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ChemicalBook > CAS DataBase List > 2-(Dicyclohexylphosphino)-3,6-dimethoxy-2'-4'-6'-tri-i-propyl-1,1'-biphenyl, min. 98% BrettPhos

2-(Dicyclohexylphosphino)-3,6-dimethoxy-2'-4'-6'-tri-i-propyl-1,1'-biphenyl, min. 98% BrettPhos

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Product Name
2-(Dicyclohexylphosphino)-3,6-dimethoxy-2'-4'-6'-tri-i-propyl-1,1'-biphenyl, min. 98% BrettPhos
CAS No.
1070663-78-3
Chemical Name
2-(Dicyclohexylphosphino)-3,6-dimethoxy-2'-4'-6'-tri-i-propyl-1,1'-biphenyl, min. 98% BrettPhos
Synonyms
BRETTPHOS;dicyclohexyl-[3,6-dimethoxy-2-[2,4,6-tri(propan-2-yl)phenyl]phenyl]phosphane;BrettPhos 96%;Brettphos Ligand;BrettPhos ChemBeads;-3,6-dimethoxybiphenyL;Dicyclohexyl(2',4',6'-tri;2-(Dicyclohexylphosphino)-3,6-diMethoxy-2'-4'-6'-tri-i-propyl-1,1';2-Dicyclohexylphosphino-2',4',6'-triisopropyl-3,6-dimethoxybiphenyl;2-Cyclohexylphosphine-3,6-dimethoxy-2',4',6'-tripropyl-1,1'-biphenyl
CBNumber
CB62129176
Molecular Formula
C35H53O2P
Formula Weight
536.77
MOL File
1070663-78-3.mol
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2-(Dicyclohexylphosphino)-3,6-dimethoxy-2'-4'-6'-tri-i-propyl-1,1'-biphenyl, min. 98% BrettPhos Property

Melting point:
191-193℃
Boiling point:
607.7±55.0 °C(Predicted)
storage temp. 
Refrigerator, under inert atmosphere
solubility 
Chloroform (Slightly), Methanol (Slightly, Sonicated)
form 
crystal
color 
white
InChI
InChI=1S/C35H53O2P/c1-23(2)26-21-29(24(3)4)33(30(22-26)25(5)6)34-31(36-7)19-20-32(37-8)35(34)38(27-15-11-9-12-16-27)28-17-13-10-14-18-28/h19-25,27-28H,9-18H2,1-8H3
InChIKey
WDVGNXKCFBOKDF-UHFFFAOYSA-N
SMILES
P(C1CCCCC1)(C1CCCCC1)C1=C(OC)C=CC(OC)=C1C1=C(C(C)C)C=C(C(C)C)C=C1C(C)C
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Safety

Risk Statements 
36/37/38
Safety Statements 
26-37-60
WGK Germany 
nwg
TSCA 
No
HS Code 
2931499090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
718742
Product name
BrettPhos
Purity
96%
Packaging
1g
Price
$183
Updated
2025/07/31
Sigma-Aldrich
Product number
718742
Product name
BrettPhos
Purity
96%
Packaging
5g
Price
$773
Updated
2025/07/31
TCI Chemical
Product number
D5664
Product name
Dicyclohexyl(2',4',6'-triisopropyl-3,6-dimethoxy-[1,1'-biphenyl]-2-yl)phosphine
Packaging
250MG
Price
$74
Updated
2025/07/31
Strem Chemicals
Product number
15-1152
Product name
2-(Dicyclohexylphosphino)-3,6-dimethoxy-2',4',6'-tri-i-propyl-1,1'-biphenyl, min. 98% BrettPhos
Packaging
250mg
Price
$49
Updated
2024/03/01
Strem Chemicals
Product number
15-1152
Product name
2-(Dicyclohexylphosphino)-3,6-dimethoxy-2',4',6'-tri-i-propyl-1,1'-biphenyl, min. 98% BrettPhos
Packaging
1g
Price
$162
Updated
2024/03/01
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2-(Dicyclohexylphosphino)-3,6-dimethoxy-2'-4'-6'-tri-i-propyl-1,1'-biphenyl, min. 98% BrettPhos Chemical Properties,Usage,Production

