ChemicalBook > CAS DataBase List > 4-BOCAMINO-NICOTINIC ACID

4-BOCAMINO-NICOTINIC ACID

Product Name: 4-BOCAMINO-NICOTINIC ACID
CAS No.: 171178-34-0
Chemical Name: 4-BOCAMINO-NICOTINIC ACID
Synonyms: 4-BOCAMINO-NICOTINIC ACID;4-TERT-BUTOXYCARBONYLAMINO-NICOTINIC ACID;4-Tert-butoxycarbonylamino-nicatinec acid;4-{[(tert-butoxy)carbonyl]aMino}pyridine-3-carboxylic acid;4-[(2-methylpropan-2-yl)oxycarbonylamino]pyridine-3-carboxylic acid;3-Pyridinecarboxylic acid, 4-[[(1,1-dimethylethoxy)carbonyl]amino]-;4-[[(2-methylpropan-2-yl)oxy-oxomethyl]amino]-3-pyridinecarboxylic acid
CBNumber: CB7692761
Molecular Formula: C11H14N2O4
Formula Weight: 238.24
MOL File: 171178-34-0.mol

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4-BOCAMINO-NICOTINIC ACID Property

Boiling point:: 348.4±27.0 °C(Predicted)
Density: 1.293±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
pka: 1.70±0.36(Predicted)
Appearance: White to light yellow Solid

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Safety

Hazard Codes: Xi
Risk Statements: 43
Safety Statements: 36/37

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H317May cause an allergic skin reaction

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

AK Scientific

Product number: W3733
Product name: 4-Boc-Aminonicotinicacid
Packaging: 100mg
Price: $81
Updated: 2021/12/16

Matrix Scientific

Product number: 072740
Product name: 4-Boc-Aminonicotinic acid
Purity: 95+%
Packaging: 1g
Price: $159
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: AAA0007033
Product name: 4-BOC-AMINONICOTINIC ACID
Purity: 95.00%
Packaging: 250MG
Price: $214.2
Updated: 2021/12/16

Matrix Scientific

Product number: 072740
Product name: 4-Boc-Aminonicotinic acid
Purity: 95+%
Packaging: 5g
Price: $1038
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: AAA0007033
Product name: 4-BOC-AMINONICOTINIC ACID
Purity: 95.00%
Packaging: 1G
Price: $1085.7
Updated: 2021/12/16

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4-BOCAMINO-NICOTINIC ACID Chemical Properties,Usage,Production

Synthesis

280115-84-6

171178-34-0

General procedure for the synthesis of 4-((tert-butoxycarbonyl)amino)nicotinic acid from methyl 4-((tert-butoxycarbonyl)amino)nicotinate: 4-((tert-butoxycarbonyl)amino)nicotinic acid methyl ester (6.02 g, 23.86 mmol) was dissolved in dioxane (100 mL), and an aqueous sodium hydroxide solution (0.970 N, 28.05 mL, 27.20 mmol ). The reaction mixture was heated to 60°C and held for 1 hr and subsequently cooled to room temperature. To the cooled mixture was added aqueous hydrochloric acid (1.03 M, 26.99 mL, 27.20 mmol) and then extracted with chloroform (5 x 100 mL). The organic phases were combined, dried over anhydrous magnesium sulfate, filtered and concentrated under reduced pressure to give 4-((tert-butoxycarbonyl)amino)nicotinic acid as a creamy solid (4.70 g, 83% yield).

References

[1] Patent: WO2006/100310, 2006, A1. Location in patent: Page/Page column 34
[2] Patent: WO2005/32481, 2005, A2. Location in patent: Page/Page column 42-43
[3] Patent: WO2005/32481, 2005, A2. Location in patent: Page/Page column 42-43

4-BOCAMINO-NICOTINIC ACID Preparation Products And Raw materials

Raw materials

Hexane Di-tert-butyl dicarbonate Triethylamine 4-Amino-3-pyridinecarboxylic acid Ethyl acetate Dichloromethane

Preparation Products

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171178-34-0, 4-BOCAMINO-NICOTINIC ACIDRelated Search:

Nicotinic acid 4-TERT-BUTOXYCARBONYLAMINO-6-METHYL-NICOTINIC ACID METHYL ESTER 4-BOCAMINO-NICOTINIC ACID 4-TERT-BUTOXYCARBONYLAMINO-6-METHYL-NICOTINIC ACID TERT-BUTYL 3-FORMYLPYRIDIN-4-YLCARBAMATE 4-(Boc-amino)pyridine

4-BOCAMINO-NICOTINIC ACID

4-TERT-BUTOXYCARBONYLAMINO-NICOTINIC ACID

4-{[(tert-butoxy)carbonyl]aMino}pyridine-3-carboxylic acid

4-[[(2-methylpropan-2-yl)oxy-oxomethyl]amino]-3-pyridinecarboxylic acid

3-Pyridinecarboxylic acid, 4-[[(1,1-dimethylethoxy)carbonyl]amino]-

4-Tert-butoxycarbonylamino-nicatinec acid

4-[(2-methylpropan-2-yl)oxycarbonylamino]pyridine-3-carboxylic acid

171178-34-0