methyl 3-bromo-4-chlorobenzoate

Product Name: methyl 3-bromo-4-chlorobenzoate
CAS No.: 107947-17-1
Chemical Name: methyl 3-bromo-4-chlorobenzoate
Synonyms: methyl 3-bromo-4-chlorobenzoate;3-Bromo-4-chlorobenzoic acid methyl ester;Benzoic acid, 3-broMo-4-chloro-, Methyl ester
CBNumber: CB41561290
Molecular Formula: C8H6BrClO2
Formula Weight: 249.49
MOL File: 107947-17-1.mol

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methyl 3-bromo-4-chlorobenzoate Property

Boiling point:: 280℃
Density: 1.604
Flash point:: 123℃
storage temp.: Sealed in dry,Room Temperature
Appearance: Off-white to light brown Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: M295490
Product name: Methyl3-bromo-4-chlorobenzoate
Packaging: 1g
Price: $75
Updated: 2021/12/16

Oakwood

Product number: 236051
Product name: Methyl3-bromo-4-chlorobenzoate
Purity: 99%
Packaging: 5g
Price: $115
Updated: 2021/12/16

Matrix Scientific

Product number: 149516
Product name: Methyl 3-bromo-4-chlorobenzoate
Purity: 95%
Packaging: 5g
Price: $119
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB157423
Product name: 3-Bromo-4-chloro-benzoic acid methyl ester
Packaging: 1g
Price: $156.2
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB157423
Product name: 3-Bromo-4-chloro-benzoic acid methyl ester
Packaging: 2g
Price: $240
Updated: 2021/12/16

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methyl 3-bromo-4-chlorobenzoate Chemical Properties,Usage,Production

Synthesis

67-56-1

42860-10-6

107947-17-1

Example 13 13.1 Synthesis of methyl 3-bromo-4-chlorobenzoate (13.1). A round bottom flask was charged with 3-bromo-4-chlorobenzoic acid (5.0 g, 21.2 mmol, CAS No. 42860-10-6, available from Aldrich), methanol (60 mL), and a cooled sulfuric acid solution (1.4 mL). The reaction mixture was heated to 80 °C and the progress of the reaction was monitored by thin layer chromatography (TLC). After 17 hours of reaction, it was cooled to room temperature and diluted with water. The aqueous phase was extracted with ether (3 x 50 mL), the organic layers were combined and dried with anhydrous magnesium sulfate. After filtration, the organic solvent was removed by distillation under reduced pressure to give a white solid product 13.1 (5.0 g, 96% yield). The 1H NMR (400 MHz, CDCl3) data of the product were as follows: δ 8.28 (1H, d, J = 2.0 Hz), 7.93 (1H, m), 7.52 (1H, d, J = 8.2 Hz), 3.93 (3H, s).

References

[1] Patent: WO2008/130514, 2008, A1. Location in patent: Page/Page column 84-85
[2] Journal of Medicinal Chemistry, 2013, vol. 56, # 23, p. 9496 - 9508
[3] Patent: WO2013/25805, 2013, A1. Location in patent: Page/Page column 89
[4] Patent: WO2008/124610, 2008, A1. Location in patent: Page/Page column 85

methyl 3-bromo-4-chlorobenzoate Preparation Products And Raw materials

Raw materials

Preparation Products

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methyl 3-bromo-4-chlorobenzoate Suppliers

China 72 India 2 Switzerland 1 United Kingdom 2 United States 8 Global 85

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View Lastest Price from methyl 3-bromo-4-chlorobenzoate manufacturers

Career Henan Chemical Co

Product: methyl 3-bromo-4-chlorobenzoate 107947-17-1
Price: US $1.00/g
Min. Order: 1g
Purity: 99%
Supply Ability: 1000KGS
Release date: 2019-12-20

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methyl 3-bromo-4-chlorobenzoate

3-Bromo-4-chlorobenzoic acid methyl ester

Benzoic acid, 3-broMo-4-chloro-, Methyl ester

107947-17-1