Reactions

  1. Ligand for palladium-catalyzed cross-coupling reactions using aryl mesylates with electron-deficient anilines.
  2. Ligand for palladium-catalyzed cross-coupling of primary arylamines at low catalyst loading.
  3. Ligand for palladium-catalyzed cross-coupling of aryl iodides and primary amines.
  4. Ligand for the Suziki-Miyaura coupling of tosylates and mesylates.
  5. Ligand for the palladium-catalyzed trifluoromethylation of aryl chlorides.
  6. Ligand for the palladium-catalyzed formation of aryl-SCF3 compounds from aryl bromides.
  7. Ligand for the nickel-catalyzed cross-coupling of styrenyl epoxides with boronic acids.
  8. Ligand for the palladium-catalyzed intramolecular CH difluoroalkylation.

Uses

Ligand for the Suziki-Miyaura coupling of tosylates and mesylates.

Uses

Buchwald Phosphine Ligands for chemical Synthesis

reaction suitability

reagent type: catalyst
reaction type: Cross Couplings

Synthesis

1070663-76-1

16523-54-9

1070663-78-3

Example 2: General procedure for the synthesis of compounds 1 to 5; A 25 mL round bottom flask was dried in an oven equipped with a magnetic stir bar and 2-iodo-2',4',6'-triisopropyl-3,6-dimethoxy-1,1'-biphenyl (1 g, 2.15 mmol) was added. The flask was evacuated and backfilled with argon and the process was repeated three times. Anhydrous THF (10 mL) was added via syringe and the reaction mixture was cooled to -78 °C. Over 10 min, n-butyllithium (2.5 M hexane solution, 940 μL, 2.36 mmol) was added dropwise. After stirring the reaction mixture for 30 min, dicyclohexylphosphonium chloride (2.26 mmol) was added dropwise over 10 min. Stirring was continued at -78 °C for 1 h. The mixture was then slowly warmed to room temperature and stirred for an additional 1.5 h. The reaction mixture was then stirred for 1.5 h. The reaction mixture was then heated to room temperature. The reaction mixture was filtered through a diatomaceous earth plug, which was pre-placed on silica (eluting with ethyl acetate). The filtrate was concentrated on a rotary evaporator to give a white solid. The crude product was recrystallized by acetone (ligands 2 to 5 were recrystallized by methanol) to give white crystals of the target product 2-(dicyclohexylphosphino)-3,6-dimethoxy-2',4',6'-triisopropyl-1,1'-biphenyl.

References

[1] Journal of the American Chemical Society, 2008, vol. 130, # 41, p. 13552 - 13554
[2] Patent: WO2009/76622, 2009, A2. Location in patent: Page/Page column 115-116

2-(Dicyclohexylphosphino)-3,6-dimethoxy-2'-4'-6'-tri-i-propyl-1,1'-biphenyl, min. 98% BrettPhos Preparation Products And Raw materials

Raw materials

Preparation Products

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2-(Dicyclohexylphosphino)-3,6-dimethoxy-2'-4'-6'-tri-i-propyl-1,1'-biphenyl, min. 98% BrettPhos Suppliers

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View Lastest Price from 2-(Dicyclohexylphosphino)-3,6-dimethoxy-2'-4'-6'-tri-i-propyl-1,1'-biphenyl, min. 98% BrettPhos manufacturers

