4-Bromomethylbenzamide

Product Name: 4-Bromomethylbenzamide
CAS No.: 58914-40-2
Chemical Name: 4-Bromomethylbenzamide
Synonyms: DK831;4-Bromomethylbenzamide;Benzamide, 4-(bromomethyl)-
CBNumber: CB42471118
Molecular Formula: C8H8BrNO
Formula Weight: 214.06
MOL File: 58914-40-2.mol

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4-Bromomethylbenzamide Property

Melting point:: 179-181 °C(Solv: ethyl acetate (141-78-6); chloroform (67-66-3))
Boiling point:: 338.4±25.0 °C(Predicted)
Density: 1.555±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 15.88±0.50(Predicted)
form: liquid
Appearance: White to off-white Solid

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Safety

Hazard Codes: N
Risk Statements: 51/53
Safety Statements: 61
HS Code: 2924297099

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

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N-Bromosuccinimide Price

TRC

Product number: B870130
Product name: 4-(bromomethyl)benzamide
Packaging: 50mg
Price: $65
Updated: 2021/12/16

Oakwood

Product number: 214679
Product name: 4-(Bromomethyl)benzamide
Purity: 95+%
Packaging: 250mg
Price: $65
Updated: 2021/12/16

Matrix Scientific

Product number: 089816
Product name: 4-(Bromomethyl)benzamide
Purity: 95+%
Packaging: 1g
Price: $250
Updated: 2021/12/16

Oakwood

Product number: 214679
Product name: 4-(Bromomethyl)benzamide
Purity: 95+%
Packaging: 1g
Price: $125
Updated: 2021/12/16

Matrix Scientific

Product number: 089816
Product name: 4-(Bromomethyl)benzamide
Purity: 95+%
Packaging: 250mg
Price: $175
Updated: 2021/12/16

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4-Bromomethylbenzamide Chemical Properties,Usage,Production

Synthesis

7719-09-7

6232-88-8

58914-40-2

1. Suspend p-bromomethylbenzoic acid (8.00 g, 37.2 mmol) in carbon tetrachloride (80 mL) under nitrogen protection with stirring. Sulfoxide chloride (6.8 mL, 93 mmol) was added slowly. 2. The reaction mixture was heated to reflux for 95 hours. Upon completion of the reaction, the reaction mixture was concentrated by rotary evaporator under reduced pressure to remove solvent and unreacted sulfoxide chloride. 3. The concentrated residue was dissolved in dichloromethane (150 mL) and ammonia (NH3) was passed through for 10 minutes and a yellowish precipitate was observed to form. 4. 5% aqueous sodium bicarbonate solution (70 mL) was added to the reaction mixture with vigorous stirring and the precipitate was collected by filtration. 5. The precipitate was washed with deionized water and subsequently dried under reduced pressure at 60 °C to afford 4-(bromomethyl)benzamide as a colorless solid (7.35 g, 92% yield).

References

[1] Patent: US6750348, 2004, B1. Location in patent: Page column 110

4-Bromomethylbenzamide Preparation Products And Raw materials

Raw materials

Benzoyl peroxide Hexane N-Bromosuccinimide Toluene Carbon tetrachloride Benzene p-Toluic acid Pyridine Thionyl chloride

Preparation Products

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