1-(4-METHOXY-1-NAPHTHYL)ETHANONE
- Product Name
- 1-(4-METHOXY-1-NAPHTHYL)ETHANONE
- CAS No.
- 24764-66-7
- Chemical Name
- 1-(4-METHOXY-1-NAPHTHYL)ETHANONE
- Synonyms
- 1-Acetyl-4-methoxynaphthalene;1-(4-METHOXY-1-PHTHYL)ETHANONE;1-(4-Methoxy-1-naphthyl)ethanone;4-Methoxy-1-Naphthyl Ethyl Ketone;1-(4-methoxynaphthalen-1-yl)ethanone;1-(4-Methoxy-1-naphthalenyl)-ethanone;Ethanone, 1-(4-methoxy-1-naphthalenyl)-
- CBNumber
- CB41490152
- Molecular Formula
- C13H12O2
- Formula Weight
- 200.23
- MOL File
- 24764-66-7.mol
1-(4-METHOXY-1-NAPHTHYL)ETHANONE Property
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- Off-white to light brown Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- M331373
- Product name
- 1-(4-Methoxy-1-naphthalenyl)-ethanone
- Packaging
- 100mg
- Price
- $90
- Updated
- 2021/12/16
- Product number
- J57174
- Product name
- 1-Acetyl-4-methoxynaphthalene
- Packaging
- 1g
- Price
- $29
- Updated
- 2021/12/16
- Product number
- 157090
- Product name
- 1-(4-Methoxy-1-naphthyl)ethanone
- Packaging
- 0.500g
- Price
- $160
- Updated
- 2021/12/16
- Product number
- 157090
- Product name
- 1-(4-Methoxy-1-naphthyl)ethanone
- Packaging
- 1g
- Price
- $200
- Updated
- 2021/12/16
- Product number
- 157090
- Product name
- 1-(4-Methoxy-1-naphthyl)ethanone
- Packaging
- 5g
- Price
- $700
- Updated
- 2021/12/16
1-(4-METHOXY-1-NAPHTHYL)ETHANONE Chemical Properties,Usage,Production
Synthesis Reference(s)
The Journal of Organic Chemistry, 36, p. 540, 1971 DOI: 10.1021/jo00803a011
Tetrahedron Letters, 31, p. 3933, 1990 DOI: 10.1016/S0040-4039(00)97510-5
Synthesis
75-36-5
2216-69-5
24764-66-7
Aluminum trichloride (800 mg, 6 mmol) in anhydrous dichloromethane (12 mL) was cooled to 0 °C under nitrogen protection and acetyl chloride (236 mg, 3 mmol) was slowly added. The reaction mixture was stirred at room temperature for 10 min before 1-methoxynaphthalene (474 mg, 3 mmol) was added and stirring was continued at room temperature overnight. After completion of the reaction, the reaction was quenched with water, the organic phase was separated, dried over anhydrous sodium sulfate and concentrated under reduced pressure. The residue was purified by silica gel column chromatography (eluent: ethyl acetate/petroleum ether=1:15, v/v) to afford 4-methoxynaphthaleneacetophenone (338 mg, 56% yield) as a white solid.1H NMR (300 MHz, CDCl3) δ: 9.01-9.96 (m, 1H), 8.32-8.35 (m, 1H), 8.03 (d, 1H), 7.63-7.65 (m, 1H), 7.53-7.58 (m, 1H), 6.79 (d, 1H), 4.07 (s, 3H), 2.72 (s, 3H).LC-MS: m/z 201 [M+1]+.
References
[1] Canadian Journal of Chemistry, 1981, vol. 59, p. 2629 - 2641
[2] Patent: US2012/220629, 2012, A1. Location in patent: Page/Page column 46
[3] Patent: WO2012/113103, 2012, A1. Location in patent: Page/Page column 62-63
[4] Recueil des Travaux Chimiques des Pays-Bas, 1945, vol. 64, p. 214,216
[5] Zhurnal Obshchei Khimii, 1938, vol. 8, p. 402,407
1-(4-METHOXY-1-NAPHTHYL)ETHANONE Preparation Products And Raw materials
Raw materials
Preparation Products
1-(4-METHOXY-1-NAPHTHYL)ETHANONE Suppliers
- Tel
- 0418-6530555 2855550
- Fax
- +86-418-6502885
- Country
- China
- ProdList
- 338
- Advantage
- 69
- Tel
- +86 (0) 571 85 58 67 18
- Fax
- 0086-571-85864795
- Country
- China
- ProdList
- 18207
- Advantage
- 66
- Tel
- 0573-85285100 18627885956
- Fax
- 0573-85285100
- isenchem@163.com
- Country
- China
- ProdList
- 9310
- Advantage
- 66
- Tel
- 400-6009262 16621234537
- Fax
- 021-64823266
- chenyj@titansci.com
- Country
- China
- ProdList
- 14101
- Advantage
- 59
- Tel
- 025-83697070
- Fax
- +86-25-83453306
- info@chemlin.com.cn
- Country
- China
- ProdList
- 15883
- Advantage
- 64
- Tel
- 025-58196018 800028039
- Fax
- 025-83453306
- sales@fartop.net
- Country
- China
- ProdList
- 2229
- Advantage
- 55
- Tel
- 18621020637 18621020637;
- sales@sunsynpharma.com
- Country
- China
- ProdList
- 288
- Advantage
- 55
- Tel
- 400-164-7117 13681763483
- Fax
- +86-21-61629029
- product02@bidepharm.com
- Country
- China
- ProdList
- 39966
- Advantage
- 60
- Tel
- 13120367189
- Fax
- 021-50315529
- mychess007@163.com
- Country
- China
- ProdList
- 1994
- Advantage
- 55
- Tel
- 15121041756
- xingui2022@126.com
- Country
- China
- ProdList
- 9979
- Advantage
- 58
View Lastest Price from 1-(4-METHOXY-1-NAPHTHYL)ETHANONE manufacturers
- Product
- 1-(4-METHOXY-1-NAPHTHYL)ETHANONE 24764-66-7
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 2000
- Release date
- 2025-04-18
- Product
- 1-(4-METHOXY-1-NAPHTHYL)ETHANONE 24764-66-7
- Price
- US $1.30/g
- Min. Order
- 1g
- Purity
- 98%
- Supply Ability
- 10kg
- Release date
- 2020-10-28