Speranza Chemical Co., Ltd.
Product
2-(Dicyclohexylphosphino)-3,6-dimethoxy-2'-4'-6'-tri-i-propyl-1,1'-biphenyl, min. 98% BrettPhos 1070663-78-3
Price
US $0.00-0.00/KG
Min. Order
5KG
Purity
98%
Supply Ability
25KG
Release date
2024-01-05
R&D Scientific Inc.
Product
2-(Dicyclohexylphosphino)-3,6-dimethoxy-2'-4'-6'-tri-i-propyl-1,1'-biphenyl 1070663-78-3
Price
US $790.00/g
Min. Order
1g
Purity
99 %
Supply Ability
5000 Kg
Release date
2025-04-10
Shanghai UCHEM Inc.
Product
2-(Dicyclohexylphosphino)-3,6-dimethoxy-2'-4'-6'-tri-i-propyl-1,1'-biphenyl 1070663-78-3
Price
US $130.00-1185.00/g
Min. Order
5g
Purity
0.98
Supply Ability
1kg
Release date
2023-12-14

1070663-78-3, 2-(Dicyclohexylphosphino)-3,6-dimethoxy-2'-4'-6'-tri-i-propyl-1,1'-biphenyl, min. 98% BrettPhosRelated Search:

CPhos Sodium tert-butoxide Potassium tert-butoxide Tri-tert-butylphosphine Palladium chloride 1,1'-Bis(diphenylphosphino)ferrocene Triphenylphosphine 2-(Dicyclohexylphosphino)-2'-methylbiphenyl 2'-(dicyclohexylphosphino)-6-methoxy-N,N-dimethylbiphenyl-2-amine 2-(Dicyclohexylphosphino)-2'-methoxybiphenyl 2-DI-TERT-BUTYLPHOSPHINO-2',4',6'-TRIISOPROPYLBIPHENYL 2-(Dicyclohexylphosphino)biphenyl 2-(Diphenylphosphino)benzoic acid 2-(Diphenylphosphino)-biphenyl 2-DICYCLOHEXYLPHOSPHINO-2',6'-DIISOPROPOXYBIPHENYL 2-Dicyclohexylphosphino-2',6'-dimethoxybiphenyl 2-Dicyclohexylphosphino-2'-(N,N-dimethylamino)biphenyl X-PHOS

