ChemicalBook > CAS DataBase List > 4-Iodo-2-methylpyridine

4-Iodo-2-methylpyridine

Product Name
4-Iodo-2-methylpyridine
CAS No.
22282-65-1
Chemical Name
4-Iodo-2-methylpyridine
Synonyms
4-Iodo-2-methylpyridine;Pyridine, 4-iodo-2-methyl-;4-Iodo-2-methylpyridine ISO 9001:2015 REACH
CBNumber
CB4967480
Molecular Formula
C6H6IN
Formula Weight
219.02
MOL File
22282-65-1.mol
More
Less

4-Iodo-2-methylpyridine Property

storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
Appearance
White to yellow Solid
More
Less

Safety

HS Code 
2933399990
More
Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

More
Less

N-Bromosuccinimide Price

TRC
Product number
B448828
Product name
4-Iodo-2-methylpyridine
Packaging
100mg
Price
$60
Updated
2021/12/16
ChemScene
Product number
CS-W018720
Product name
4-Iodo-2-methylpyridine
Purity
97.68%
Packaging
1g
Price
$105
Updated
2021/12/16
Matrix Scientific
Product number
118958
Product name
4-Iodo-2-methylpyridine
Purity
95+%
Packaging
250mg
Price
$144
Updated
2021/12/16
SynQuest Laboratories
Product number
3H32-H-65
Product name
4-Iodo-2-methylpyridine
Purity
98%
Packaging
1g
Price
$148
Updated
2021/12/16
ChemScene
Product number
CS-W018720
Product name
4-Iodo-2-methylpyridine
Purity
97.68%
Packaging
5g
Price
$312
Updated
2021/12/16
More
Less

4-Iodo-2-methylpyridine Chemical Properties,Usage,Production

Synthesis

3678-63-5

22282-65-1

General procedure for the synthesis of 2-methyl-4-iodopyridine from 4-chloro-2-methylpyridine: 4-chloro-2-methylpyridine (10 g, 78 mmol), sodium iodide (17.8 g, 118 mmol), and hydriodic acid (57%, 26 mL, 196 mmol) were heated and reacted in a sealed tube for 7 days at 140 °C. Upon completion of the reaction, the reaction mixture was slowly poured into ice water and neutralized with sodium hydroxide solution. Subsequently, the mixture was extracted three times with dichloromethane (300 mL each time). The organic phases were combined, dried with magnesium sulfate, filtered and concentrated under reduced pressure. The resulting product was an off-white solid (14.7 g, 85% yield) and could be used in subsequent reactions without further purification.

References

[1] Patent: WO2004/80998, 2004, A1. Location in patent: Page 27
[2] Patent: US2002/40040, 2002, A1
[3] Chemical & Pharmaceutical Bulletin, 1982, vol. 30, # 5, p. 1731 - 1737

4-Iodo-2-methylpyridine Preparation Products And Raw materials

Raw materials

Preparation Products

More
Less

4-Iodo-2-methylpyridine Suppliers

Shanghai Synthfine Chemical Co.,Ltd
Tel
15921303235
Fax
QQ489466966
Email
sales@synthfine.com
Country
China
ProdList
1043
Advantage
58
Chiba Pharmaceutical Science and technology Co, Ltd.
Tel
0531-81313138 13066006660
Fax
QQ: 3366077777
Email
chibapharm@foxmail.com
Country
China
ProdList
3992
Advantage
55
SynAsst Chemical.
Tel
021-60343070
Fax
021-35122006
Country
China
ProdList
12740
Advantage
55
Bide Pharmatech Ltd.
Tel
400-164-7117 13681763483
Fax
+86-21-61629029
Email
product02@bidepharm.com
Country
China
ProdList
39966
Advantage
60
Synchem OHG
Tel
+49 5662 408730
Fax
+49 5662 4087320
Email
info@synchem.de
Country
Germany
ProdList
4705
Advantage
70
Shanghai HuanChuan Industry Co.,Ltd.
Tel
021-61478794
Fax
021-61478794
Email
sales@hcshhai.com
Country
China
ProdList
9793
Advantage
50
NovoChemy Ltd.
Tel
86-(0)21-31261262 373522135
Fax
86-(0)21-33250524
Email
sales@novochemy.com
Country
China
ProdList
6498
Advantage
58
Shanghai YuanYe Biotechnology Co., Ltd.
Tel
021-61312847; 18021002903
Fax
QQ:3008007432
Email
3008007409@qq.com
Country
China
ProdList
71826
Advantage
60
Amadis Chemical Company Limited
Tel
571-89925085
Fax
0086-571-89925065
Email
sales@amadischem.com
Country
China
ProdList
131957
Advantage
58
Dangyang bigfish Biotechnology Limited
Tel
18818274458
Email
177802831@qq.com
Country
China
ProdList
75
Advantage
58
More
Less

View Lastest Price from 4-Iodo-2-methylpyridine manufacturers

Dideu Industries Group Limited
Product
4-Iodo-2-methylpyridine 22282-65-1
Price
US $1.10/g
Min. Order
1g
Purity
99.00%
Supply Ability
100 Tons min
Release date
2021-09-01