ChemicalBook > CAS DataBase List > 6-BROMOBENZO[D]ISOXAZOL-3-YLAMINE

6-BROMOBENZO[D]ISOXAZOL-3-YLAMINE

Product Name: 6-BROMOBENZO[D]ISOXAZOL-3-YLAMINE
CAS No.: 177995-39-0
Chemical Name: 6-BROMOBENZO[D]ISOXAZOL-3-YLAMINE
Synonyms: 3-Amino-6-bromobenzisoxazole;6-broMo-1,2-benzoxazol-3-aMine;6-BROMOBENZO[D]ISOXAZOL-3-AMINE;6-Bromo-1,2-benzisoxazol-3-amine;3-AMino-6-broMobenzo[d]isoxazole;3-Amino-6-bromo-1,2-benzisoxazole;1,2-Benzisoxazol-3-amine,6-bromo-
CBNumber: CB51091675
Molecular Formula: C7H5BrN2O
Formula Weight: 213.03
MOL File: 177995-39-0.mol

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6-BROMOBENZO[D]ISOXAZOL-3-YLAMINE Property

Boiling point:: 371.1±22.0 °C(Predicted)
Density: 1.804±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 0.72±0.30(Predicted)
Appearance: Off-white to light brown Solid

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Safety

Hazard Codes: Xn
Risk Statements: 22
HS Code: 2934999090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

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N-Bromosuccinimide Price

TRC

Product number: B807853
Product name: 6-Bromobenzo[D]isoxazol-3-amine
Packaging: 100mg
Price: $60
Updated: 2021/12/16

ChemScene

Product number: CS-W005980
Product name: 6-Bromobenzo[d]isoxazol-3-amine
Packaging: 1g
Price: $64
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB53367
Product name: 6-Bromobenzo[d]isoxazol-3-ylamine
Packaging: 100mg
Price: $75
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB53367
Product name: 6-Bromobenzo[d]isoxazol-3-ylamine
Packaging: 250mg
Price: $97.5
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H56-9-L0
Product name: 6-Bromo-1,2-benzisoxazol-3-amine
Packaging: 1g
Price: $100
Updated: 2021/12/16

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6-BROMOBENZO[D]ISOXAZOL-3-YLAMINE Chemical Properties,Usage,Production

Uses

6-Bromobenzo[D]Isoxazol-3-Amine is a useful research reagent for organic synthesis.

Synthesis

546-88-3

105942-08-3

177995-39-0

Step A: 6-Bromobenzo[d]isoxazol-3-amine (1.13 g, 15.0 mmol) and N-hydroxyacetamide were dissolved in N,N-dimethylformamide (DMF, 20 mL). Potassium tert-butoxide (KOt-Bu, 1.68 g, 15.0 mmol) was added to the reaction system and stirred at room temperature for 30 min. Subsequently, 4-bromo-2-fluorobenzonitrile (2.0 g, 10.0 mmol) was added and the reaction was continued at room temperature for 2 hours. After completion of the reaction, the reaction mixture was diluted with ethyl acetate (50 mL) and water (50 mL). The aqueous layer was separated and extracted with ethyl acetate. The organic phases were combined, washed with water, dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure. The crude product was purified by fast column chromatography using ethyl acetate/hexane (1:4, v/v) and ethyl acetate/hexane (1:3, v/v) sequentially as eluent to afford the target compound 3-amino-6-bromobenzo[D]isoxazole (1.35 g, 63% yield). Mass spectra (APCI) m/z: 215.2, 217.1 ([M+H]+).

References

[1] Tetrahedron Letters, 1996, vol. 37, # 17, p. 2885 - 2886
[2] Patent: US2007/49603, 2007, A1. Location in patent: Page/Page column 61-62
[3] Patent: WO2010/51042, 2010, A1. Location in patent: Page/Page column 135
[4] Patent: WO2014/151147, 2014, A1. Location in patent: Paragraph 00502
[5] Patent: US2014/357651, 2014, A1. Location in patent: Paragraph 0485

6-BROMOBENZO[D]ISOXAZOL-3-YLAMINE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 6-BROMOBENZO[D]ISOXAZOL-3-YLAMINE manufacturers

Hebei Chuanghai Biotechnology Co,.LTD

Product: 6-BROMOBENZO[D]ISOXAZOL-3-YLAMINE 177995-39-0
Price: US $1.90/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 10 ton
Release date: 2024-08-20

Career Henan Chemical Co

Product: 6-BROMOBENZO[D]ISOXAZOL-3-YLAMINE 177995-39-0
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 1ton
Release date: 2018-08-06

177995-39-0, 6-BROMOBENZO[D]ISOXAZOL-3-YLAMINERelated Search:

3-AMINO-4-CYANOPYRIDINE 3-AMINO-6-BROMOPYRAZINE-2-CARBONITRILE 3-aMino-5-broMo-4-chloropyridine 3-Amino-6-trifluoromethyl-pyridin-2-ol 3-AMINO-6-IODOPYRAZINE-2-CARBOXYLIC ACID METHYL ESTER 3-amino-6-chloropyrazine-2-carboxylic acid 3-AMINO-4-METHOXYPYRIDINE 3-AMINO-3-(4-CYANOPHENYL)PROPANOIC ACID 3-Amino-5-chloropyridin-2-ol HCl (3-aminopyrazin-2-yl)methanol 3-Amino-3-(4-methoxyphenyl)propionic acid 3-PYRIDINAMINE, 6-(1-METHYLETHYL)- 3-AMINO-5-HYDROXYBENZOIC ACID 2-CHLORO-5-IODO-PYRIDIN-3-YLAMINE 2-CHLORO-5-(TRIFLUOROMETHYL)-3-PYRIDINAMINE 7-Bromobenzo[d]isoxazol-3-amine 3-Amino-1,2-benzisoxazole 6-BROMOBENZO[D]ISOXAZOL-3-YLAMINE

6-broMo-1,2-benzoxazol-3-aMine

3-AMino-6-broMobenzo[d]isoxazole

6-Bromo-1,2-benzisoxazol-3-amine

1,2-Benzisoxazol-3-amine,6-bromo-

6-BROMOBENZO[D]ISOXAZOL-3-AMINE

3-Amino-6-bromobenzisoxazole

3-Amino-6-bromo-1,2-benzisoxazole

177995-39-0