3-bromo-5-methylbenzoic acid

Product Name: 3-bromo-5-methylbenzoic acid
CAS No.: 58530-13-5
Chemical Name: 3-bromo-5-methylbenzoic acid
Synonyms: 5-broMo-3-Methylbenzoic acid;3-bromo-5-methylbenzoic acid;Benzoic acid, 3-bromo-5-methyl-
CBNumber: CB61558780
Molecular Formula: C8H7BrO2
Formula Weight: 215.04
MOL File: 58530-13-5.mol

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3-bromo-5-methylbenzoic acid Property

Melting point:: 178-179.5℃
Boiling point:: 320.3±30.0 °C(Predicted)
Density: 1.599±0.06 g/cm3 (20 ºC 760 Torr)
storage temp.: Sealed in dry,Room Temperature
form: solid
pka: 3.88±0.10(Predicted)
color: Pale yellow
InChIKey: NWOMVQDBDBUANF-UHFFFAOYSA-N

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Safety

HS Code: 2916310090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: S17907
Product name: 3-BROMO-5-METHYLBENZOIC ACID
Purity: Aldrich
Packaging: 100mg
Price: $179
Updated: 2024/03/01

TRC

Product number: B687935
Product name: 3-BROMO-5-METHYLBENZOIC ACID
Packaging: 5g
Price: $415
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB71947
Product name: 3-Bromo-5-methylbenzoic acid
Packaging: 25g
Price: $550
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2721-9-18
Product name: 3-Bromo-5-methylbenzoic acid
Packaging: 25g
Price: $864
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0068600
Product name: 3-BROMO-5-METHYL-BENZOIC ACID
Purity: 95.00%
Packaging: 1G
Price: $958.65
Updated: 2021/12/16

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3-bromo-5-methylbenzoic acid Chemical Properties,Usage,Production

Chemical Properties

Off-white powder

Uses

3-Bromo-5-methylbenzoic Acid is an intermediate used to synthesize quinoline amide derivatives as novel VEGFR-2 inhibitors

Synthesis

1-bromo-3,5-dimethylbenzene (15 g, 81 mmol, 1.0 eq) in a mixture of pyridine (133 mL) and H2O (83 mL) was heated to 80°C. KMnO4 (25.6 g, 162 mmol, 2.0 eq) was added in portions over 45 min. After the addition was completed, heating was continued at 80°C for 1.5 h. The hot solution was then filtered, and the filtrate was acidified by addition of concentrated hydrochloric acid. The aqueous solution was extracted with EtOAc and the combined organic extracts washed with water and brine, dried (Na2SO4), filtered and evaporated in vacuo. The residue was purified by column chromatography (CH2Cl2 : MeOH, 80:1 to 40:1) to give 3-bromo-5-methylbenzoic acid. White solid, yield (5.2 g, 29 %). LC-MS: m/z 212.9, 215 [M+H]+. 1H NMR (400 MHz, MeOD) δ 7.91 (s, 1H), 7.79 (s, 1H), 7.57 (s, 1H), 2.38 (s, 3H).

3-bromo-5-methylbenzoic acid Preparation Products And Raw materials

Raw materials

Preparation Products

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3-bromo-5-methylbenzoic acid Suppliers

China 116 India 1 United Kingdom 2 United States 10 Global 129

Shanghai ACT chemical Limited

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Email: sales@actchemical.com
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Beijing Eternalchem Co,. Ltd.

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View Lastest Price from 3-bromo-5-methylbenzoic acid manufacturers

Hebei Weibang Biotechnology Co., Ltd

Product: 3-bromo-5-methylbenzoic acid 58530-13-5
Price: US $10.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 10 mt
Release date: 2024-11-05

Changzhou Anxuan Chemical Co., Ltd

Product: 3-bromo-5-methylbenzoic acid 58530-13-5
Price: US $0.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 1TON
Release date: 2023-02-15

Henan Bao Enluo International TradeCo.，LTD

Product: 3-bromo-5-methylbenzoic acid 58530-13-5
Price: US $50.00/kg
Min. Order: 1kg
Purity: 99.9%
Supply Ability: 10000MT
Release date: 2023-08-02

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3-bromo-5-methylbenzoic acid

5-broMo-3-Methylbenzoic acid

Benzoic acid, 3-bromo-5-methyl-

58530-13-5