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3-tert-Butoxycarbonylphenylboronic acid

Product Name
3-tert-Butoxycarbonylphenylboronic acid
CAS No.
220210-56-0
Chemical Name
3-tert-Butoxycarbonylphenylboronic acid
Synonyms
B2006G1;T-BUTYL 3-BORONOBENZOATE;3-tert-Butoxycarbonylphenyl;tert-Butyl 3-boronobenzoate;3-(Tert-Butoxycarbonyl)Phenylb;3-(T-BUTOXYCARBONYL)PHENYLBORONIC ACID;1-(1,1-Dimethylethyl) 3-boronobenzoate;3-(T-BUTOXYCARBONYL)PHENYLBORBONIC ACID;3-(TERT-BUTOXYCARBONYL)PHENYLBORONIC ACID;3-(TERT-BUTOXYCARBONYL)BENZENEBORONIC ACID
CBNumber
CB7303214
Molecular Formula
C11H15BO4
Formula Weight
222.05
MOL File
220210-56-0.mol
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3-tert-Butoxycarbonylphenylboronic acid Property

Melting point:
96-102°C
Boiling point:
375.0±44.0 °C(Predicted)
Density 
1.15±0.1 g/cm3(Predicted)
storage temp. 
Keep in dark place,Sealed in dry,Room Temperature
solubility 
soluble in Methanol
form 
powder to crystal
pka
7.72±0.10(Predicted)
color 
White to Almost white
CAS DataBase Reference
220210-56-0(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-36/37/39-60-37
Hazard Note 
Irritant/Keep Cold
HS Code 
29319000
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TCI Chemical
Product number
B4726
Product name
3-(tert-Butoxycarbonyl)phenylboronic Acid (contains varying amounts of Anhydride)
Packaging
1g
Price
$42
Updated
2024/03/01
TCI Chemical
Product number
B4726
Product name
3-(tert-Butoxycarbonyl)phenylboronic Acid (contains varying amounts of Anhydride)
Packaging
5g
Price
$181
Updated
2024/03/01
Alfa Aesar
Product number
H53007
Product name
3-(tert-Butoxycarbonyl)benzeneboronic acid, 98%
Packaging
1g
Price
$53.4
Updated
2022/04/27
Alfa Aesar
Product number
H53007
Product name
3-(tert-Butoxycarbonyl)benzeneboronic acid, 98%
Packaging
5g
Price
$209
Updated
2021/12/16
TRC
Product number
B809218
Product name
3-t-Butoxycarbonylphenylboronicacid
Packaging
500mg
Price
$65
Updated
2021/12/16
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3-tert-Butoxycarbonylphenylboronic acid Chemical Properties,Usage,Production

Chemical Properties

White to light yellow crystal powde

Preparation

The 10L glass reactor is equipped with mechanical stirring, thermometer and constant pressure dropping funnel. Under nitrogen protection, add 3 moles of raw material m-carboxybenzene boric acid and 4kg tetrahydrofuran. Add 4.5 moles of thionyl chloride dropwise under reflux and stirring, react for 4 hours, cool to 0-5°C, add 7.5 moles of potassium tert-butoxide in batches, continue stirring for 1 hour after the addition, add 2kg of water, and acidify with acetic acid. Let sit and let the liquid separate. The organic phase was concentrated to obtain a crude product, which was recrystallized by adding 2 kg of petroleum ether to obtain a solid product, 3-tert-Butoxycarbonylphenylboronic acid, with a purity of 98% and a molar yield of 95%.

3-tert-Butoxycarbonylphenylboronic acid Preparation Products And Raw materials

Raw materials

Preparation Products

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3-tert-Butoxycarbonylphenylboronic acid Suppliers

Carbosynth
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View Lastest Price from 3-tert-Butoxycarbonylphenylboronic acid manufacturers

Henan Fengda Chemical Co., Ltd
Product
3-tert-Butoxycarbonylphenylboronic acid 220210-56-0
Price
US $34.00-1.20/kg
Min. Order
1kg
Purity
99%
Supply Ability
g-kg-tons, free sample is available
Release date
2024-04-08
Zhuozhou Wenxi import and Export Co., Ltd
Product
3-tert-Butoxycarbonylphenylboronic acid 220210-56-0
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-07-11
Zhuozhou Wenxi import and Export Co., Ltd
Product
3-tert-Butoxycarbonylphenylboronic acid 220210-56-0
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-07-09

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