2-AMINO-5-IODOPYRIMIDINE

Product Name: 2-AMINO-5-IODOPYRIMIDINE
CAS No.: 1445-39-2
Chemical Name: 2-AMINO-5-IODOPYRIMIDINE
Synonyms: 5-iodopyrimidin-2-amine;5-Iodo-2-pyrimidinamine;2-PyriMidinaMine,5-iodo-;2-AMINO-5-IODOPYRIMIDINE;5-Iodo-pyriMidin-2-ylaMine;2-Amino-5-iodopyrimidine,97%;2-Amino-5-Iodopyrimidine 98%;2-AMINO-5-IODOPYRIMIDINE ISO 9001：2015 REACH;5-Iodopyrimidin-2-amine, 2-Amino-5-iodo-1,3-diazine
CBNumber: CB5746880
Molecular Formula: C4H4IN3
Formula Weight: 221
MOL File: 1445-39-2.mol

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2-AMINO-5-IODOPYRIMIDINE Property

Melting point:: 219 °C
Boiling point:: 364.9±34.0 °C(Predicted)
Density: 2.204±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
form: powder
pka: 2.08±0.10(Predicted)
Appearance: Off-white to light yellow Solid
Sensitive: Light Sensitive
InChI: InChI=1S/C4H4IN3/c5-3-1-7-4(6)8-2-3/h1-2H,(H2,6,7,8)
InChIKey: HAFKCGZQRIIADX-UHFFFAOYSA-N
SMILES: C1(N)=NC=C(I)C=N1
CAS DataBase Reference: 1445-39-2(CAS DataBase Reference)

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38-41-37/38-22
Safety Statements: 37/39-26-39
WGK Germany: 3
HS Code: 2933599590

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H318Causes serious eye damage

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 691844
Product name: 2-Amino-5-iodopyrimidine
Purity: 97%
Packaging: 5g
Price: $243
Updated: 2023/06/20

TRC

Product number: A612675
Product name: 2-Amino-5-iodopyrimidine
Packaging: 10g
Price: $240
Updated: 2021/12/16

TRC

Product number: A612675
Product name: 2-Amino-5-iodopyrimidine
Packaging: 5g
Price: $145
Updated: 2021/12/16

TRC

Product number: A612675
Product name: 2-Amino-5-iodopyrimidine
Packaging: 1g
Price: $50
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA61596
Product name: 2-Amino-5-iodopyrimidine
Packaging: 2g
Price: $50
Updated: 2021/12/16

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2-AMINO-5-IODOPYRIMIDINE Chemical Properties,Usage,Production

Chemical Properties

cream to brown crystalline powder

Uses

2-Amino-5-iodopyrimidine is used as a reactant in the synthesis of aminopyrimidine and cyclic guanidine amino acids.

Synthesis

109-12-6

1445-39-2

General procedure for the synthesis of 2-amino-5-iodopyrimidine from 2-aminopyrimidine: a mixture of 2-aminopyrimidine (2.4 g, 25 mmol, 1.0 eq.) and elemental iodine (2.7 g, 10.7 mmol, 0.43 eq.) was dissolved in 60 mL of glacial acetic acid, followed by the addition of periodate (0.86 g, 3.76 mmol, 0.15 eq.) and 0.5 mL of concentrated sulfuric acid dissolved in 3 mL of water. The reaction mixture was heated to 80 °C and maintained for 24 h under nitrogen protection. Upon completion of the reaction, the reaction mixture was poured into saturated aqueous sodium thiosulfate solution until the solution was clarified (200 mL each time for 3 times) and then extracted with dichloromethane. The organic phases were combined, dried with anhydrous sodium sulfate, filtered and concentrated under reduced pressure. Purification by silica gel column chromatography afforded 2-amino-5-iodopyrimidine (1.4 g, 22.2% yield) as a white solid.

References

[1] Heterocycles, 1984, vol. 22, # 5, p. 1195 - 1210
[2] Journal of Organic Chemistry, 2000, vol. 65, # 22, p. 7468 - 7474
[3] Journal of Organic Chemistry, 2008, vol. 73, # 23, p. 9326 - 9333
[4] Synthesis, 1984, # 3, p. 252 - 254
[5] Patent: CN105622638, 2016, A. Location in patent: Paragraph 0362

2-AMINO-5-IODOPYRIMIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-AMINO-5-IODOPYRIMIDINE Suppliers

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View Lastest Price from 2-AMINO-5-IODOPYRIMIDINE manufacturers

Shaanxi Dideu New Materials Co. Ltd

Product: 2-AMINO-5-IODOPYRIMIDINE 1445-39-2
Price: US $0.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 1000kg
Release date: 2025-07-05

Hebei Chuanghai Biotechnology Co., Ltd

Product: 2-AMINO-5-IODOPYRIMIDINE 1445-39-2
Price: US $10.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 10 mt
Release date: 2024-11-04

Hebei Zhuanglai Chemical Trading Co.,Ltd

Product: 2-AMINO-5-IODOPYRIMIDINE 1445-39-2
Price: US $10.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 20ton
Release date: 2024-06-03

1445-39-2, 2-AMINO-5-IODOPYRIMIDINERelated Search:

5-IODOPYRIMIDINE 4-Amino-5-iodopyrimidine 5-AMINO-2-IODOPYRIMIDINE 4-Iodopyrimidin-2-amine 4-AMINO-6-IODOPYRIMIDINE 2-AMINO-4-HYDROXY-5-IODO-6-PHENYLPYRIMIDINE 2-AMINO-4-HYDROXY-5-IODO-6-PHENOXYPYRIMIDINE 5-Iodo-2-(piperazin-1-yl)pyrimidine 2-AMINO-4,6-DIMETHYL-5-IODOPYRIMIDINE 2-AMINO-5-IODOPYRIMIDINE

2-AMINO-5-IODOPYRIMIDINE

5-Iodo-2-pyrimidinamine

2-Amino-5-iodopyrimidine,97%

5-Iodo-pyriMidin-2-ylaMine

5-iodopyrimidin-2-amine

5-Iodopyrimidin-2-amine, 2-Amino-5-iodo-1,3-diazine

2-PyriMidinaMine,5-iodo-

2-AMINO-5-IODOPYRIMIDINE ISO 9001：2015 REACH

2-Amino-5-Iodopyrimidine 98%

1445-39-2

1445-29-2

C4H4IN3

AMINO

Chemical Synthesis

Halogenated Heterocycles

Heterocyclic Building Blocks

Pyridines

Heterocycle-Pyrimidine series

Building Blocks

Pyridines, Pyrimidines, Purines and Pteredines

Pyrimidine series

Pyrimidine

Halogenated Heterocycles

Heterocyclic Building Blocks

Pyrimidines