Acridine, 2,7-dibroMo-9,10-dihydro-9,9-diMethyl-
- Product Name
- Acridine, 2,7-dibroMo-9,10-dihydro-9,9-diMethyl-
- CAS No.
- 1333316-35-0
- Chemical Name
- Acridine, 2,7-dibroMo-9,10-dihydro-9,9-diMethyl-
- Synonyms
- 2,7-dibromo-9,9-dimethylacridan;2,7-Dibromo-9,9-dimethylacridine;2,7-dibromo-9,9-dimethyl-9,10-dihydroacridine;2,7-dibroMo-9,10-dihydro-9,9-diMethyl-Acridine;Acridine, 2,7-dibroMo-9,10-dihydro-9,9-diMethyl-
- CBNumber
- CB42728876
- Molecular Formula
- C15H13Br2N
- Formula Weight
- 367.08
- MOL File
- 1333316-35-0.mol
Acridine, 2,7-dibroMo-9,10-dihydro-9,9-diMethyl- Property
- Boiling point:
- 416.7±45.0 °C(Predicted)
- Density
- 1.576±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C(protect from light)
- solubility
- Chloroform; Dichloromethane; DMSO
- pka
- 0.46±0.40(Predicted)
- form
- Solid
- color
- Light Green
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- D426570
- Product name
- 2,7-Dibromo-9,10-dihydro-9,9-dimethylacridine
- Packaging
- 500mg
- Price
- $195
- Updated
- 2021/12/16
- Product number
- D426570
- Product name
- 2,7-Dibromo-9,10-dihydro-9,9-dimethylacridine
- Packaging
- 1g
- Price
- $330
- Updated
- 2021/12/16
- Product number
- D426570
- Product name
- 2,7-Dibromo-9,10-dihydro-9,9-dimethylacridine
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- 4472DT
- Product name
- 2,7-Dibromo-9,9-dimethyl-9,10-dihydroacridine
- Packaging
- 1g
- Price
- $186
- Updated
- 2021/12/16
- Product number
- 1333316350
- Product name
- 2,7-Dibromo-9,9-dimethyl-9,10-dihydroacridine
- Packaging
- 5g
- Price
- $765
- Updated
- 2021/12/16
Acridine, 2,7-dibroMo-9,10-dihydro-9,9-diMethyl- Chemical Properties,Usage,Production
Uses
2,7-Dibromo-9,10-dihydro-9,9-dimethylacridine is an intermediate in the synthesis of 2,7-Diisopropyl-9,9-dimethyl-4a,9,9a,10-tetrahydroacridine (D455760). 2,7-Diisopropyl-9,9-dimethyl-4a,9,9a,10-tetrahydroacridine is a useful chemical reagent. Also, it is derived from 9,9-Dimethyl-9,10-dihydroacridine (D474300), which are currently being used in the development of thermally activated delayed fluorescence (TADF) molecules which are being researched for their possible efficient deep-?blue TADF emitting potential.
Synthesis
6267-02-3
1333316-35-0
9,9-Dimethyl-9,10-dihydroacridine (2.7 g, 12.93 mmol) was dissolved in chloroform (200 ml) under the protection of nitrogen (by N2 purge) with continuous stirring. Subsequently, 3 equivalents of bromine were added slowly and dropwise. After 8 hours of reaction, the reaction was quenched by addition of aqueous sodium thiosulfate. The reaction mixture was then subjected to an extraction process. Purification by column chromatography using a solvent mixture of methylene chloride (MC) and hexane (1:5) as the unfolding agent resulted in 2,7-dibromo-9,9-dimethyl-9,10-dihydroacridine as a white solid (4.24 g, 90% yield).
References
[1] Patent: US2018/166636, 2018, A1. Location in patent: Paragraph 0115; 0116
[2] Patent: WO2014/165307, 2014, A2. Location in patent: Paragraph 0321
Acridine, 2,7-dibroMo-9,10-dihydro-9,9-diMethyl- Preparation Products And Raw materials
Raw materials
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View Lastest Price from Acridine, 2,7-dibroMo-9,10-dihydro-9,9-diMethyl- manufacturers
- Product
- 2,7-Dibromo-9,9-dimethyl-9,10-dihydroacridine 1333316-35-0
- Price
- US $0.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- Customise
- Release date
- 2025-09-16