ChemicalBook > CAS DataBase List > 1-(1-Methyl-2-piperidinyl)acetone

1-(1-Methyl-2-piperidinyl)acetone

Product Name
1-(1-Methyl-2-piperidinyl)acetone
CAS No.
18747-42-7
Chemical Name
1-(1-Methyl-2-piperidinyl)acetone
Synonyms
Methylisopunicine;Methylisopelletierine;N-Methylisopelletierine;(+/-)-1-Methylpelletierine;1-(1-Methyl-2-piperidinyl)acetone;1-(1-methylpiperidin-2-yl)propan-2-one;1-(1-Methyl-2-piperidinyl)-2-propanone;2-Propanone, 1-(1-methyl-2-piperidinyl)-
CBNumber
CB41237281
Molecular Formula
C9H17NO
Formula Weight
155.24
MOL File
18747-42-7.mol
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1-(1-Methyl-2-piperidinyl)acetone Property

Boiling point:
217℃
Density 
0.920
refractive index 
1.4674
Flash point:
67℃
storage temp. 
Refrigerator
solubility 
Chloroform (Slightly), DMSO (Slightly), Ethanol (Slightly)
form 
Oil
pka
9.53±0.10(Predicted)
color 
Orange to Very Dark Orange
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC
Product number
M223080
Product name
Methylisopelletierine
Packaging
50mg
Price
$175
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
PXT0005157
Product name
METHYLISOPELLETIERINE
Purity
95.00%
Packaging
5MG
Price
$498.04
Updated
2021/12/16
Crysdot
Product number
CD32002150
Product name
Methylisopelletierine
Purity
95+%
Packaging
5mg
Price
$590
Updated
2021/12/16
Arctom
Product number
AS365294
Product name
Methylisopelletierine
Purity
≥98%
Packaging
5mg
Price
$226
Updated
2021/12/16
Arctom
Product number
CFN99865
Product name
Methylisopelletierine
Packaging
5mg
Price
$373
Updated
2021/12/16
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1-(1-Methyl-2-piperidinyl)acetone Chemical Properties,Usage,Production

Description

This alkaloid occurs in the bark of Punica Granatum L. and was first isolated by Piccinini under the name of isomethylpelletierine. The base is an oily liquid with an alkaline reaction, miscible with H20 and optically inactive. The hydrochloride has m.p. lS6°C; the hydrobromide, m.p. lSI-2°C; the aurichloride forms rosettes of orange-yellow needles, m.p. lIS-7°C and the picrate has m.p. lS7-8°C. The alkaloid may be resolved into its optically active components. (+)-methy1isopelletierine (+)-hydrogen tartrate has m.p. 133-4°C; [α]20D + 22.7°, the corresponding figures for the antipode being m.p. 132-40c;~aH)S - 20.83° while the two hydrochlorides have [α]18D + 11.08° and - 10.64° respectively.
The base gives a semicarbazone as colourless crystals, m.p. 169°C; an oxime, b.p. 1600C/12 mm and a hydrazone, b.p. lS4-SoC/29 mm. The methiodide yields cubic crystals, m.p. lS6°C. Oxidation with chromic acid in H2S04 furnishes N-methylpiperidine-2-carboxylic acid.

Definition

ChEBI: N-Methylpelletierine is a citraconoyl group.

References

Piccinini., Gazzetta, 29, ii, 311 (1899)
Hess et al., Ber., SO, 344, 1386 (1917)
Hess et al., ibid, 51,741 (1918)
Hess et al., ibid, 52, 964, 100S (1919)

1-(1-Methyl-2-piperidinyl)acetone Preparation Products And Raw materials

Raw materials

Preparation Products

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1-(1-Methyl-2-piperidinyl)acetone Suppliers

China 54 United States 6 Global 60
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  • 1-(1-Methyl-2-piperidinyl)acetone
  • 1-(1-methylpiperidin-2-yl)propan-2-one
  • Methylisopelletierine
  • (+/-)-1-Methylpelletierine
  • 1-(1-Methyl-2-piperidinyl)-2-propanone
  • Methylisopunicine
  • N-Methylisopelletierine
  • 2-Propanone, 1-(1-methyl-2-piperidinyl)-
  • 18747-42-7