1-BROMO-2,4,6-TRIMETHOXYBENZENE
- Product Name
- 1-BROMO-2,4,6-TRIMETHOXYBENZENE
- CAS No.
- 1131-40-4
- Chemical Name
- 1-BROMO-2,4,6-TRIMETHOXYBENZENE
- Synonyms
- RARECHEM AH CK 0052;2,4,6-TRIMETHOXYBROMOBENZENE;BROMO-2,4,6-TRIMETHOXYBENZENE;2,4,6-Trimethoxyphenyl bromide;2-BROMO-1,3,5-TRIMETHOXYBENZENE;1-BROMO-2,4,6-TRIMETHOXYBENZENE;Benzene, 2-bromo-1,3,5-trimethoxy-;2-Bromo-1,3,5-trimethoxybenzene 98%;1-Bromo-2,4,6-trimethoxybenzene 98%;N-methylcarbamic acid [(5-methyl-1,3-benzoxazol-2-yl)-(2-methylphenyl)methyl] ester
- CBNumber
- CB6117225
- Molecular Formula
- C9H11BrO3
- Formula Weight
- 247.09
- MOL File
- 1131-40-4.mol
1-BROMO-2,4,6-TRIMETHOXYBENZENE Property
- Melting point:
- 97-99°C
- Boiling point:
- 303.5±37.0 °C(Predicted)
- Density
- 1.391±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- form
- solid
- color
- White
- InChI
- InChI=1S/C9H11BrO3/c1-11-6-4-7(12-2)9(10)8(5-6)13-3/h4-5H,1-3H3
- InChIKey
- BPWYNWSOQOXOPI-UHFFFAOYSA-N
- SMILES
- C1(OC)=CC(OC)=CC(OC)=C1Br
- CAS DataBase Reference
- 1131-40-4(CAS DataBase Reference)
- EPA Substance Registry System
- 2-Bromo-1,3,5-trimethoxybenzene (1131-40-4)
Safety
- Hazard Codes
- Xi
- Risk Statements
- 20/21/22
- Safety Statements
- 22-36/37/39
- Hazard Note
- Irritant
- HS Code
- 29093090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B6448
- Product name
- 2-Bromo-1,3,5-trimethoxybenzene
- Purity
- min. 98.0 %
- Packaging
- 1G
- Price
- $57
- Updated
- 2025/07/31
- Product number
- B6448
- Product name
- 2-Bromo-1,3,5-trimethoxybenzene
- Purity
- min. 98.0 %
- Packaging
- 5G
- Price
- $171
- Updated
- 2025/07/31
- Product number
- 2200BA
- Product name
- 2-Bromo-1,3,5-trimethoxybenzene
- Packaging
- 10g
- Price
- $185
- Updated
- 2021/12/16
- Product number
- FB68031
- Product name
- 1-Bromo-2,4,6-trimethoxybenzene
- Packaging
- 25g
- Price
- $200
- Updated
- 2021/12/16
- Product number
- 126932
- Product name
- 2-Bromo-1,3,5-trimethoxybenzene
- Purity
- >95%
- Packaging
- 5g
- Price
- $252
- Updated
- 2021/12/16
1-BROMO-2,4,6-TRIMETHOXYBENZENE Chemical Properties,Usage,Production
Synthesis
570-02-5
1131-40-4
General procedure for the synthesis of 1-bromo-2,4,6-trimethoxybenzene from 2,4,6-trimethoxybenzoic acid: a mixture of 2,4,6-trimethoxybenzoic acid (1 eq., 0.5 mmol), CuBr2 or CuCl2 (2 eq., 1 mmol), Ag2CO3 (1 eq., 0.5 mmol), and PdCl2 (0.1 eq.) was dissolved in THF (3 mL) and the reaction was refluxed at 110 °C for 24 hours. Upon completion of the reaction, the reaction mixture was concentrated under reduced pressure and purified by column chromatography to afford the target product 1-bromo-2,4,6-trimethoxybenzene.
References
[1] Tetrahedron Letters, 2013, vol. 54, # 24, p. 3079 - 3081
[2] Journal of Organic Chemistry, 2016, vol. 81, # 7, p. 2794 - 2803
1-BROMO-2,4,6-TRIMETHOXYBENZENE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 1-BROMO-2,4,6-TRIMETHOXYBENZENE manufacturers
- Product
- 1-BROMO-2,4,6-TRIMETHOXYBENZENE 1131-40-4
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 99.0%
- Supply Ability
- 5000KG
- Release date
- 2024-07-18
- Product
- 1-BROMO-2,4,6-TRIMETHOXYBENZENE 1131-40-4
- Price
- US $0.10/KG
- Min. Order
- 1KG
- Purity
- 98.0%
- Supply Ability
- 10
- Release date
- 2024-07-14