ChemicalBook > CAS DataBase List > 4-AMINO-3,5-DIIODOPYRIDINE

4-AMINO-3,5-DIIODOPYRIDINE

Product Name
4-AMINO-3,5-DIIODOPYRIDINE
CAS No.
98136-86-8
Chemical Name
4-AMINO-3,5-DIIODOPYRIDINE
Synonyms
3,5-Diiodopyridin-4-amine;4-AMINO-3,5-DIIODOPYRIDINE;3,4-diiodo-4-aminopyridine;3,5-diiodo-4-aminopyridine;4-Pyridinamine, 3,5-diiodo-;Pyridine,4-aMino-3,5-diiodo-;4-AMINO-3,5-DIIODOPYRIDINE ISO 9001:2015 REACH
CBNumber
CB4129112
Molecular Formula
C5H4I2N2
Formula Weight
345.91
MOL File
98136-86-8.mol
More
Less

4-AMINO-3,5-DIIODOPYRIDINE Property

Melting point:
135-136℃
Boiling point:
408.1±45.0 °C(Predicted)
Density 
2.679
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
pka
5.42±0.24(Predicted)
form 
solid
Appearance
White to off-white Solid
More
Less

Safety

Hazard Codes 
Xi,Xn
Risk Statements 
22
WGK Germany 
3
Hazard Note 
Irritant
HS Code 
2933399990
More
Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

More
Less

N-Bromosuccinimide Price

Sigma-Aldrich
Product number
VBP00076
Product name
3,5-Diiodopyridin-4-amine
Purity
Aldrich
Packaging
1g
Price
$179
Updated
2025/07/31
TRC
Product number
A632038
Product name
4-Amino-3,5-diiodopyridine
Packaging
100mg
Price
$60
Updated
2021/12/16
TRC
Product number
A632038
Product name
4-Amino-3,5-diiodopyridine
Packaging
500mg
Price
$130
Updated
2021/12/16
Apolloscientific
Product number
OR9959
Product name
4-Amino-3,5-diiodopyridine
Packaging
1g
Price
$56
Updated
2021/12/16
SynQuest Laboratories
Product number
3H30-H-X2
Product name
4-Amino-3,5-diiodopyridine
Packaging
1g
Price
$90
Updated
2021/12/16
More
Less

4-AMINO-3,5-DIIODOPYRIDINE Chemical Properties,Usage,Production

Synthesis

504-24-5

98136-86-8

General procedure for the synthesis of 3,5-diiodo-4-aminopyridine from 4-aminopyridine: 500 mL of methanol, 3000 mL of water, 94.11 g (1.0 mol) of 4-aminopyridine, 224.10 g (1.35 mol) of potassium iodide, and 149.80 g (0.70 mol) of potassium iodate were added sequentially to the reaction flask. 160 mL of hydrochloric acid was slowly added dropwise with controlled titration rate, and the titration process lasted for 3 hours. After the dropwise addition, the reaction was continued for 1 hour. Subsequently, 50 mL of an aqueous solution containing 17.73 g (0.20 mol) of sodium chlorite was added dropwise. After the dropwise addition was completed, the reaction process was monitored by HPLC and the reaction was continued for 0.5 hours. Upon completion of the reaction, the reaction solution was diluted with 4000 mL of water, and then 6000 mg of trichloromethane was added in three portions as an extractant. The organic phase was washed sequentially with an aqueous solution containing sodium thiosulfate and an aqueous solution of sodium bicarbonate, separated and dried with anhydrous magnesium sulfate. The solvent was removed by concentration under reduced pressure to give the crude product of 3,5-diiodo-4-aminopyridine in gray color. The crude product was recrystallized with a mixed solvent of ethanol and water to give 318.23 g of white crystalline solid in 92.0% yield.

References

[1] Patent: CN104262242, 2016, B. Location in patent: Paragraph 0030; 0031
[2] Tetrahedron Letters, 2007, vol. 48, # 11, p. 1983 - 1986

