2-METHOXY-N-METHYLBENZYLAMINE 97

Product Name: 2-METHOXY-N-METHYLBENZYLAMINE 97
CAS No.: 6851-80-5
Chemical Name: 2-METHOXY-N-METHYLBENZYLAMINE 97
Synonyms: 2-METHOXY-N-METHYLBE;(2-methoxybenzyl)methylamine;2-Methoxy-N-methylbenzylamine;N-methyl-o-methoxybenzylamine;(2-methoxybenzyl)-methyl-amine;2-Methoxy-N-methylbenzylamine 97%;N-(2-METHOXYBENZYL)-N-METHYLAMINE;2-METHOXY-N-METHYLBENZYLAMINE 97;2-Methoxy-N-methylbenzylamine;BENZENEMETHANAMINE, 2-METHOXY-N-METHYL-
CBNumber: CB6505204
Molecular Formula: C9H13NO
Formula Weight: 151.21
MOL File: 6851-80-5.mol

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2-METHOXY-N-METHYLBENZYLAMINE 97 Property

Boiling point:: 234-235 °C(lit.)
Density: 1.015 g/mL at 25 °C(lit.)
refractive index: n20/D 1.5325(lit.)
Flash point:: 222 °F
storage temp.: 2-8°C(protect from light)
form: Liquid
color: Colorless

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Safety

Hazard Codes: Xn
Risk Statements: 22-37/38-41
Safety Statements: 26-36
WGK Germany: 3
HazardClass: 8
HS Code: 2922290090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H318Causes serious eye damage

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 593958
Product name: 2-Methoxy-N-methylbenzylamine
Purity: 97%
Packaging: 1g
Price: $62.3
Updated: 2023/01/07

Sigma-Aldrich

Product number: 593958
Product name: 2-Methoxy-N-methylbenzylamine
Purity: 97%
Packaging: 5g
Price: $202
Updated: 2023/01/07

TRC

Product number: M265983
Product name: 2-Methoxy-N-methylbenzylamine
Packaging: 25mg
Price: $45
Updated: 2021/12/16

TRC

Product number: M265983
Product name: 2-Methoxy-N-methylbenzylamine
Packaging: 50mg
Price: $60
Updated: 2021/12/16

TRC

Product number: M265983
Product name: 2-Methoxy-N-methylbenzylamine
Packaging: 250mg
Price: $75
Updated: 2021/12/16

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2-METHOXY-N-METHYLBENZYLAMINE 97 Chemical Properties,Usage,Production

Synthesis

135-02-4

74-89-5

6851-80-5

Step A: 2-methoxybenzaldehyde (5.56 g, 40 mmol) was dissolved in methanol (40 mL) and methylamine (40 wt% aqueous solution, 6.9 mL, 80 mmol) and acetic acid (240 mg, 4 mmol) were added sequentially. The reaction mixture was stirred at room temperature for 16 h and then cooled in an ice bath. Sodium borohydride (1.51 g, 40 mmol) was added in batches under ice bath cooling conditions. After addition, the reaction mixture was continued to stir at room temperature for 3 hours. After completion of the reaction, most of the solvent was removed by concentration under reduced pressure. The residue was diluted with distilled water (100 mL) and ethyl acetate (100 mL) and partitioned. The aqueous phase was extracted with ethyl acetate (2 × 100 mL) and the organic phases were combined. The organic phase was washed sequentially with saturated brine, dried over anhydrous sodium sulfate, and concentrated under reduced pressure to afford the target product N-methyl-2-methoxybenzylamine (4.7 g, 79% yield). The product was characterized by 1H NMR (CDCl3, 500 MHz): δ 7.23 (d, J = 7.4 Hz, 2H), 6.91 (t, J = 7.4 Hz, 1H), 6.86 (d, J = 7.9 Hz, 1H), 3.83 (s, 3H), 3.75 (s, 2H), 2.42 (s, 3H); ESI MS m/z = 152 [M + H]+. The crude product obtained can be used directly in the subsequent reaction without further purification.

References

[1] Patent: US2006/52378, 2006, A1. Location in patent: Page/Page column 144
[2] Bioorganic and Medicinal Chemistry Letters, 2016, vol. 26, # 10, p. 2539 - 2543
[3] Journal of the American Chemical Society, 1944, vol. 66, p. 1875,1879
[4] European Journal of Medicinal Chemistry, 2014, vol. 76, p. 314 - 331
[5] Bioorganic and Medicinal Chemistry, 2015, vol. 23, # 5, p. 911 - 923

2-METHOXY-N-METHYLBENZYLAMINE 97 Preparation Products And Raw materials

Raw materials

Methylamine Sodium borohydride Ethyl acetate Acetic acid Methanol o-Anisaldehyde

Preparation Products

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2-METHOXY-N-METHYLBENZYLAMINE 97 Suppliers

China 64 India 2 Switzerland 1 Ukraine 1 United States 8 Global 76

Alchem Pharmtech,Inc.

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6851-80-5, 2-METHOXY-N-METHYLBENZYLAMINE 97Related Search:

NAPHTHOL AS-D ACETATE CALCEIN BLUE NAPHTHOL AS-D CHLOROACETATE Protopine NAPHTHOL AS ACETATE NAPHTHOL AS-TR ACETATE NAPHTHOL AS-E ACETATE D-TUBOCURARINE CHLORIDE NAPHTHOL AS-MX ACETATE N-(4-Methoxybenzyl)-N-methylamine 3-METHOXY-N-METHYLBENZYLAMINE 97 MERSALYL ACID NAPHTHOL AS-OL ACETATE 2-METHOXY-N-METHYLBENZYLAMINE 97 N-Methylbenzylamine N-ALLYL-2-(CARBOXYMETHOXYL)BENZAMIDE 10,11-DIHYDRODIBENZ[B,F][1,4]OXAZEPIN-11-ONE 3-CHLOROACETOXY-2-NAPHTHOIC ACID ANILIDE

2-METHOXY-N-METHYLBENZYLAMINE 97

N-(2-METHOXYBENZYL)-N-METHYLAMINE

2-Methoxy-N-methylbenzylamine

2-METHOXY-N-METHYLBE

2-Methoxy-N-methylbenzylamine 97%

(2-methoxybenzyl)methylamine

(2-methoxybenzyl)-methyl-amine

N-methyl-o-methoxybenzylamine

BENZENEMETHANAMINE, 2-METHOXY-N-METHYL-

2-Methoxy-<i>N</i>-methylbenzylamine

6851-80-5

H3COC6H4CH2NHCH3

Amines

C9 to C10

Nitrogen Compounds