1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE

Product Name: 1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE
CAS No.: 439811-37-7
Chemical Name: 1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE
Synonyms: 1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE;tert-butyl 4-(4-broMobenzoyl)piperidine-1-carboxylate;tert-butyl 4-[(4-broMophenyl)carbonyl]piperidine-1-carboxylate;4-(4-bromobenzoyl)piperidine-1-carboxylic acid tert-butyl ester;1-Piperidinecarboxylic acid, 4-(4-bromobenzoyl)-, 1,1-dimethylethyl ester
CBNumber: CB5413232
Molecular Formula: C17H22BrNO3
Formula Weight: 368.27
MOL File: 439811-37-7.mol

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1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE Property

Boiling point:: 452.3±40.0 °C(Predicted)
Density: 1.325±0.06 g/cm3(Predicted)
storage temp.: 2-8°C
pka: -2.47±0.40(Predicted)
Appearance: Off-white to light yellow Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P403+P233Store in a well-ventilated place. Keep container tightly closed.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: B200940
Product name: 1-Boc-4-(4-bromo-benzoyl)-piperidine
Packaging: 100mg
Price: $100
Updated: 2021/12/16

TRC

Product number: B200940
Product name: 1-Boc-4-(4-bromo-benzoyl)-piperidine
Packaging: 250mg
Price: $200
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB51872
Product name: 1-Boc-4-(4-bromo-benzoyl)piperidine
Packaging: 500mg
Price: $220
Updated: 2021/12/16

Matrix Scientific

Product number: 074243
Product name: 1-Boc-4-(4-Bromobenzoyl)piperidine
Purity: 95+%
Packaging: 250mg
Price: $231
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB51872
Product name: 1-Boc-4-(4-bromo-benzoyl)piperidine
Packaging: 100mg
Price: $111
Updated: 2021/12/16

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1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE Chemical Properties,Usage,Production

Synthesis

746550-66-3

24424-99-5

439811-37-7

Step 1. Synthesis of tert-butyl 4-(4-bromobenzoyl)-piperidine-1-carboxylate. To a 250 mL round bottom flask was added 4-(4-bromobenzoyl)piperidine (5 g, 20 mmol), tetrahydrofuran (30 mL), water (30 mL), sodium carbonate (10 g, 90 mmol) and di-tert-butyl dicarbonate (4.35 g, 20.0 mmol). The reaction mixture was stirred at room temperature for 2 h and then partitioned with ethyl acetate and water. The aqueous layer was extracted twice with ethyl acetate, the organic phases were combined, washed with brine, dried, filtered and concentrated to give 7.1 g (100% yield) of tert-butyl 4-(4-bromobenzoyl)-piperidine-1-carboxylate.

References

[1] Patent: WO2016/205590, 2016, A1. Location in patent: Paragraph 00596
[2] Patent: WO2013/147711, 2013, A1. Location in patent: Page/Page column 231
[3] Patent: US2014/371199, 2014, A1. Location in patent: Paragraph 0801
[4] Patent: US2005/54628, 2005, A1. Location in patent: Page/Page column 23-24
[5] Patent: US2005/49269, 2005, A1. Location in patent: Page/Page column 12; 21

1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE Suppliers

China 53 Germany 1 India 1 United Kingdom 1 United States 12 Global 68

Pure Chemistry Scientific Inc.

Tel: 001-857-928-2050 or 1-888-588-9418
Fax: 001-617-206-9595
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Accela ChemBio Inc.

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Fax: +1(858) 876-1948
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Accela ChemBio Inc.

Tel: +1-858-6993322
Fax: (+1)-858-876-1948
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Alchem Pharmtech,Inc.

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3B Scientific Corporation

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J & W PharmLab, LLC

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View Lastest Price from 1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE manufacturers

Career Henan Chemical Co

Product: 1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE 439811-37-7
Price: US $9.80/KG
Min. Order: 1g
Purity: ≥99%
Supply Ability: 100kg
Release date: 2020-01-08

Career Henan Chemical Co

Product: 1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE 439811-37-7
Price: US $1.00/KG
Min. Order: 1KG
Purity: 95-99%
Supply Ability: 1ton
Release date: 2020-01-08

439811-37-7, 1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINERelated Search:

1-BOC-4-HYDROXY-4-(HYDROXYMETHYL)-PIPERIDINE 1-Benzhydrylazetane-3-carbonitrile 1-BOC-2-PHENYL-PIPERIDIN-4-ONE (4-OXO-4-PHENYL-BUTYL)-CARBAMIC ACID TERT-BUTYL ESTER (4-bromophenyl)(piperidin-4-yl)methanone 1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE 4-Acetyl-piperidine-1-carboxylic acid tert-butyl ester

1-BOC-4-(4-BROMO-BENZOYL)-PIPERIDINE

tert-butyl 4-(4-broMobenzoyl)piperidine-1-carboxylate

tert-butyl 4-[(4-broMophenyl)carbonyl]piperidine-1-carboxylate

1-Piperidinecarboxylic acid, 4-(4-bromobenzoyl)-, 1,1-dimethylethyl ester

4-(4-bromobenzoyl)piperidine-1-carboxylic acid tert-butyl ester

439811-37-7