ChemicalBook > CAS DataBase List > 2-Chloro-6-methoxyisonicotinic acid

2-Chloro-6-methoxyisonicotinic acid

Product Name
2-Chloro-6-methoxyisonicotinic acid
CAS No.
15855-06-8
Chemical Name
2-Chloro-6-methoxyisonicotinic acid
Synonyms
BUTTPARK 43\57-34;TIMTEC-BB SBB005427;2-Chloro-6-methoxypyridine-4-c;2-Chloro-6-methoxyisonicotinicaci;2-CHLORO-6-METHOXYISONICOTINIC ACID;2-Chloro-6-methoxy-4-pyridinecarboxylic acid;2-CHLORO-6-METHOXYPYRIDINE-4-CARBOXYLIC ACID;4-Pyridinecarboxylic acid, 2-chloro-6-methoxy-;2-Chloro-6-methoxyisonicotinic acid ISO 9001：2015 REACH;2-Chloro-6-methoxypyridine-4-carboxylic acid, 4-Carboxy-2-chloro-6-methoxypyridine
CBNumber
CB5255740
Molecular Formula
C7H6ClNO3
Formula Weight
187.58
MOL File
15855-06-8.mol
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2-Chloro-6-methoxyisonicotinic acid Property

Melting point:
214 °C
Boiling point:
209-213℃
Density 
1.430±0.06 g/cm3(Predicted)
storage temp. 
Store at room temperature
form 
powder
pka
2.88±0.10(Predicted)
color 
White
InChIKey
PJQBTHQTVJMCFX-UHFFFAOYSA-N
CAS DataBase Reference
15855-06-8(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-36/37/39-37/39-36/37
WGK Germany 
3
HazardClass 
IRRITANT
HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
700614
Product name
2-Chloro-6-methoxypyridine-4-carboxylic acid
Packaging
1g
Price
$107
Updated
2023/01/07
TRC
Product number
C596680
Product name
2-Chloro-6-methoxyisonicotinicAcid
Packaging
50mg
Price
$45
Updated
2021/12/16
TRC
Product number
C596680
Product name
2-Chloro-6-methoxyisonicotinicAcid
Packaging
500mg
Price
$90
Updated
2021/12/16
AK Scientific
Product number
A972
Product name
2-Chloro-6-methoxyisonicotinicacid
Packaging
250mg
Price
$26
Updated
2021/12/16
Apolloscientific
Product number
OR27363
Product name
2-Chloro-6-methoxyisonicotinicacid
Packaging
1g
Price
$37
Updated
2021/12/16
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2-Chloro-6-methoxyisonicotinic acid Chemical Properties,Usage,Production

Synthesis

67-56-1

5398-44-7

15855-06-8

a) 2,6-Dichloroisonicotinic acid (200 g, 1.04 mol) was dissolved in methanol (3 L) and 32% aqueous sodium hydroxide solution (770 mL) was added. The stirred mixture was heated to 34°C, then warmed to 70°C and kept at this temperature for 4 hours of reaction. After the reaction was completed, it was cooled to room temperature. The reaction mixture was neutralized with 32% aqueous hydrochloric acid solution (100 mL) and 25% aqueous hydrochloric acid solution (700 mL). The mixture was stirred at room temperature overnight. The white precipitate formed was collected by filtration, washed with methanol and dried. The filtrate was evaporated and the residue was suspended in water (200 mL). The resulting mixture was heated to 60 °C and the solid product was collected, washed with water and dried. All products were combined to give 2-chloro-6-methoxyisonicotinic acid (183 g) as a white solid; LC-MS: t R = 0.80 min, [M + 1] + = 187.93.

References

[1] Tetrahedron, 2002, vol. 58, # 34, p. 6951 - 6963
[2] Organic Letters, 2000, vol. 2, # 22, p. 3421 - 3423
[3] Patent: WO2011/7324, 2011, A1. Location in patent: Page/Page column 20
[4] Patent: US2012/108638, 2012, A1. Location in patent: Page/Page column 8
[5] Patent: US2013/303514, 2013, A1. Location in patent: Paragraph 0192

2-Chloro-6-methoxyisonicotinic acid Preparation Products And Raw materials

Raw materials

Preparation Products

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2-Chloro-6-methoxyisonicotinic acid Suppliers

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View Lastest Price from 2-Chloro-6-methoxyisonicotinic acid manufacturers

Dideu Industries Group Limited
Product
2-Chloro-6-methoxyisonicotinic acid 15855-06-8
Price
US $1.10/g
Min. Order
1g
Purity
99.00%
Supply Ability
100 Tons Min
Release date
2021-10-28
Career Henan Chemical Co
Product
2-Chloro-6-methoxyisonicotinic acid 15855-06-8
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
100KG
Release date
2019-12-31

15855-06-8, 2-Chloro-6-methoxyisonicotinic acidRelated Search:

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  • 2-Chloro-6-methoxypyridine-4-carboxylic acid, 4-Carboxy-2-chloro-6-methoxypyridine
  • 2-Chloro-6-methoxy-4-pyridinecarboxylic acid
  • 2-Chloro-6-methoxypyridine-4-c
  • TIMTEC-BB SBB005427
  • 2-CHLORO-6-METHOXYISONICOTINIC ACID
  • 2-CHLORO-6-METHOXYPYRIDINE-4-CARBOXYLIC ACID
  • BUTTPARK 43\57-34
  • 4-Pyridinecarboxylic acid, 2-chloro-6-methoxy-
  • 2-Chloro-6-methoxyisonicotinicaci
  • 2-Chloro-6-methoxyisonicotinic acid ISO 9001：2015 REACH
  • 15855-06-8
  • Carboxylic Acids
  • Pyridines
  • Carboxylic Acids