Isopropyl 2-(3-nitrobenzylidene)acetoacetate
- Product Name
- Isopropyl 2-(3-nitrobenzylidene)acetoacetate
- CAS No.
- 39562-25-9
- Chemical Name
- Isopropyl 2-(3-nitrobenzylidene)acetoacetate
- Synonyms
- Nilvadipine Impurity L;Azelnidipine Impurity 5;2-(3-nitrobenzylidene)acetoacetate;Isopropyl 2-(3-nitrobenzylidene)acetoacetate;Isopropyl-2-(3-Nitrobenzolidene)Acetoacetate;isopropyl 2-(3-nitrobenzylidene) acetacetate;Isopropyl 2-3- nitrobcnzylidcnelacetoucctatc;ISOPROPYL 2-(M-NITROBENZYLIDENE)-ACETOACETATE;Isopropyl 2-(3- Nitrobenzylidine)Acetoacetate;Isopropyl 2-(3-nitrobenzylidene)-3-oxobutanoate
- CBNumber
- CB5683877
- Molecular Formula
- C14H15NO5
- Formula Weight
- 277.27
- MOL File
- 39562-25-9.mol
Isopropyl 2-(3-nitrobenzylidene)acetoacetate Property
- Melting point:
- 94 °C
- Boiling point:
- 404.9±35.0 °C(Predicted)
- Density
- 1.229±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- I872775
- Product name
- Isopropyl2-(3-nitrobenzylidene)acetoacetate
- Packaging
- 100mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- I872775
- Product name
- Isopropyl2-(3-nitrobenzylidene)acetoacetate
- Packaging
- 500mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- J50802
- Product name
- Isopropyl2-(3-nitrobenzylidene)-3-oxobutanoate
- Packaging
- 5g
- Price
- $160
- Updated
- 2021/12/16
- Product number
- CHM0078655
- Product name
- ISOPROPYL 2-(3-NITROBENZYLIDENE)ACETOACETATE
- Purity
- 95.00%
- Packaging
- 5G
- Price
- $909.56
- Updated
- 2021/12/16
- Product number
- CD12075576
- Product name
- Isopropyl2-(3-nitrobenzylidene)-3-oxobutanoate
- Purity
- 97%
- Packaging
- 100g
- Price
- $481
- Updated
- 2021/12/16
Isopropyl 2-(3-nitrobenzylidene)acetoacetate Chemical Properties,Usage,Production
Synthesis
A preparation method of isopropyl 2-(3-nitrobenzylidene)acetoacetate comprises the following steps: carrying out condensation reaction on 3-nitrobenzaldehyde and isopropyl acetoacetate as initial raw materials by using an organic solvent as a solvent in the presence of catalysts acetic acid and piperidine for 2-8 hours; after carrying out vacuum concentration on the filtrate at 80 ℃ to 2/3-3/4 by volume, cooling to -5-5 ℃ while stirring to crystallize overnight; and filtering, and recrystallizing with isopropanol to finally obtain the isopropyl 2-(3-nitrobenzylidene)acetoacetate.
Isopropyl 2-(3-nitrobenzylidene)acetoacetate Preparation Products And Raw materials
Raw materials
Preparation Products
Isopropyl 2-(3-nitrobenzylidene)acetoacetate Suppliers
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View Lastest Price from Isopropyl 2-(3-nitrobenzylidene)acetoacetate manufacturers
- Product
- Isopropyl 2-(3-nitrobenzylidene)acetoacetate 39562-25-9
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 1Ton
- Release date
- 2022-10-10
- Product
- Isopropyl 2-(3-nitrobenzylidene)acetoacetate 39562-25-9
- Price
- US $120.00/Kg/Bag
- Min. Order
- 25Kg/Bag
- Purity
- 99%
- Supply Ability
- 20 Tons
- Release date
- 2020-11-16
- Product
- Isopropyl 2-(3-nitrobenzylidene)acetoacetate 39562-25-9
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100kg
- Release date
- 2019-07-11