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Boron trifluoride tetrahydrofuran complex

Product Name
Boron trifluoride tetrahydrofuran complex
CAS No.
462-34-0
Chemical Name
Boron trifluoride tetrahydrofuran complex
Synonyms
trifluoro(tetrahydrofuran)boron;Boron trifluoride tetrahydrofuran complex,50%;Boron trifL;JACS-462-34-0;Boron Trifluoride in THF;Trifluor(tetrahydrofuran)bor;Borontrifluoride THF coMplex;uoride tetrahydrofuran compL;BORON TRIFLUORIDE TETRAHYDROFURANE;trifluoro(oxolan-1-ium-1-yl)boranuide
CBNumber
CB5727881
Molecular Formula
C4H8BF3O
Formula Weight
139.91
MOL File
462-34-0.mol
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Boron trifluoride tetrahydrofuran complex Property

Melting point:
11-13 °C (lit.)
Boiling point:
180 °C (lit.)
Density 
1.268 g/mL at 25 °C (lit.)
vapor pressure 
11Pa
Flash point:
198 °F
storage temp. 
Store below +30°C.
solubility 
Miscible with dimethyl formamide.
form 
liquid
explosive limit
2.3-17.7%(V)
Water Solubility 
hydrolysis
Sensitive 
Moisture Sensitive
InChI
InChI=1S/C4H8BF3O/c6-5(7,8)9-3-1-2-4-9/h1-4H2
InChIKey
XYMZNNGTHKHCJH-UHFFFAOYSA-N
SMILES
[B+3](O1CCCC1)([F-])([F-])[F-]
CAS DataBase Reference
462-34-0(CAS DataBase Reference)
EPA Substance Registry System
Boron, trifluoro(tetrahydrofuran)-, (T-4)- (462-34-0)
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Safety

Hazard Codes 
C,T
Risk Statements 
34-48/23-35-20/22
Safety Statements 
26-27-36/37/39-45-28A-23-28
RIDADR 
UN 3265 8/PG 2
WGK Germany 
1
Hazard Note 
Toxic/Corrosive
TSCA 
TSCA listed
HazardClass 
8
PackingGroup 
II
HS Code 
29321900
Storage Class
6.1C - Combustible acute toxic Cat.3
toxic compounds or compounds which causing chronic effects
Hazard Classifications
Acute Tox. 4 Inhalation
Acute Tox. 4 Oral
Eye Dam. 1
Skin Corr. 1B
STOT RE 1 Inhalation
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H314Causes severe skin burns and eye damage

H373May cause damage to organs through prolonged or repeated exposure

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P314Get medical advice/attention if you feel unwell.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
434280
Product name
Boron trifluoride tetrahydrofuran complex
Purity
contains >0.5% sulfur dioxide as peroxide formation suppressor
Packaging
100ml
Price
$50.5
Updated
2026/03/19
Sigma-Aldrich
Product number
434280
Product name
Boron trifluoride tetrahydrofuran complex
Purity
contains >0.5% sulfur dioxide as peroxide formation suppressor
Packaging
500ml
Price
$137
Updated
2026/03/19
TRC
Product number
T793643
Product name
Trifluoro(tetrahydrofuran)boron
Packaging
5ml
Price
$45
Updated
2021/12/16
TRC
Product number
T793643
Product name
Trifluoro(tetrahydrofuran)boron
Packaging
50ml
Price
$65
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
ING0002517
Product name
BORON TRIFLUORIDE TETRAHYDROFURAN COMPLEX
Purity
95.00%
Packaging
25G
Price
$118.65
Updated
2021/12/16
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Boron trifluoride tetrahydrofuran complex Chemical Properties,Usage,Production

Chemical Properties

Colorless to light yellow liqui

Uses

Reactant or reagent involved in:

  • Deoxofluorination of alcohols and carbonyls
  • Synthesis of methacrylate-PEG-methacrylate-boron trifluoride self-doped gel polymer electrolytes
  • Hydroboration-oxidation of divinylferrocene

Reagent involved in the synthesis of biologically active molecules such as:
  • NK1 receptor antagonists
  • Complex polyketide natural products
  • Selective serotonin reuptake inhibitors

Flammability and Explosibility

Non flammable

reaction suitability

core: boron
reagent type: Lewis acid
reagent type: catalyst

Synthesis

CN202010573013.3 provides a method of preparing a boron trifluoride tetrahydrofuran complex, said method of preparation enables instantaneous complexation of tetrahydrofuran and boron trifluoride, is able to avoid oxidative discoloration of tetrahydrofuran under vacuum conditions, adopts an independent desulphurization process, eliminates the process of distillation and desulphurization, and reduces the water and sulfur dioxide contents in the product.

