ChemicalBook > CAS DataBase List > 2-METHOXY-5-NITRO-6-PICOLINE

2-METHOXY-5-NITRO-6-PICOLINE

Product Name: 2-METHOXY-5-NITRO-6-PICOLINE
CAS No.: 5467-69-6
Chemical Name: 2-METHOXY-5-NITRO-6-PICOLINE
Synonyms: 6-Methoxy-2-methyL;2-Methoxy-5-nitropyridine;6-Methoxy-3-nitro-picoline;6-METHOXY-3-NITRO-2-ICOLINE;2-METHOXY-5-NITRO-6-PICOLINE;6-METHOXY-3-NITRO-2-PICOLINE;2-Methoxy-5-nitro-6-iodopyridine;2-Methoxy-6-methyl-5-nitropyridine;2-METHOXY-5-NITRO-6-METHYLPYRIDINE;6-Methoxy-3-nitro-2-methylpyridine
CBNumber: CB4695084
Molecular Formula: C7H8N2O3
Formula Weight: 168.15
MOL File: 5467-69-6.mol

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2-METHOXY-5-NITRO-6-PICOLINE Property

Melting point:: 104-108 ºC
Boiling point:: 261.1±35.0 °C(Predicted)
Density: 1.247±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
pka: 0.09±0.10(Predicted)
Appearance: White to light yellow Solid
CAS DataBase Reference: 5467-69-6(CAS DataBase Reference)

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 26-37/39
HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: E937543
Product name: 1-Ethyl-6-methyl-5-nitropyridin-2(1H)-one
Packaging: 100mg
Price: $60
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H54-1-CA
Product name: 6-Methoxy-2-methyl-3-nitropyridine
Packaging: 1g
Price: $144
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H54-1-CA
Product name: 6-Methoxy-2-methyl-3-nitropyridine
Packaging: 5G
Price: $264
Updated: 2021/12/16

Matrix Scientific

Product number: 118053
Product name: 6-Methoxy-2-methyl-3-nitropyridine
Packaging: 5g
Price: $550
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0027789
Product name: 2-METHOXY-5-NITRO-6-PICOLINE
Purity: 95.00%
Packaging: 1G
Price: $757
Updated: 2021/12/16

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2-METHOXY-5-NITRO-6-PICOLINE Chemical Properties,Usage,Production

Synthesis

63071-03-4

5467-69-6

2-Methoxy-6-methylpyridine (1.95 g, 15 mmol) was used as starting material and 60% nitric acid (7 mL) was added. The reaction mixture gradually changed to reddish brown color, accompanied by exothermic phenomenon and generation of nitrogen dioxide gas. Subsequently, concentrated sulfuric acid (7 mL) was added slowly. The reaction system was stirred at 80°C overnight. Upon completion of the reaction, the cooled reaction mixture was slowly poured into ice water (70 mL) and neutralized with calcium carbonate. The aqueous phase was extracted with ethyl acetate (3 x 50 mL), the organic phases were combined and dried over anhydrous sodium sulfate. The desiccant was removed by filtration and the organic phase was concentrated to dryness under reduced pressure to give 6-methoxy-2-methyl-3-nitropyridine (2.25 g, 86% yield) as a yellow solid. Nuclear magnetic resonance hydrogen spectroscopy (1H NMR, DMSO-d6) data were as follows: δ 8.3 (d, 1H), 6.8 (d, 1H), 4.0 (s, 3H), 2.7 (s, 3H).

References

[1] Patent: WO2004/62665, 2004, A1. Location in patent: Page/Page column 44-45

2-METHOXY-5-NITRO-6-PICOLINE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-METHOXY-5-NITRO-6-PICOLINE manufacturers

Dideu Industries Group Limited

Product: 2-METHOXY-5-NITRO-6-PICOLINE 5467-69-6
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons min
Release date: 2021-08-25

Career Henan Chemical Co

Product: 2-METHOXY-5-NITRO-6-PICOLINE 5467-69-6
Price: US $9.80/KG
Min. Order: 1g
Purity: ≥99%
Supply Ability: 100kg
Release date: 2020-01-03

5467-69-6, 2-METHOXY-5-NITRO-6-PICOLINERelated Search:

2-METHOXY-3-NITRO-6-PICOLINE 2-Methoxy-5-(trifluoromethyl)pyridine 4-CHLORO-2-METHOXY-PYRIDINE 2-Methoxy-4-methylpyridine 5-Chloro-2-methoxypyridine 5-Bromo-2-methoxypyridine 2-METHOXY-5-PICOLINE 2-Methoxy-5-nitropyridine 4-Amino-2-methoxypyridine 2-Methoxy-6-methylaminopyridine 2-Methoxy-5-methyl-N,N-bis(1-methylethyl)-3-phenylbenzenepropanamine fumarate 5-Bromo-2-methoxy-6-picoline 2-METHOXY-5-NITRO-6-PICOLINE 2-Methoxy-3-Nitro-5-Picoline 2-METHOXY-3-NITRO-4-PICOLINE 3-Methoxy-2-Nitro-6-Picoline 2-Methyl-3-nitropyridine 2-Picoline

6-Methoxy-3-nitro-2-methylpyridine

2-METHOXY-5-NITRO-6-METHYLPYRIDINE

2-METHOXY-5-NITRO-6-PICOLINE (2-METHOXY-6-METHYL-5-NITROPYRIDINE)

6-methoxy-2-methyl-3-nitropyridine

2-Methyl-3-nitro-6-methyoxypyridine

6-Metho×y-2-Methyl-3-nitropyridine

6-Methoxy-2-Methyl-3-nitro-pyridin

Pyridine,6-Methoxy-2-Methyl-3-nitro-

2-Methoxy-5-nitropyridine

2-Methoxy-6-methyl-5-nitropyridine

4-(5,10-diiodo-1,3-dihydrophenanthro[9,10-d]imidazol-2-ylidene)-1-cyclohexa-2,5-dienone

2-METHOXY-5-NITRO-6-PICOLINE

6-METHOXY-3-NITRO-2-PICOLINE

2-methyl-3-nitro-6-methoxypyridine

6-METHOXY-3-NITRO-2-ICOLINE

6-Methoxy-3-nitro-picoline

2-Methoxy-5-nitro-6-iodopyridine

6-Methoxy-2-methyL

2-METHOXY-5-NITRO-6-PICOLINE ISO 9001：2015 REACH

5467-69-6

5647-69-6

Pyridine

Pyridines

Boronic Acid