5-Fluoro-2-iodopyridine
- Product Name
- 5-Fluoro-2-iodopyridine
- CAS No.
- 159870-80-1
- Chemical Name
- 5-Fluoro-2-iodopyridine
- Synonyms
- 2-Iodo-5-Fluoropyridine;5-FLUORO-2-IODOPYRIDINE;Pyridine, 5-fluoro-2-iodo-;5-Fluoro-2-iodopyridine 97%;5-FLUORO-2-IODOPYRIDINE ISO 9001：2015 REACH
- CBNumber
- CB5451508
- Molecular Formula
- C5H3FIN
- Formula Weight
- 222.99
- MOL File
- 159870-80-1.mol
5-Fluoro-2-iodopyridine Property
- Boiling point:
- 197℃
- Density
- 2.046
- Flash point:
- 73℃
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- pka
- -0.58±0.10(Predicted)
- color
- yellow to off-white solid
Safety
- HS Code
- 2933399990
N-Bromosuccinimide Price
- Product number
- F598843
- Product name
- 5-Fluoro-2-iodopyridine
- Packaging
- 250mg
- Price
- $85
- Updated
- 2021/12/16
- Product number
- 3H32-K-33
- Product name
- 5-Fluoro-2-iodopyridine
- Packaging
- 250mg
- Price
- $96
- Updated
- 2021/12/16
- Product number
- 3H32-K-33
- Product name
- 5-Fluoro-2-iodopyridine
- Packaging
- 1g
- Price
- $237
- Updated
- 2021/12/16
- Product number
- 076243
- Product name
- 5-Fluoro-2-iodopyridine
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $297
- Updated
- 2021/12/16
- Product number
- PC445023
- Product name
- 5-Fluoro-2-iodopyridine
- Purity
- 97%
- Packaging
- 1g
- Price
- $148
- Updated
- 2021/12/16
5-Fluoro-2-iodopyridine Chemical Properties,Usage,Production
Synthesis
41404-58-4
159870-80-1
General procedure for the synthesis of 5-fluoro-2-iodopyridine from 2-bromo-5-fluoropyridine: under nitrogen protection, Cu2O (7.2 mg, 10 mol%), L-proline (11.5 mg, 20 mol%), 2-bromo-5-fluoropyridine (0.50 mmol), potassium iodide (KI, 249 mg, 0.75 mmol) and ethanol (EtOH, 1.5 mL). After sealing the Schlenk tube with a PTFE valve, the reaction mixture was stirred at 110 °C. The reaction process was monitored by gas chromatography (GC) analysis. Upon completion of the reaction, the yield was determined by GC using an appropriate internal standard (e.g., chlorobenzene or 1-chloro-4-methylbenzene) for highly volatile products; or the solvent was removed by distillation under reduced pressure. The resulting crude product was purified by silica gel column chromatography (eluent ratio of petroleum ether/ethyl acetate = 10/1) to give the target product 5-fluoro-2-iodopyridine.
References
[1] Catalysis Today, 2016, vol. 274, p. 129 - 132
5-Fluoro-2-iodopyridine Preparation Products And Raw materials
Raw materials
Preparation Products
5-Fluoro-2-iodopyridine Suppliers
- Tel
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- Fax
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- sales@apolloscientific.co.uk
- Country
- United Kingdom
- ProdList
- 6084
- Advantage
- 88
- Tel
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- Fax
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- Country
- United Kingdom
- ProdList
- 6309
- Advantage
- 46
View Lastest Price from 5-Fluoro-2-iodopyridine manufacturers
- Product
- 5-Fluoro-2-iodopyridine 159870-80-1
- Price
- US $0.00/kg
- Min. Order
- 25kg
- Purity
- 98%
- Supply Ability
- Inquiry
- Release date
- 2023-07-12
- Product
- 5-Fluoro-2-iodopyridine 159870-80-1
- Price
- US $0.00-0.00/G
- Min. Order
- 0.0001G
- Purity
- 98%min
- Supply Ability
- 50kgs/month
- Release date
- 2022-08-18
- Product
- 5-FLUORO-2-IODOPYRIDINE 159870-80-1
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons min
- Release date
- 2021-09-01