5-Chloro-2-methoxypyridine

Product Name: 5-Chloro-2-methoxypyridine
CAS No.: 13473-01-3
Chemical Name: 5-Chloro-2-methoxypyridine
Synonyms: 5-CHLORO-2-METHOXYPYRIDINE;2-METHOXY-5-CHLORO PYRIDINE;Pyridine, 5-chloro-2-methoxy-;5-Chloro-2-methoxypyridine 97%;5-Chloro-2-methoxypyridine >5-Chloro-2-methoxypyridine ISO 9001：2015 REACH
CBNumber: CB5456538
Molecular Formula: C6H6ClNO
Formula Weight: 143.57
MOL File: 13473-01-3.mol

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5-Chloro-2-methoxypyridine Property

Boiling point:: 181-182 °C (lit.)
Density: 1.193 g/mL at 25 °C (lit.)
refractive index: n20/D 1.5260(lit.)
Flash point:: 128 °F
storage temp.: Sealed in dry,Room Temperature
solubility: soluble in Methanol
form: powder to lump
pka: 1.12±0.10(Predicted)
Specific Gravity: 1.193
color: White to Almost white
CAS DataBase Reference: 13473-01-3(CAS DataBase Reference)

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Safety

Hazard Codes: Xn,Xi
Risk Statements: 10-22-41-36/37/38
Safety Statements: 26-39-37/39
RIDADR: UN 1993 3/PG 3
WGK Germany: 3
HazardClass: 3
PackingGroup: III
HS Code: 29333990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H226Flammable liquid and vapour

H302Harmful if swallowed

H315Causes skin irritation

H318Causes serious eye damage

H319Causes serious eye irritation

Precautionary statements

P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.

P233Keep container tightly closed.

P240Ground/bond container and receiving equipment.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P403+P235Store in a well-ventilated place. Keep cool.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 642967
Product name: 5-Chloro-2-methoxypyridine
Purity: 97%
Packaging: 1g
Price: $41
Updated: 2023/06/20

Sigma-Aldrich

Product number: 642967
Product name: 5-Chloro-2-methoxypyridine
Purity: 97%
Packaging: 10g
Price: $237
Updated: 2022/05/15

TCI Chemical

Product number: C2522
Product name: 5-Chloro-2-methoxypyridine
Purity: >98.0%(GC)
Packaging: 1g
Price: $34
Updated: 2025/07/31

TCI Chemical

Product number: C2522
Product name: 5-Chloro-2-methoxypyridine
Purity: >98.0%(GC)
Packaging: 5g
Price: $100
Updated: 2025/07/31

TRC

Product number: C597108
Product name: 5-Chloro-2-methoxypyridine
Packaging: 10mg
Price: $45
Updated: 2021/12/16

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5-Chloro-2-methoxypyridine Chemical Properties,Usage,Production

Chemical Properties

Colorless to light yellow liquid

Uses

Reactant for:

Preparation of biaryls via palladium-catalyzed Hiyama cross-coupling with aryltrifluorosilanes
Suzuki-Miyaura cross-coupling reactions

Synthesis

16110-09-1

67-56-1

13473-01-3

1. Sodium hydride (60% dispersed in mineral oil, 5.50 g, 115 mmol, 2 eq.) was added in batches to dry methanol (distilled after treatment with magnesium strips, 25 mL) under nitrogen protection. 2. 2,5-Dichloropyridine (10.0 g, 68 mmol) was added to the above solution. 3. The reaction mixture was refluxed for 18 hours. 4. After completion of the reaction, the reaction was cooled to room temperature and treated with an excess of solid potassium bicarbonate. 5. and treated with excess solid potassium bicarbonate.5. The reaction mixture was filtered and the filtrate was concentrated to 50% of the original volume, at which point solids precipitated out of the solution.6. The solids were washed with hexane, and the washings were combined and concentrated to give the oily material.7. 2-methoxy-5-chloropyridine was purified by distillation under reduced pressure (102 °C, 2400 Pascals) to give 6.30 g (65% yield) as a colorless oily material. colorless oil. Mass spectra (chemical ionization, CH4) m/z: 144 (M+, 100), 146 (44), 172 (M+28, 19), 124 (9).

References

[1] Journal of the Chemical Society, Perkin Transactions 1, 2000, # 8, p. 1245 - 1249
[2] Patent: US5512575, 1996, A

5-Chloro-2-methoxypyridine Preparation Products And Raw materials

Raw materials

Preparation Products

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5-Chloro-2-methoxypyridine Suppliers

Americas 1 Canada 1 China 176 Europe 2 France 3 Germany 5 India 9 Japan 2 Switzerland 1 United Kingdom 6 United States 34 Global 240

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View Lastest Price from 5-Chloro-2-methoxypyridine manufacturers

Shanghai Yongzeng Technology Co.,Ltd

Product: 5-Chloro-2-methoxypyridine 13473-01-3
Price: US $0.00/gm
Min. Order: 100gm
Purity: 99%min
Supply Ability: 100kgs
Release date: 2024-09-04

Henan Fengda Chemical Co., Ltd

Product: 5-Chloro-2-methoxypyridine 13473-01-3
Price: US $200.00-1.00/KG
Min. Order: 1KG
Purity: 99%, 99.5% Sublimated
Supply Ability: g-kg-tons, free sample is available
Release date: 2023-12-30

Dideu Industries Group Limited

Product: 5-Chloro-2-methoxypyridine 13473-01-3
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons Min
Release date: 2021-10-25

13473-01-3, 5-Chloro-2-methoxypyridineRelated Search:

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5-CHLORO-2-METHOXYPYRIDINE

2-METHOXY-5-CHLORO PYRIDINE

5-Chloro-2-methoxypyridine 97%

Pyridine, 5-chloro-2-methoxy-

5-Chloro-2-methoxypyridine &gt

5-Chloro-2-methoxypyridine ISO 9001：2015 REACH

13473-01-3

13474-01-3

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