2-Amino-3-methoxypyridine
- Product Name
- 2-Amino-3-methoxypyridine
- CAS No.
- 10201-71-5
- Chemical Name
- 2-Amino-3-methoxypyridine
- Synonyms
- 3-Methoxy-2-PyridinaMine;3-Methoxypyridin-2-amine;2-Amino-3-methoxypyridine;3-Methoxy-2-aMinopyridine;2-PyridinaMine, 3-Methoxy-;2-Amino-3-methoxypyridine, >=98%;2-Amino-3-methoxypyridine ISO 9001:2015 REACH
- CBNumber
- CB6967323
- Molecular Formula
- C6H8N2O
- Formula Weight
- 124.14
- MOL File
- 10201-71-5.mol
2-Amino-3-methoxypyridine Property
- Boiling point:
- 235.0±20.0 °C(Predicted)
- Density
- 1.139±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- pka
- 8.43±0.10(Predicted)
- form
- solid
- color
- Dark brown
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- A634710
- Product name
- 2-Amino-3-methoxypyridine
- Packaging
- 500mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- FA54411
- Product name
- 2-Amino-3-methoxypyridine
- Packaging
- 500mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- OR8879
- Product name
- 2-Amino-3-methoxypyridine
- Packaging
- 1g
- Price
- $95
- Updated
- 2021/12/16
- Product number
- 4H30-1-01
- Product name
- 2-Amino-3-methoxypyridine
- Purity
- 97%
- Packaging
- 250mg
- Price
- $30
- Updated
- 2021/12/16
- Product number
- X8586
- Product name
- 2-Amino-3-methoxypyridine
- Packaging
- 1g
- Price
- $39
- Updated
- 2021/12/16
2-Amino-3-methoxypyridine Chemical Properties,Usage,Production
Chemical Properties
solid
Synthesis
20265-37-6
10201-71-5
Under nitrogen protection, 2-nitro-3-methoxypyridine (32 g, 208 mmol) was dissolved in a solvent mixture of ethyl acetate (150 mL) and methanol (35 mL) and 10% palladium-carbon catalyst (1.5 g, 1.4 mmol) was added. After displacing the reaction system with hydrogen three times, the reaction mixture was stirred under hydrogen atmosphere for 3 hours. Upon completion of the reaction, the system was again displaced three times with nitrogen, the reaction mixture was filtered through a diatomaceous earth pad, and the filter cake was washed with ethyl acetate (2 x 35 mL). The filtrates were combined, concentrated under reduced pressure and dried under high vacuum to give 25.8 g of 2-amino-3-methoxypyridine (100% yield). The product was analyzed by LC-MS showing m/z: 125.0 (MH+); 1H NMR (300 MHz, CDCl3) δ: 7.66 (m, 1H), 6.90 (m, 1H), 6.61 (m, 2H), 4.64 (s, br, 2H), 3.83 (s, 3H).
References
[1] Patent: US2013/210818, 2013, A1. Location in patent: Paragraph 0380
[2] Patent: WO2009/115572, 2009, A2. Location in patent: Page/Page column 114-115
[3] Patent: WO2014/206903, 2014, A1. Location in patent: Page/Page column 15; 16
[4] Green Chemistry, 2017, vol. 19, # 3, p. 809 - 815
[5] Patent: WO2013/92739, 2013, A1. Location in patent: Page/Page column 16
2-Amino-3-methoxypyridine Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-Amino-3-methoxypyridine manufacturers
- Product
- 2-Amino-3-methoxypyridine 10201-71-5
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons Min
- Release date
- 2021-10-26
- Product
- 2-Amino-3-methoxypyridine 10201-71-5
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 200kg
- Release date
- 2019-12-26