Fmoc-L-citrulline
- Product Name
- Fmoc-L-citrulline
- CAS No.
- 133174-15-9
- Chemical Name
- Fmoc-L-citrulline
- Synonyms
- FMOC-CIT-OH;FMOC-L-CIT-OH;FMOC-CITRULLINE;FMOC-L-CITRULLINE;FMOC-D-ORN(CONH2)-OH;Nα-Fmoc-L-citrulline;FMOC-ORN(CARBAMOYL)-OH;Fmoc-L-citrulline - 5 g;Fmoc-L-Orn(carbamoyl)-OH;N-ALPHA-FMOC-L-CITRULLINE
- CBNumber
- CB7170261
- Molecular Formula
- C21H23N3O5
- Formula Weight
- 397.42
- MOL File
- 133174-15-9.mol
Fmoc-L-citrulline Property
- Boiling point:
- 671.5±55.0 °C(Predicted)
- Density
- 1.316±0.06 g/cm3(Predicted)
- refractive index
- -10 ° (C=1, DMF)
- storage temp.
- 2-8°C
- solubility
- Soluble in Chloroform,Dichloromethane,Ethyl Acetate,DMSO,Acetone,etc.
- form
- Solid
- pka
- 3.84±0.21(Predicted)
- color
- White to Almost white
- BRN
- 7780987
- Major Application
- peptide synthesis
- InChIKey
- NBMSMZSRTIOFOK-SFHVURJKSA-N
- SMILES
- NC(=O)NCCC[C@H](NC(=O)OCC1c2ccccc2-c3ccccc13)C(O)=O
- CAS DataBase Reference
- 133174-15-9(CAS DataBase Reference)
Safety
- WGK Germany
- 3
- F
- 10
- HazardClass
- IRRITANT
- HS Code
- 29242990
- Storage Class
- 11 - Combustible Solids
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 8.52025
- Product name
- Fmoc-Cit-OH
- Purity
- Novabiochem?
- Packaging
- 1g
- Price
- $33.8
- Updated
- 2025/07/31
- Product number
- 8.52025
- Product name
- Fmoc-Cit-OH
- Purity
- Novabiochem?
- Packaging
- 5G
- Price
- $141
- Updated
- 2025/07/31
- Product number
- 8.52025
- Product name
- Fmoc-Cit-OH
- Purity
- Novabiochem?
- Packaging
- 25g
- Price
- $555
- Updated
- 2025/07/31
- Product number
- 47518
- Product name
- Fmoc-Cit-OH
- Purity
- ≥97.0% (HPLC)
- Packaging
- 5G
- Price
- $185
- Updated
- 2025/07/31
- Product number
- F0626
- Product name
- Nalpha-[(9H-Fluoren-9-ylmethoxy)carbonyl]-L-citrulline
- Purity
- >98.0%(HPLC)
- Packaging
- 1g
- Price
- $23
- Updated
- 2025/07/31
Fmoc-L-citrulline Chemical Properties,Usage,Production
Chemical Properties
White powder
Uses
peptide synthesis
reaction suitability
reaction type: Fmoc solid-phase peptide synthesis
Synthesis
L-citrulline (1.1 equiv.) and sodium bicarbonate (2.2 equiv.) were stirred in water (0.2 M) at room temperature for 1.0h, then ethylene glycol dimethyl ether was added to the above (dimethyl ether:water= 1:1, total concentration of 0.1 M) reaction mixture, and then Fmoc-Cl (1.0 equiv.) was added, and the reaction was stirred at room temperature for 24.0h, the solvent dimethyl ether was removed under reduced pressure . The aqueous solution was extracted three times with ethyl acetate. The aqueous phase was acidified with 2M HCl (pH=1) to form a white precipitate. 10% iPrOH-EtOAc was added to the precipitate in water and stirred well to dissolve all the white precipitate in the organic solvent. The organic phase was collected and the aqueous layer was further extracted 2 times with the same 10% iPrOH-EtOAc solvent. The collected organic phase was dried over sodium sulfate. The solvent was evaporated under reduced pressure to give a clear viscous liquid. Ultrasonication with ether gave the white solid powder product Fmoc-L-citrulline, the white solid was further dried under vacuum in 96% yield.
Fmoc-L-citrulline Preparation Products And Raw materials
Raw materials
Preparation Products
Fmoc-L-citrulline Suppliers
- Tel
- 18210857532; 18210857532
- Fax
- 86-10-82849933
- jkinfo@jkchemical.com
- Country
- China
- ProdList
- 96815
- Advantage
- 76
- Tel
- 4006356688 18621169109
- Fax
- 86-21-61259102
- market03@meryer.com
- Country
- China
- ProdList
- 40228
- Advantage
- 62
- Tel
- 400-6106006
- Fax
- 021-67582001/03/05
- saleschina@alfa-asia.com
- Country
- China
- ProdList
- 30123
- Advantage
- 84
- Tel
- 021-67121386
- Fax
- 021-67121385
- Sales-CN@TCIchemicals.com
- Country
- China
- ProdList
- 24529
- Advantage
- 81
- Tel
- 021-021-58432009 400-005-6266
- Fax
- 021-58436166
- sales8178@energy-chemical.com
- Country
- China
- ProdList
- 44801
- Advantage
- 61
- Tel
- 21-61263452 13641803416
- Fax
- 86-21-61263399
- ymbetter@glbiochem.com
- Country
- China
- ProdList
- 9981
- Advantage
- 64
- Tel
- +86 (0) 571 85 58 67 18
- Fax
- 0086-571-85864795
- Country
- China
- ProdList
- 18207
- Advantage
- 66
- Tel
- +86-21-54098501
- Fax
- +86-21-54096319
- sales@sinch.com.cn
- Country
- China
- ProdList
- 11598
- Advantage
- 64
- Tel
- 021-50795510 4000665055
- Fax
- 021-50795055
- sales@accelachem.com
- Country
- China
- ProdList
- 11034
- Advantage
- 64
- Tel
- 021-58099652-8005 13585536065
- Fax
- 021-58099609
- bin.wu@shlschem.com
- Country
- China
- ProdList
- 9888
- Advantage
- 59
View Lastest Price from Fmoc-L-citrulline manufacturers
- Product
- Fmoc-L-citrulline 133174-15-9
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 20kg
- Release date
- 2018-08-15