2-Chloro-6-methoxyisonicotinic acid
- Product Name
- 2-Chloro-6-methoxyisonicotinic acid
- CAS No.
- 15855-06-8
- Chemical Name
- 2-Chloro-6-methoxyisonicotinic acid
- Synonyms
- BUTTPARK 43\57-34;TIMTEC-BB SBB005427;2-Chloro-6-methoxypyridine-4-c;2-Chloro-6-methoxyisonicotinicaci;2-CHLORO-6-METHOXYISONICOTINIC ACID;2-Chloro-6-methoxy-4-pyridinecarboxylic acid;2-CHLORO-6-METHOXYPYRIDINE-4-CARBOXYLIC ACID;4-Pyridinecarboxylic acid, 2-chloro-6-methoxy-;2-Chloro-6-methoxyisonicotinic acid ISO 9001：2015 REACH;2-Chloro-6-methoxypyridine-4-carboxylic acid, 4-Carboxy-2-chloro-6-methoxypyridine
- CBNumber
- CB5255740
- Molecular Formula
- C7H6ClNO3
- Formula Weight
- 187.58
- MOL File
- 15855-06-8.mol
2-Chloro-6-methoxyisonicotinic acid Property
- Melting point:
- 214 °C
- Boiling point:
- 209-213℃
- Density
- 1.430±0.06 g/cm3(Predicted)
- storage temp.
- Store at room temperature
- form
- powder
- pka
- 2.88±0.10(Predicted)
- color
- White
- InChIKey
- PJQBTHQTVJMCFX-UHFFFAOYSA-N
- CAS DataBase Reference
- 15855-06-8(CAS DataBase Reference)
Safety
- Hazard Codes
- Xi
- Risk Statements
- 36/37/38
- Safety Statements
- 26-36/37/39-37/39-36/37
- WGK Germany
- 3
- HazardClass
- IRRITANT
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 700614
- Product name
- 2-Chloro-6-methoxypyridine-4-carboxylic acid
- Packaging
- 1g
- Price
- $107
- Updated
- 2023/01/07
- Product number
- C596680
- Product name
- 2-Chloro-6-methoxyisonicotinicAcid
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- C596680
- Product name
- 2-Chloro-6-methoxyisonicotinicAcid
- Packaging
- 500mg
- Price
- $90
- Updated
- 2021/12/16
- Product number
- OR27363
- Product name
- 2-Chloro-6-methoxyisonicotinicacid
- Packaging
- 5g
- Price
- $124
- Updated
- 2021/12/16
- Product number
- 4H21-5-Y1
- Product name
- 2-Chloro-6-methoxyisonicotinic acid
- Packaging
- 5G
- Price
- $136
- Updated
- 2021/12/16
2-Chloro-6-methoxyisonicotinic acid Chemical Properties,Usage,Production
Synthesis
67-56-1
5398-44-7
15855-06-8
a) 2,6-Dichloroisonicotinic acid (200 g, 1.04 mol) was dissolved in methanol (3 L) and 32% aqueous sodium hydroxide solution (770 mL) was added. The stirred mixture was heated to 34°C, then warmed to 70°C and kept at this temperature for 4 hours of reaction. After the reaction was completed, it was cooled to room temperature. The reaction mixture was neutralized with 32% aqueous hydrochloric acid solution (100 mL) and 25% aqueous hydrochloric acid solution (700 mL). The mixture was stirred at room temperature overnight. The white precipitate formed was collected by filtration, washed with methanol and dried. The filtrate was evaporated and the residue was suspended in water (200 mL). The resulting mixture was heated to 60 °C and the solid product was collected, washed with water and dried. All products were combined to give 2-chloro-6-methoxyisonicotinic acid (183 g) as a white solid; LC-MS: t R = 0.80 min, [M + 1] + = 187.93.
References
[1] Tetrahedron, 2002, vol. 58, # 34, p. 6951 - 6963
[2] Organic Letters, 2000, vol. 2, # 22, p. 3421 - 3423
[3] Patent: WO2011/7324, 2011, A1. Location in patent: Page/Page column 20
[4] Patent: US2012/108638, 2012, A1. Location in patent: Page/Page column 8
[5] Patent: US2013/303514, 2013, A1. Location in patent: Paragraph 0192
2-Chloro-6-methoxyisonicotinic acid Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-Chloro-6-methoxyisonicotinic acid manufacturers
- Product
- 2-Chloro-6-methoxyisonicotinic acid 15855-06-8
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons Min
- Release date
- 2021-10-28
- Product
- 2-Chloro-6-methoxyisonicotinic acid 15855-06-8
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100KG
- Release date
- 2019-12-31