Product number: CD32002150
Product name: Methylisopelletierine
Purity: 95+%
Packaging: 5mg
Price: $590
Updated: 2021/12/16

Arctom

Product number: AS365294
Product name: Methylisopelletierine
Purity: ≥98%
Packaging: 5mg
Price: $226
Updated: 2021/12/16

Arctom

Product number: CFN99865
Product name: Methylisopelletierine
Packaging: 5mg
Price: $373
Updated: 2021/12/16

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1-(1-Methyl-2-piperidinyl)acetone Chemical Properties,Usage,Production

Description

This alkaloid occurs in the bark of Punica Granatum L. and was first isolated by Piccinini under the name of isomethylpelletierine. The base is an oily liquid with an alkaline reaction, miscible with H20 and optically inactive. The hydrochloride has m.p. lS6°C; the hydrobromide, m.p. lSI-2°C; the aurichloride forms rosettes of orange-yellow needles, m.p. lIS-7°C and the picrate has m.p. lS7-8°C. The alkaloid may be resolved into its optically active components. (+)-methy1isopelletierine (+)-hydrogen tartrate has m.p. 133-4°C; [α]²⁰_D + 22.7°, the corresponding figures for the antipode being m.p. 132-40c;~aH)S - 20.83° while the two hydrochlorides have [α]¹⁸_D + 11.08° and - 10.64° respectively.
The base gives a semicarbazone as colourless crystals, m.p. 169°C; an oxime, b.p. 1600C/12 mm and a hydrazone, b.p. lS4-SoC/29 mm. The methiodide yields cubic crystals, m.p. lS6°C. Oxidation with chromic acid in H2S04 furnishes N-methylpiperidine-2-carboxylic acid.

Definition

ChEBI: N-Methylpelletierine is a citraconoyl group.

References

Piccinini., Gazzetta, 29, ii, 311 (1899)
Hess et al., Ber., SO, 344, 1386 (1917)
Hess et al., ibid, 51,741 (1918)
Hess et al., ibid, 52, 964, 100S (1919)

1-(1-Methyl-2-piperidinyl)acetone Preparation Products And Raw materials

Raw materials

Preparation Products

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18747-42-7