4-AMINO-3,5-DIIODOPYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

More
Less

4-AMINO-3,5-DIIODOPYRIDINE Suppliers

JinYan Chemicals(ShangHai) Co.,Ltd.
Tel
13817811078
Fax
86-021-50426522,50426273
Email
sales@jingyan-chemical.com
Country
China
ProdList
9976
Advantage
60
Chengdu Forest Science and Technology Development Co., Ltd.
Tel
18030648795
Fax
028-61777050
Email
sales@cdforestchem.com
Country
China
ProdList
2000
Advantage
58
Chiba Pharmaceutical Science and technology Co, Ltd.
Tel
0531-81313138 13066006660
Fax
QQ: 3366077777
Email
chibapharm@foxmail.com
Country
China
ProdList
3991
Advantage
55
Shijiazhuang suchen Chemical Technology Co. LTD
Tel
186-33933494 18032288352
Fax
0311-85310887
Email
1130239@qq.com
Country
China
ProdList
202
Advantage
60
Shanghai T&W Pharmaceutical Co., Ltd.
Tel
+86 21 61551611
Fax
+86 21 50676805
Country
China
ProdList
9891
Advantage
58
Shanghai Yolne Chemical Co., Ltd.
Tel
021-62960152
Fax
021-52212593
Email
934678158@qq.com
Country
China
ProdList
9899
Advantage
55
Bide Pharmatech Ltd.
Tel
400-164-7117 13681763483
Fax
+86-21-61629029
Email
product02@bidepharm.com
Country
China
ProdList
39966
Advantage
60
ShangHai AmK Pharmaceutical Technology Co., Ltd.
Tel
微信 17321281695 18019252918
Fax
17321281695
Email
sale@amkchem.com
Country
China
ProdList
15136
Advantage
55
Shanghai Yongye Biotechnology Co., Ltd.
Tel
86-021-61559134 15921386130
Fax
021-55068248
Email
3423497944@qq.com
Country
China
ProdList
8144
Advantage
55
Jiangsu Aikon Biopharmaceutical R&D co.,Ltd.
Tel
025-66028182 18626450290
Email
yftan@aikonchem.com
Country
China
ProdList
16679
Advantage
50
Bellen Chemistry Co., Ltd.
Tel
010-60400365-8001 15910885229
Fax
010-60400361
Email
service@bellenchem.com
Country
China
ProdList
4514
Advantage
60
ChengDu TongChuangYuan Pharmaceutical Co.Ltd
Tel
028-83379370 13880556291
Fax
028-87747383
Email
tcy@tcypharm.com
Country
China
ProdList
7218
Advantage
58
Amadis Chemical Company Limited
Tel
571-89925085
Fax
0086-571-89925065
Email
sales@amadischem.com
Country
China
ProdList
131957
Advantage
58
Nanijing m&m biotechnology Co. ,Ltd.
Tel
025-87782433 18021532344
Fax
025-87782433
Email
1345332203@qq.com
Country
China
ProdList
4135
Advantage
58
Sichuan BaiPeng Biotechnology Co., Ltd.
Tel
028-65791793 18140026355
Fax
QQ568470422
Email
568470422@qq.com
Country
China
ProdList
9997
Advantage
58
Wuhan FengyaoTonghui Chemical Products Co., Ltd.
Tel
027-87466105 15377573527
Email
2678564200@qq.com
Country
China
ProdList
17987
Advantage
58
3A Chemicals
Tel
400-668-9898
Fax
010-51582189
Email
service@3achem.com
Country
China
ProdList
20557
Advantage
58
Shanghai Jizhi Biochemical Technology Co. Ltd.
Tel
4009004166/18616739031 18616739031
Email
3007523370@qq.com
Country
China
ProdList
52687
Advantage
58
Cool Pharm, Ltd
Tel
021-58581007 18019463053
Fax
021-50966098
Email
sales@coolpharm.com
Country
China
ProdList
12878
Advantage
58
Guangdong wengjiang Chemical Reagent Co., Ltd.
Tel
0751-2815688 13927872512
Fax
0751-8963795
Email
3007421951@qq.com
Country
China
ProdList
9939
Advantage
58
Chengdu Forest Science and Technology Development Co,. Ltd
Tel
028-87925786 18010564218
Fax
028-61777050
Email
vendi@cdforestchem.com
Country
China
ProdList
1992
Advantage
58
ANHUI WITOP BIOTECH CO., LTD
Tel
+8615255079626
Email
eric@witopchemical.com
Country
China
ProdList
23541
Advantage
58
Nanjing Hengbei Chemicals Co., Ltd.
Tel
+86-25-58393656
Fax
+86-25-58393656
Email
sales@hengbeichem.cn
Country
China
ProdList
6854
Advantage
58
Labnetwork lnc.
Tel
+86-27-50766799 +8618062016861
Email
contact@labnetwork.com
Country
China
ProdList
19987
Advantage
58
sgtlifesciences pvt ltd
Tel
+8617013299288
Email
dj@sgtlifesciences.com
Country
China
ProdList
12373
Advantage
58
Dideu Industries Group Limited
Tel
+86-29-89586680 +86-15129568250
