ChemicalBook > CAS DataBase List > 5-AMINO-2-FLUOROBENZYL ALCOHOL

5-AMINO-2-FLUOROBENZYL ALCOHOL

Product Name
5-AMINO-2-FLUOROBENZYL ALCOHOL
CAS No.
84832-00-8
Chemical Name
5-AMINO-2-FLUOROBENZYL ALCOHOL
Synonyms
(5-Amino-2-fluorophenyl);5-AMINO-2-FLUOROBENZYL ALCOHOL;5-Amino-2-fluorobenzylalcohol99%;5-Amino-2-fluorobenzyl alcohol 99%;Benzenemethanol, 5-amino-2-fluoro-;(5-AMINO-2-FLUORO-PHENYL)-METHANOL;5-AMINO-2-FLUOROBENZYL ALCOHOL ISO 9001：2015 REACH;(5-Amino-2-fluorophenyl)methanol, 4-Fluoro-3-(hydroxymethyl)aniline
CBNumber
CB4341817
Molecular Formula
C7H8FNO
Formula Weight
141.14
MOL File
84832-00-8.mol
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5-AMINO-2-FLUOROBENZYL ALCOHOL Property

Melting point:
99-100°
Boiling point:
295.4±25.0 °C(Predicted)
Density 
1.286±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Inert atmosphere,Room temperature
pka
14.05±0.10(Predicted)
Appearance
Off-white to gray Solid
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Safety

Hazard Codes 
Xi
HazardClass 
IRRITANT
HS Code 
2906290090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
A630308
Product name
(5-Amino-2-fluorophenyl)methanol
Packaging
500mg
Price
$155
Updated
2021/12/16
ChemScene
Product number
CS-W021111
Product name
(5-Amino-2-fluorophenyl)methanol
Purity
>98.0%
Packaging
1g
Price
$50
Updated
2021/12/16
Apolloscientific
Product number
PC5127
Product name
5-Amino-2-fluorobenzylalcohol
Purity
99%
Packaging
1g
Price
$56
Updated
2021/12/16
Matrix Scientific
Product number
047420
Product name
(5-Amino-2-fluorophenyl)methanol
Purity
95+%
Packaging
1g
Price
$59
Updated
2021/12/16
SynQuest Laboratories
Product number
4656-3-Y0
Product name
5-Amino-2-fluorobenzyl alcohol
Purity
99%
Packaging
1g
Price
$61
Updated
2021/12/16
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5-AMINO-2-FLUOROBENZYL ALCOHOL Chemical Properties,Usage,Production

Synthesis Reference(s)

Journal of Medicinal Chemistry, 33, p. 327, 1990 DOI: 10.1021/jm00163a053

Synthesis

63878-73-9

84832-00-8

2-Fluoro-5-nitrobenzyl alcohol (2.00 g, 11.9 mmol) was used as starting material and mixed with iron powder (3.72 g, 66.8 mmol) and hydrochloric acid (265.84 mg, 7.28 mmol). The mixture was heated under reflux conditions for 2 hours. After completion of the reaction, it was filtered through diatomaceous earth while hot and cooled to room temperature. Subsequently, the aqueous phase was alkalized with saturated sodium bicarbonate solution and extracted with dichloromethane (CH2Cl2). The organic layer was separated, dried over anhydrous sodium sulfate (Na2SO4), filtered and concentrated by rotary evaporator to afford the brown solid crude product 5-amino-2-fluorobenzyl alcohol (1.51 g, 10.7 mmol, 90% yield). The product was identified by infrared spectroscopy (KBr), which showed that the absorption peaks were located at 3568, 3410, 2930, 1628, 1512, 1439, 1358, 1036, 874, 818, 737 cm-1 ; the 1H-NMR (CDCl3) spectrum showed the chemical shifts δ: 7.26 (broad single peak, 2H), 6.84 (triple peak, J = 9.2 Hz , 1H), 6.75-6.69 (multiple peaks, 1H), 6.61-6.50 (multiple peaks, 1H), 4.67 (single peak, 2H).

References

[1] Journal of Medicinal Chemistry, 2009, vol. 52, # 7, p. 1828 - 1844
[2] Chemical and Pharmaceutical Bulletin, 2016, vol. 64, # 6, p. 594 - 601
[3] Journal of Medicinal Chemistry, 1990, vol. 33, # 1, p. 327 - 336
[4] ACS Medicinal Chemistry Letters, 2014, vol. 5, # 5, p. 527 - 532
[5] Patent: WO2004/4720, 2004, A1. Location in patent: Page/Page column 76-77

5-AMINO-2-FLUOROBENZYL ALCOHOL Preparation Products And Raw materials

Raw materials

Preparation Products

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5-AMINO-2-FLUOROBENZYL ALCOHOL Suppliers

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