3-(3-PYRIDINYL)BENZOIC ACID
- Product Name
- 3-(3-PYRIDINYL)BENZOIC ACID
- CAS No.
- 4385-77-7
- Chemical Name
- 3-(3-PYRIDINYL)BENZOIC ACID
- Synonyms
- AKOS BAR-0408;3-PYRID-3-YLBENZOIC ACID;3-(3'-Pyridyl)benzoic acid;3-(3-PYRIDINYL)BENZOIC ACID;3-PYRIDIN-3-YL-BENZOIC ACID;3-(3-Carboxyphenyl)pyridine;Benzoic acid, 3-(3-pyridinyl)-;3-(3'-Pyridyl)benzoic acid ,97%;3-pyridine-3-basic benzoic acid;3-(Pyridin-3-yl)benzoic acid 95%
- CBNumber
- CB7210691
- Molecular Formula
- C12H9NO2
- Formula Weight
- 199.21
- MOL File
- 4385-77-7.mol
3-(3-PYRIDINYL)BENZOIC ACID Property
- Melting point:
- 202-205.5
- Boiling point:
- 420.1±28.0 °C(Predicted)
- Density
- 1.241±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- form
- solid
- pka
- 3.78±0.10(Predicted)
- color
- white
- CAS DataBase Reference
- 4385-77-7(CAS DataBase Reference)
Safety
- Hazard Codes
- Xi,Xn
- Risk Statements
- 22-36/37/38
- Safety Statements
- 22-26-36/37/39
- Hazard Note
- Harmful
- HazardClass
- IRRITANT
- HS Code
- 29333990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
N-Bromosuccinimide Price
- Product number
- P996963
- Product name
- 3-(Pyridin-3-yl)benzoicAcid
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- JK171400
- Product name
- 3-(3'-Pyridyl)benzoicacid
- Purity
- 97%
- Packaging
- 250mg
- Price
- $56
- Updated
- 2021/12/16
- Product number
- 007709
- Product name
- 3-(3-Pyridinyl)benzoic acid
- Purity
- 97%
- Packaging
- 500mg
- Price
- $30
- Updated
- 2021/12/16
- Product number
- 007709
- Product name
- 3-(3-Pyridinyl)benzoic acid
- Purity
- 97%
- Packaging
- 1g
- Price
- $43
- Updated
- 2021/12/16
- Product number
- JK171400
- Product name
- 3-(3'-Pyridyl)benzoicacid
- Purity
- 97%
- Packaging
- 1g
- Price
- $185
- Updated
- 2021/12/16
3-(3-PYRIDINYL)BENZOIC ACID Chemical Properties,Usage,Production
Chemical Properties
White or off-white solid
Synthesis
626-55-1
25487-66-5
4385-77-7
Example 163 A Synthesis of 3-(pyridin-3-yl)benzoic acid: 3-Carboxyphenylboronic acid (1.5 g, 9 mmol) and 3-bromopyridine (1.5 g, 9.9 mmol) were dissolved in a solvent mixture of acetonitrile (40 mL) and water (40 mL). Potassium carbonate (5.5 g, 40 mmol) and bis(triphenylphosphine)palladium(II) chloride (400 mg, 0.37 mmol) were subsequently added. The reaction mixture was stirred under reflux conditions overnight. Upon completion of the reaction, the suspension was filtered while hot and the filtrate was concentrated to half the original volume. The concentrated aqueous phase was washed with dichloromethane. Subsequently, the aqueous phase was adjusted to pH=3 with 1 M hydrochloric acid, the precipitated solid was filtered and washed with water. Finally, the solid residue was dried under vacuum to give 1.5 g of 3-(pyridin-3-yl)benzoic acid in 83% yield.LC-MS (ESI) m/z: 200 (M + 1)+.
References
[1] Synlett, 2000, # 6, p. 829 - 831
[2] Patent: US2009/197863, 2009, A1. Location in patent: Page/Page column 76
[3] Journal of the American Chemical Society, 2013, vol. 135, # 5, p. 1853 - 1863
[4] Patent: JP5743418, 2015, B2. Location in patent: Paragraph 0142; 0143; 0144
3-(3-PYRIDINYL)BENZOIC ACID Preparation Products And Raw materials
Raw materials
Preparation Products
3-(3-PYRIDINYL)BENZOIC ACID Suppliers
- Tel
- --
- Fax
- --
- synthesis@chimmed.ru
- Country
- Russia
- ProdList
- 5006
- Advantage
- 81
View Lastest Price from 3-(3-PYRIDINYL)BENZOIC ACID manufacturers
- Product
- 3-Pyridin-3-yl-benzoic acid 4385-77-7
- Price
- US $1.10-9.90/KG
- Min. Order
- 1KG
- Purity
- 99% min
- Supply Ability
- 100kg
- Release date
- 2025-08-18