ChemicalBook > CAS DataBase List > 6-METHOXY-PYRIDINE-2-CARBOXYLICACIDMETHYLESTER

6-METHOXY-PYRIDINE-2-CARBOXYLICACIDMETHYLESTER

Uses

Product Name: 6-METHOXY-PYRIDINE-2-CARBOXYLICACIDMETHYLESTER
CAS No.: 26256-72-4
Chemical Name: 6-METHOXY-PYRIDINE-2-CARBOXYLICACIDMETHYLESTER
Synonyms: Methyl 6-methoxy;Methyl 6-methoxypicolinate;methyl 6-methoxy-2-pyridinecarboxylate;6-Methoxypyridinecarboxylic acid methyl ester;6-Methoxy-2-Pyridinecarboxylic Acid Methyl Ester;2-Pyridinecarboxylic acid, 6-Methoxy-, Methyl ester;Methyl 6-methoxypyridine-2-carboxylate
CBNumber: CB51229335
Molecular Formula: C8H9NO3
Formula Weight: 167.16
MOL File: 26256-72-4.mol

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6-METHOXY-PYRIDINE-2-CARBOXYLICACIDMETHYLESTER Property

Melting point:: 33-38℃
Boiling point:: 256.6±20.0 °C(Predicted)
Density: 1.156±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
form: solid
pka: 0.41±0.10(Predicted)
color: White
InChI: InChI=1S/C8H9NO3/c1-11-7-5-3-4-6(9-7)8(10)12-2/h3-5H,1-2H3
InChIKey: QCCJUEURAZMEGY-UHFFFAOYSA-N
SMILES: C1(C(OC)=O)=NC(OC)=CC=C1

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Safety

Hazard Codes: Xi
Risk Statements: 37/38-41
Safety Statements: 26-39
WGK Germany: 3
HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H315Causes skin irritation

H318Causes serious eye damage

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: M338445
Product name: Methyl6-Methoxypicolinate
Packaging: 10mg
Price: $45
Updated: 2021/12/16

AK Scientific

Product number: Z0452
Product name: Methyl 6-methoxypyridine-2-carboxylate
Packaging: 1g
Price: $53
Updated: 2021/12/16

AK Scientific

Product number: Z0452
Product name: Methyl 6-methoxypyridine-2-carboxylate
Packaging: 5g
Price: $147
Updated: 2021/12/16

Ambeed

Product number: A178187
Product name: Methyl6-methoxypicolinate
Purity: 98%
Packaging: 10g
Price: $197
Updated: 2021/12/16

Chemenu

Product number: CM171471
Product name: Methyl6-methoxypicolinate
Purity: 98%
Packaging: 10g
Price: $218
Updated: 2021/12/16

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6-METHOXY-PYRIDINE-2-CARBOXYLICACIDMETHYLESTER Chemical Properties,Usage,Production

Uses

Methyl 6-methoxy-2-pyridinecarboxylate is a useful research chemical.

Synthesis Reference(s)

Tetrahedron Letters, 15, p. 4339, 1974 DOI: 10.1016/S0040-4039(01)92158-6

Synthesis

19621-92-2

74-88-4

26256-72-4

General procedure for the synthesis of methyl 6-methoxypyridine-2-carboxylate from 6-hydroxypyridine-2-carboxylic acid and iodomethane: 6-hydroxypyridine-2-carboxylic acid (1 g, 7.19 mmol) and silver carbonate (2.2 g, 7.90 mmol) were placed in a round-bottomed flask, and chloroform (20 mL) was added to dissolve. Subsequently, iodomethane (1 mL, 15.81 mmol) was added slowly and dropwise. The reaction mixture was stirred at 60°C for 26 hours. After completion of the reaction, the mixture was filtered and extracted with chloroform. Next, the extract was vacuum filtered and vacuum distilled to remove the solvent. Finally, the residue was purified by column chromatography (eluent ratio of ethyl acetate: hexane = 1:5) to afford the target product methyl 6-methoxypyridine-2-carboxylate (1.25 g, 100% yield).

References

[1] Patent: WO2014/3483, 2014, A1. Location in patent: Page/Page column 34
[2] Organic and Biomolecular Chemistry, 2006, vol. 4, # 6, p. 1071 - 1084
[3] Organic Letters, 2009, vol. 11, # 23, p. 5562 - 5565
[4] Patent: WO2011/79076, 2011, A1. Location in patent: Page/Page column 93

6-METHOXY-PYRIDINE-2-CARBOXYLICACIDMETHYLESTER Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 6-METHOXY-PYRIDINE-2-CARBOXYLICACIDMETHYLESTER manufacturers

Zibo Hangyu Biotechnology Development Co., Ltd

Product: 6-METHOXY-PYRIDINE-2-CARBOXYLICACIDMETHYLESTER 26256-72-4
Price: US $100.00-600.00/g
Min. Order: 5g
Purity: 99%
Supply Ability: 50
Release date: 2024-07-11

Career Henan Chemical Co

Product: 6-METHOXY-PYRIDINE-2-CARBOXYLICACIDMETHYLESTER 26256-72-4
Price: US $5.50/KG
Min. Order: 1KG
Purity: 98%min
Supply Ability: 1kg-100kg
Release date: 2020-01-10

26256-72-4, 6-METHOXY-PYRIDINE-2-CARBOXYLICACIDMETHYLESTERRelated Search:

4-AMINO-6-METHOXYQUINOLINE 6-Methoxyisoquinolin-3-aMine 6-Methoxy-3- quinolinecarboxvlic acid 6-METHOXYISOINDOLIN-1-ONE (6-methoxypyridin-3-yl)methanol 6-Methoxy-1H-indole-3-carbaldehyde 6-METHOXY-QUINOLINE-2-CARBOXYLIC ACID 6-methoxyimidazo[1,2-a]pyridine-3-carbaldehyde 6-methoxypyridine-2-carbonitrile 6-FORMYL-2-PYRIDINE CARBOXYLIC ACID METHYL ESTER 6-methoxypyrazine-2-carboxylic acid 6-METHOXYPYRIDINE-2-CARBOXYLIC ACID 6-METHOXY-PYRIDINE-2-CARBOXYLICACIDMETHYLESTER 4-FORMYL-6-METHOXY-PYRIDINE-2-CARBOXYLIC ACID PROPYL ESTER RARECHEM AL BF 1374 6-METHOXY-5-METHYL-PYRIDINE-2-CARBOXYLIC ACID METHYL ESTER 5-BROMOMETHYL-6-METHOXY-PYRIDINE-2-CARBOXYLIC ACID METHYL ESTER RARECHEM AL BI 1374

Methyl 6-methoxypicolinate

2-Pyridinecarboxylic acid, 6-Methoxy-, Methyl ester

6-Methoxy-2-Pyridinecarboxylic Acid Methyl Ester

methyl 6-methoxy-2-pyridinecarboxylate

Methyl 6-methoxy

6-Methoxypyridinecarboxylic acid methyl ester

Methyl 6-<WBR>methoxypyridine-<WBR>2-<WBR>carboxylate

26256-72-4

Building Blocks

C8 to C9

Chemical Synthesis

Heterocyclic Building Blocks

Pyridines