Email
1026@dideu.com
Country
China
ProdList
20284
Advantage
58
CD Chemical Group Limited
Tel
+8615986615575
Fax
0086-13651442114
Email
info@codchem.com
Country
China
ProdList
20342
Advantage
58
Dayang Chem (Hangzhou) Co.,Ltd.
Tel
+86-0571-88938639 +8617705817739
Fax
+86-571-88938652,+86-571- 88492614
Email
info@dycnchem.com
Country
China
ProdList
52846
Advantage
58
Hefei Hirisun Pharmatech Co., Ltd
Tel
+8615056975894
Fax
86-0551-62678551
Email
shawn@hirisunpharm.com
Country
CHINA
ProdList
9911
Advantage
58
Chemwill Asia Co.,Ltd.
Tel
86-21-51086038
Fax
86-21-51861608
Email
chemwill_asia@126.com
Country
CHINA
ProdList
23912
Advantage
58
Shanghai Hongshun Biological Technology Co., Ltd.
Tel
15901914505 15901914505;
Fax
021-54389085
Email
3187892335@qq.com
Country
China
ProdList
9889
Advantage
58
Hubei xin bonus chemical co. LTD
Tel
86-13657291602
Fax
027-59338440
Email
linda@hubeijusheng.com
Country
CHINA
ProdList
22963
Advantage
58
Accela ChemBio Co.,Ltd.
Tel
021-50795510 4000665055
Email
sales@accelachem.com
Country
China
ProdList
10467
Advantage
58
Qi Qi hang Biotechnology Co., Ltd.
Tel
18151111370
Email
1046215251@qq.com
Country
China
ProdList
5999
Advantage
58
Shanghai Kaiwei Chemical Technology Co., Ltd.
Tel
021-58461859 15821823057
Email
service@aiviche.com
Country
China
ProdList
49312
Advantage
58
career henan chemical co
Tel
+86-0371-86658258 +8613203830695
Fax
0086-371-86658258
Email
factory@coreychem.com
Country
China
ProdList
29798
Advantage
58
Shanghai Qianlai Pharmaceutical Technology Co., Ltd.
Tel
021-57216911 17740831186
Email
482109853@qq.com
Country
China
ProdList
462
Advantage
58
Zhengzhou Convergence Chemical Co. LTD
Tel
0371-0371-53736046 13393710386
Fax
QQ:2853979814
Email
2853979814@qq.com
Country
China
ProdList
9948
Advantage
58
LEWOO PHARMATECH (SHANGHAI) CO.,LTD
Tel
15800805830
Fax
021 67898603
Email
miao@lewoopharma.com.cn
Country
China
ProdList
932
Advantage
58
Shanghai UCHEM Inc.
Tel
18939844854
Fax
QQ3004479448
Email
sales6@myuchem.com
Country
China
ProdList
4997
Advantage
58
Huaian Jiamu Biotechnology Co., Ltd.
Tel
0517-83187139 18205232085
Email
cai@jiamu-bio.com
Country
China
ProdList
2996
Advantage
58
Beijing yanruicheng Pharmaceutical Technology Co., Ltd
Tel
18616022633
Email
1094628792@qq.com
Country
China
ProdList
340
Advantage
58
Shaanxi Dideu Medichem Co. Ltd
Tel
029-81124267 17392282731
Fax
029-88380327
Email
1073@dideu.com
Country
China
ProdList
9992
Advantage
58
Shanghai Haohong Pharmaceutical Co., Ltd.
Tel
400-8210725 4008210725
Email
malulu@leyan.com
Country
China
ProdList
40000
Advantage
58
Bide Pharmatech Ltd.
Tel
400-6005915
Email
sales@picasso-e.com
Country
China
ProdList
39665
Advantage
58
Shanghai Lingfu Pharmaceutical Research Co. LTD
Tel
+86(21)5895 0110 19945755304
Email
sales@chemany.com
Country
China
ProdList
9984
Advantage
58
Pushan Industry (Shaanxi) Co., Ltd.
Tel
029-81310890 13571859809
Email
info@pushanshiye.com
Country
China
ProdList
9955
Advantage
58
Zhengzhou Hong Sheng Pharmaceutical Technology Co. Ltd.
Tel
0371-55695890 15637198702
Email
1677336983@qq.com
Country
China
ProdList
13191
Advantage
58
Jiaxing Deyi Chemical Co., Ltd
Tel
0573-85866609 13588473046
Email
824930988@qq.com
Country
China
ProdList
7865
Advantage
58
Guangdong Fangxin Biotechnology Co., Ltd.
Tel
0751-2838688 13376594225
Email
1276075424@qq.com
Country
China
ProdList
9942
Advantage
58
More
Less

View Lastest Price from 4-AMINO-3,5-DIIODOPYRIDINE manufacturers

Dideu Industries Group Limited
Product
4-AMINO-3,5-DIIODOPYRIDINE 98136-86-8
Price
US $1.10/g
Min. Order
1g
Purity
99.00%
Supply Ability
100 Tons min
Release date
2021-09-01
Career Henan Chemical Co
Product
4-AMINO-3,5-DIIODOPYRIDINE 98136-86-8
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
100KG
Release date
2019-12-25