3-Methoxy-5-nitrobenzotrifluoride
- Product Name
- 3-Methoxy-5-nitrobenzotrifluoride
- CAS No.
- 328-79-0
- Chemical Name
- 3-Methoxy-5-nitrobenzotrifluoride
- Synonyms
- TIMTEC-BB SBB010016;3-METHOXY-5-NITROBENZOTRIFLUORIDE;5-methoxy-3-nitrobenzotrifluoride;3-Nitro-5-(trifluoroMethyl)anisole;3-Methoxy-5-nitrobenzotrifluoride99%;3-Methoxy-5-nitrobenzotrifluoride 99%;1-Methoxy-3-nitro-5-(trifluoromethyl)benzene;Benzene, 1-methoxy-3-nitro-5-(trifluoromethyl)-
- CBNumber
- CB4270562
- Molecular Formula
- C8H6F3NO3
- Formula Weight
- 221.13
- MOL File
- 328-79-0.mol
3-Methoxy-5-nitrobenzotrifluoride Property
- Melting point:
- 36-38 °C (lit.)
- Boiling point:
- 246.9±40.0 °C(Predicted)
- Density
- 1.392±0.06 g/cm3(Predicted)
- Flash point:
- >230 °F
- storage temp.
- 2-8°C
- form
- solid
- color
- Low-mwlting
- CAS DataBase Reference
- 328-79-0(CAS DataBase Reference)
- NIST Chemistry Reference
- 3-Methoxy-5-nitrobenzotrifluoride(328-79-0)
Safety
- Hazard Codes
- C,Xi
- Risk Statements
- 34-36/38-21/22
- Safety Statements
- 26-27-28-36/37/39-45
- RIDADR
- UN 1759 8/PG 2
- WGK Germany
- 3
- Hazard Note
- Irritant
- HazardClass
- 8
- PackingGroup
- III
- HS Code
- 2909309090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H314Causes severe skin burns and eye damage
- Precautionary statements
-
P260Do not breathe dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P363Wash contaminated clothing before reuse.
N-Bromosuccinimide Price
- Product number
- 303674
- Product name
- 3-Methoxy-5-nitrobenzotrifluoride
- Purity
- 99%
- Packaging
- 5g
- Price
- $51.5
- Updated
- 2023/06/20
- Product number
- M327028
- Product name
- 3-Methoxy-5-nitrobenzotrifluoride
- Packaging
- 500mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- M327028
- Product name
- 3-Methoxy-5-nitrobenzotrifluoride
- Packaging
- 100mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- CHM0023699
- Product name
- 3-METHOXY-5-NITROBENZOTRIFLUORIDE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $597.87
- Updated
- 2021/12/16
- Product number
- CHM0023699
- Product name
- 3-METHOXY-5-NITROBENZOTRIFLUORIDE
- Purity
- 95.00%
- Packaging
- 5G
- Price
- $803.15
- Updated
- 2021/12/16
3-Methoxy-5-nitrobenzotrifluoride Chemical Properties,Usage,Production
Uses
3-Methoxy-5-nitrobenzotrifluoride may be used in chemical synthesis.
Synthesis
401-99-0
124-41-4
328-79-0
To a solution of 3,5-dinitrobenzotrifluoride (10 g, 42.4 mmol) in anhydrous methanol (100 mL) was slowly added a solution of sodium methanolate (3.43 g, 63.5 mmol) in anhydrous methanol (20 mL). The reaction mixture was heated to reflux for 1 hour and subsequently concentrated by rotary evaporation to remove the methanol solvent. The concentrated residue was diluted with ethyl acetate (80 mL) and water (30 mL) to separate the organic phase. The organic phase was dried over anhydrous sodium sulfate (Na2SO4), filtered and concentrated to give 3-nitro-5-(trifluoromethyl)anisole (8.5 g) as a red solid. The product was analyzed by LC-MS (ESI): no [M + H]+ peak was observed; retention time was 1.85 min.
References
[1] Journal of the Chemical Society, 1951, p. 2013,2016
[2] Journal of the American Chemical Society, 1955, vol. 77, p. 2284,2285
[3] Patent: WO2013/13503, 2013, A1. Location in patent: Page/Page column 43
3-Methoxy-5-nitrobenzotrifluoride Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-Methoxy-5-nitrobenzotrifluoride manufacturers
- Product
- 3-Methoxy-5-nitrobenzotrifluoride 328-79-0
- Price
- US $0.00-0.00/KG
- Min. Order
- 10mg
- Purity
- 99%HPLC
- Supply Ability
- 2000tons
- Release date
- 2020-01-10
- Product
- 3-Methoxy-5-nitrobenzotrifluoride 328-79-0
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 97.8%
- Supply Ability
- 100 tons
- Release date
- 2022-02-18
- Product
- 3-Methoxy-5-nitrobenzotrifluoride 328-79-0
- Price
- US $1.00/g
- Min. Order
- 1g
- Purity
- 99%
- Supply Ability
- 1000KGS
- Release date
- 2019-12-24