Using the first vacuum pump 2, the second vacuum pump 12 and the third vacuum pump 17 to evacuate the said tetrahydrofuran vaporization tank 6, the reaction tank 13 and the desulfurization tank 21 to -0.1 MPa, respectively, and keep them for 1h;

Under the condition of stirring (80 rpm), 50 kg of tetrahydrofuran was added to the tetrahydrofuran vaporization tank 6 to heat the tetrahydrofuran in said tetrahydrofuran vaporization tank 6 through the first steam heating device, and to maintain the temperature of said tetrahydrofuran at 80C and to reach the gas-liquid equilibrium state (0.15 MPa);

The cold water was passed through the cold water inlet 9, and the tetrahydrofuran vapor was passed into the reaction tank 13 at the rate of 25 kg/h and the boron trifluoride vapor was passed into the reaction tank 13 at the rate of 23.61 kg/h to start the complexation reaction, and at the end of the reaction the temperature of the reaction solution was 80 C. and cooled down to 50 C. under the condition of stirring (80 revolutions/min) to obtain the crude product of the boron trifluoride tetrahydrofuran complex;

_ x000D_

The crude product of said boron trifluoride tetrahydrofuran complex is conveyed into a desulfurization tank and heated to 50C by a second steam heating device under stirring (80 rpm) and maintaining vacuum (-0.1 MPa) conditions for 3h for desulfurization, then cooled down to 25C and discharged to obtain said boron trifluoride tetrahydrofuran.

Boron trifluoride tetrahydrofuran complex Preparation Products And Raw materials

Raw materials

Preparation Products

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Boron trifluoride tetrahydrofuran complex Suppliers

Shandong Qianyuan Polymer Material Co. , Ltd.
Tel
18678041314 18765609661
Email
2547772582@qq.com
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China
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968
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Henan Wanxiang Chemical Industry Co., Ltd.
Tel
0371-56669001 13949088811
Fax
0371-56669008
Email
Sales@58chem.cn
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China
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Shanghai Heng Pan Biological Medicine Co., LTD
Tel
18217762875
Email
2136632918@qq.com
Country
China
ProdList
11
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58
Nanjing Yili Biotechnology Co., Ltd.
Tel
15380789538
Email
2885743537@qq.com
Country
China
ProdList
8204
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Qingdao Dexin Chemical Co., Ltd
Tel
18353358123
Email
839877395@qq.com
Country
China
ProdList
280
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58
NANJING YIHUA BIOTECHNOLOGY Co., Ltd
Tel
13236563309
Email
289498891@qq.com
Country
China
ProdList
249
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J & K SCIENTIFIC LTD.
Tel
18210857532; 18210857532
Fax
86-10-82849933
Email
jkinfo@jkchemical.com
Country
China
ProdList
96815
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Meryer (Shanghai) Chemical Technology Co., Ltd.
Tel
4006356688 18621169109
Fax
86-21-61259102
Email
market03@meryer.com
Country
China
ProdList
40228
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Alfa Aesar
Tel
400-6106006
Fax
021-67582001/03/05
Email
saleschina@alfa-asia.com
Country
China
ProdList
30123
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Energy Chemical
Tel
021-021-58432009 400-005-6266
Fax
021-58436166
Email
sales8178@energy-chemical.com
Country
China
ProdList
44802
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View Lastest Price from Boron trifluoride tetrahydrofuran complex manufacturers

Shaanxi Dideu Medichem Co. Ltd
Product
Boron trifluoride tetrahydrofuran complex 462-34-0
Price
US $0.00-0.00/KG
Min. Order
1g
Purity
99%
Supply Ability
2000tons
Release date
2019-12-31
XINGTAI XINGJIU NEW MATERIAL TECHNOLOGY CO., LTD
Product
Borontrifluoridetetrahydrofurancomplex 462-34-0
Price
US $5.00/KG
Min. Order
1KG
Purity
99.9%
Supply Ability
500MT/month
Release date
2022-01-11
Career Henan Chemical Co
Product
Boron trifluoride tetrahydrofuran complex 462-34-0
Price
US $1.00/kg
Min. Order
1kg
Purity
as need
Supply Ability
as request
Release date
2018-12-21

462-34-0, Boron trifluoride tetrahydrofuran complexRelated Search:


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  • 462-34-0
  • C4H11BF3O
  • BF3THF
  • BF3C4H8O
  • C4H8BF3O
  • C4H8OBF3
  • Lewis Acids
  • Synthetic Reagents
  • Boron
  • BoronSynthetic Reagents
  • Catalysis and Inorganic Chemistry
  • Chemical Synthesis
  • Lewis Acids
  • Furan&Benzofuran