(3-AMINO-PYRIDIN-4-YL)-METHANOL
- Product Name
- (3-AMINO-PYRIDIN-4-YL)-METHANOL
- CAS No.
- 152398-05-5
- Chemical Name
- (3-AMINO-PYRIDIN-4-YL)-METHANOL
- Synonyms
- 3-Aminopyridine-4-methanol;(3-Amino-4-pyridyl)methanol;4-Pyridinemethanol, 3-amino-;(3-amino-4-pyridinyl)methanol;3-AMINO-4-HYDROXYMETHYLPYRIDINE;(3-AMINO-PYRIDIN-4-YL)-METHANOL;4-Pyridinemethanol,3-amino-(9CI);(3-Amino-pyridin-4-yl)-methanol ,96%;3-Amino-4-hydroxymethylpyridine ,96%;(3-Amino-pyridin-4-yl)-methanol AldrichCPR
- CBNumber
- CB5695319
- Molecular Formula
- C6H8N2O
- Formula Weight
- 124.14
- MOL File
- 152398-05-5.mol
(3-AMINO-PYRIDIN-4-YL)-METHANOL Property
- Melting point:
- 118.7-118.9°C
- Boiling point:
- 366.6±27.0 °C(Predicted)
- Density
- 1.257±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- form
- solid
- pka
- 13.31±0.10(Predicted)
- Appearance
- White to yellow Solid
Safety
- Hazard Codes
- Xi,Xn
- Risk Statements
- 22-36/37/38
- Safety Statements
- 26-36
- WGK Germany
- 3
- HazardClass
- IRRITANT
- HS Code
- 29333990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- ADE000287
- Product name
- (3-Amino-pyridin-4-yl)-methanol
- Purity
- AldrichCPR
- Packaging
- 1g
- Price
- $179
- Updated
- 2025/07/31
- Product number
- A616715
- Product name
- (3-Amino-pyridin-4-yl)-methanol
- Packaging
- 250mg
- Price
- $215
- Updated
- 2021/12/16
- Product number
- OR303706
- Product name
- (3-Amino-4-pyridinyl)methanol
- Packaging
- 1g
- Price
- $247
- Updated
- 2021/12/16
- Product number
- JK206828
- Product name
- (3-Amino-pyridin-4-yl)methanol
- Purity
- 96%
- Packaging
- 1g
- Price
- $258
- Updated
- 2021/12/16
- Product number
- FA50916
- Product name
- (3-Aminopyridin-4-yl)methanol
- Packaging
- 1g
- Price
- $311.4
- Updated
- 2021/12/16
(3-AMINO-PYRIDIN-4-YL)-METHANOL Chemical Properties,Usage,Production
Chemical Properties
White solid
Synthesis
7579-20-6
152398-05-5
Step 2: Three aliquots were carefully added to an anhydrous THF (200 mL) slurry of solid compound 3-aminoisonicotinic acid (9.5 g, 69 mmol) to LiAlH4 (9.5 g, 250 mmol). The resulting reaction mixture was stirred at room temperature for 2 days. Upon completion of the reaction, it was cooled in an ice bath and water (10 mL), 15% NaOH aqueous solution (10 mL) and water (30 mL) were added sequentially dropwise to quench the reaction. The reaction mixture was filtered through a diatomaceous earth pad and washed several times with THF. After evaporation of the solvent, the resulting oil solidified on standing. The reaction mixture was purified using silica gel fast chromatography with 5% CH3OH (containing NH3)/EtOAc as eluent to afford the target product 3-amino-4-hydroxymethylpyridine 6.21 g (72% yield).LC-MS: m/z = 125 ([M+H]+).
References
[1] Patent: WO2004/831, 2003, A1. Location in patent: Page 22
[2] Patent: WO2008/108957, 2008, A2. Location in patent: Page/Page column 95
[3] Australian Journal of Chemistry, 1993, vol. 46, # 7, p. 987 - 993
[4] Patent: WO2011/38572, 2011, A1. Location in patent: Page/Page column 71; 72
(3-AMINO-PYRIDIN-4-YL)-METHANOL Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from (3-AMINO-PYRIDIN-4-YL)-METHANOL manufacturers
- Product
- (3-AMINO-PYRIDIN-4-YL)-METHANOL 152398-05-5
- Price
- US $60.00-600.00/KG
- Min. Order
- 1KG
- Purity
- 0.99
- Supply Ability
- 20 tons
- Release date
- 2023-10-12