  • 2-(Dicyclohexylphosphino)-3,6-diMethoxy-2'-4' -6'-tri-i-propyl-1,1'-biphenyl
  • 2-Dicyclohexylphosphino-2',4',6'-triisopropyl-3,6-diMethoxybiphenyl, 97+%
  • 2-Dicyclohexylphosphino-2',4',6'-tri-i-propyl-3,6-diMethoxy-1,1'-biphenyl, 98% (BrettPhos)
  • BrettPhos 96%
  • 2-(Dicyclohexylphosphino)-3,6-dimethoxy-2'-4'-6'-tri-i-propyl-1,1'-biphenyl, min. 98% BrettPhos
  • 2-(Dicyclohexylphosphino)3,6-dimethoxy-2′,4′,6′-triisopropyl-1,1′-biphenyl
  • BRETTPHOS
  • Dicyclohexyl[3,6-dimethoxy-2',4',6'-tris(1-methylethyl)[1,1'-biphenyl]-2-yl]phosphine
  • 2-(Dicyclohexylphosphino)-3,6-dimethoxy-2'-4'-6'-tri-i-propyl-1,1'-biphenyl(BrettPhos)
  • BrettPhos / 2-(Dicyclohexylphosphino)-3,6-dimethoxy-2'-4'-6'-tri-i-propyl-1,1'-biphenyl
  • 2-(Dicyclohexylphosphino)-3,6-diMethoxy-2'-4'-6'-tri-i-propyl-1,1'
  • 2-(Dicyclohexylphosphino)-3,6-dimethoxy-2'-4'-6'-tri-i-propyl-1,1'-bipheny
  • 2-Dicyclohexylphosphino-2',4',6'-triisopropyl-3,6-dimethoxybiphenyl
  • 2-(Dicyclohexyl phosphino)-3,6-dimethoxy-2',4',6'-tri-i-propyl-1,1'-biphenly
  • 2-Dicyclohexylphosphino-2',4',6'-tri-i-propyl-3,6-dimethoxy-1,1'-biphenyl, (BrettPhos)
  • dicyclohexyl[3,6-dimethoxy-2',4',6'-tris(propan-2-yl)-[1,1'-biphenyl]-2-yl]phosphane
  • dicyclohexyl-[3,6-dimethoxy-2-[2,4,6-tri(propan-2-yl)phenyl]phenyl]phosphane
  • 2-(Dicyclohexylphosphino)-3,6-dimethoxy-2'-4'-6'-tri-i-propyl-1,1'-biphenyl, min. BrettPhos
  • Dicyclohexyl(2',4',6'-tri
  • Phosphine, dicyclohexyl[3,6-dimethoxy-2',4',6'-tris(1-methylethyl)[1,1'-biphenyl]-2-yl]-
  • -3,6-dimethoxybiphenyL
  • icyclohexyl-[3,6-dimethoxy-2-[2,4,6-tri(propan-2-yl)phenyl]phenyl]phosphane
  • 2-(Dicyclohexylphosphino)-3,6-dimethoxy-2'-4'-6'-tri-i-propyl-1,1'-biphenyl, min. 98% BrettPhos ISO 9001：2015 REACH
  • 2-Dicyclohexylphosphino-3,6-dimethoxy-2',4',61-trisopropyl-1,1'-biphenyl(Brettphos)
  • high purity 1070663-78-3 in China /2-(Dicyclohexylphosphino)-3,6-dimethoxy-2'-4'-6'-tri-i-propyl-1,1'-biphenyl good supplier
  • 2-Dicyclohexylphosphino-3,6-dimethoxy-2',4',6'-triisopropyl -1,1' -biphenyl (BrettPhos)
  • dicyclohexyl(2',4',6'-triisopropyl-3,6-dimethoxy-[1,1'-biphenyl]-2-yl)phosphane
  • 2-(Dicyclohexylphosphino)-3,6-dimethoxy-2'-4'-6'-tri-i-propyl-1,1'-biphenyl, min
  • Dicyclohexyl-[3,6-dimethoxy-2-[2,4,6-tri(propan-2-yl) phenyl]phenyl]phosphane (Brettphos)
  • Brettphos Ligand
  • 2-(Dicyclohexylphosphino)-3,6-dimethoxy-2'-4'-6'-tri-i-propyl-1,1'-biphenyl (BRETTPHOS)Brettphos
  • 2-(Dicyclohexylphosphino)-3,6-dimethoxy-2'-4'-6'-tri-i-propyl-1,1'-biphenyl
  • Dicyclohexyl(2',4',6'-triisopropyl-3,6-dimethoxy-[1,1'-biphenyl]-2-yl)phosphine
  • 2-(Dicyclohexylphosphino)-3,6-dimethoxy-2'-4'-6'-tri-i-propyl-1,1'-biphenyl( BrettPhos)
  • Dicydohexyl(2',4,6'-trisopropyl-3,6-dimethoxy-[1,1'-biphenyl] -2-yl)phosphine
  • 2-(Dicyclohexylphosphino)-2’,4’,6’-triisopropyl-3,6-dimethoxybiphenyl
  • BrettPhos ChemBeads
  • 2-(Dicyclohexylphosphino)-3,6-dimethoxy-2'-4'-6'-tri-1-propyl-11'-biphenyl
  • 2-Cyclohexylphosphine-3,6-dimethoxy-2',4',6'-tripropyl-1,1'-biphenyl
  • 2-(Dicyclohexylphosphoryl)-3,6-dimethoxy-2',4',6'-tripropyl-1,1'-biphenyl
  • 1070663-78-3
  • C35H53O2P
  • Achiral Phosphine
  • Aryl Phosphine
  • Buchwald Ligands Series
  • Buchwald Ligands&Precatalysts