4-AMINO-N-METHYLPHTHALIMIDE
- Product Name
- 4-AMINO-N-METHYLPHTHALIMIDE
- CAS No.
- 2307-00-8
- Chemical Name
- 4-AMINO-N-METHYLPHTHALIMIDE
- Synonyms
- AKOS BBS-00002874;IFLAB-BB F1386-0358;4-AMINO-N-METHYLPHTH;N-Amino-4-nitrophthalimide;4-AMINO-N-METHYLPHTHALIMIDE;N-METHYL-4-AMINO-PHTHALIMIDE;4-AMINO-N-METHYLPHTHALIMIDINE;4-Amino-N-methylphthalimide 97%;4-Amino-N-methylphthalimide >4-Amino-N-methylphthalimide
- CBNumber
- CB7389922
- Molecular Formula
- C9H8N2O2
- Formula Weight
- 176.17
- MOL File
- 2307-00-8.mol
4-AMINO-N-METHYLPHTHALIMIDE Property
- Melting point:
- 246-248 °C(lit.)
- Boiling point:
- 368.3±25.0 °C(Predicted)
- Density
- 1.411±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- pka
- -0.27±0.20(Predicted)
- Appearance
- Light yellow to yellow Solid
- CAS DataBase Reference
- 2307-00-8(CAS DataBase Reference)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 247715
- Product name
- 4-Amino-N-methylphthalimide
- Purity
- 97%
- Packaging
- 1g
- Price
- $151
- Updated
- 2023/06/20
- Product number
- A1561
- Product name
- 4-Amino-N-methylphthalimide
- Purity
- >98.0%(HPLC)(N)
- Packaging
- 5g
- Price
- $52
- Updated
- 2025/07/31
- Product number
- A1561
- Product name
- 4-Amino-N-methylphthalimide
- Purity
- >98.0%(HPLC)(N)
- Packaging
- 25g
- Price
- $155
- Updated
- 2025/07/31
- Product number
- JK477887
- Product name
- 4-Amino-N-methylphthalimide
- Purity
- 98%
- Packaging
- 5g
- Price
- $281
- Updated
- 2021/12/16
- Product number
- 080915
- Product name
- 5-Amino-2-methyl-1H-isoindole-1,3(2H)-dione
- Packaging
- 5g
- Price
- $399
- Updated
- 2021/12/16
4-AMINO-N-METHYLPHTHALIMIDE Chemical Properties,Usage,Production
General Description
The intermediate charge-transfer transients of 4-amino-N-methylphthalimide (4AMP) has been characterized by laser flash photolysis, steady-state and time-resolved fluorescence studies. 4AMP is a solvatochromic fluorescent dye. Transient solvation of 4AMP in binary supercritical fluids composed of 2-propanol and CO2 has been studied by frequency-domain fluorescence spectroscopy.
Synthesis
3676-85-5
74-88-4
2307-00-8
GENERAL STEPS: Potassium hydroxide (0.35 g, 6.17 mmol) was added to a solution of 4-amino-phthalimide (1.00 g, 6.17 mmol) in dimethylformamide (30 mL) and the reaction mixture was stirred at room temperature for 2 hours. Subsequently, iodomethane (0.88 g, 6.17 mmol) was added and stirring was continued at the same temperature for 18 hours. Upon completion of the reaction, water (50 mL) and ethyl acetate (50 mL) were added for extraction and the organic phase was separated. The organic phase was washed sequentially with saturated saline, dried with anhydrous sodium sulfate and concentrated under reduced pressure to remove the solvent. The crude product was purified by silica gel column chromatography (elution gradient: 0-100% cyclohexane solution of ethyl acetate) to afford N-methyl-4-amino phthalimide as a yellow solid (1.00 g, 92% yield). The product was characterized as follows: 1H NMR (DMSO-d6) δ 7.46 (d, J = 8.24 Hz, 1H), 6.90 (d, J = 2.00 Hz, 1H), 6.77 (dd, J = 8.24, 2.00 Hz, 1H), 6.42 (br.s, 2H), 2.94 (s, 3H); 13C NMR (DMSO-d6) δ 168.87, 168.57, 155.27, 135.10, 125.17, 117.33, 116.84, 107.42, 23.83; MS (m/z): 177 [M + H]+.
References
[1] Molecules, 2017, vol. 22, # 9,
4-AMINO-N-METHYLPHTHALIMIDE Preparation Products And Raw materials
Raw materials
Preparation Products
4-AMINO-N-METHYLPHTHALIMIDE Suppliers
- Tel
- 800-4238616
- Fax
- +1-888-520-1075 / +1-503-283-1987
- sales@tciamerica.com
- Country
- Americas
- ProdList
- 23653
- Advantage
- 75
View Lastest Price from 4-AMINO-N-METHYLPHTHALIMIDE manufacturers
- Product
- N-Methyl-4-aminophthalimide 2307-00-8
- Price
- US $3.00-9.00/KG
- Min. Order
- 0.1KG
- Purity
- 99%
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2025-06-27
- Product
- 4-Amino-N-methylphthalimide 2307-00-8
- Price
- US $46.51/Kg/Drum
- Min. Order
- 25Kg/Drum
- Purity
- 98.00%HPLC
- Supply Ability
- 3tons/month
- Release date
- 2023-03-10
- Product
- 5-amino-2-methylisoindole-1,3-dione 2307-00-8
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98%HPLC
- Supply Ability
- 10tons
- Release date
- 2020-02-03