Methyl 3-amino-2-methylbenzoate

Product Name: Methyl 3-amino-2-methylbenzoate
CAS No.: 18583-89-6
Chemical Name: Methyl 3-amino-2-methylbenzoate
Synonyms: AKOS BB-3100;3-Amino-2-Methylbenzoate;METHYL 3-AMINO-O-TOLUATE;Lenalidomide Impurity 27;Lenalidomide Impurity 98;3-aminotoluene methyl ester;METHYL 3-AMINO-2-METHYLBENZOATE;METHYL 2-METHYL-3-AMINO BENZOATE;Methyl 3-Amino-2-melthyl benzoate;Methyl 3-amino-2-methylbenzoate 96%
CBNumber: CB7702334
Molecular Formula: C9H11NO2
Formula Weight: 165.19
MOL File: 18583-89-6.mol

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Methyl 3-amino-2-methylbenzoate Property

Boiling point:: 300 °C (lit.)
Density: 1.146 g/mL at 25 °C (lit.)
refractive index: n20/D 1.573(lit.)
Flash point:: 220 °F
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
solubility: Chloroform (Sparingly), Methanol (Slightly)
form: Liquid
pka: 3.31±0.10(Predicted)
color: Colorless to brown
CAS DataBase Reference: 18583-89-6(CAS DataBase Reference)

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 26-36
WGK Germany: 3
HazardClass: IRRITANT
HS Code: 2922498590

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 530271
Product name: Methyl 3-amino-2-methylbenzoate
Purity: 96%
Packaging: 25g
Price: $162
Updated: 2023/06/20

TCI Chemical

Product number: A1563
Product name: Methyl 3-Amino-2-methylbenzoate
Purity: >98.0%(GC)(T)
Packaging: 5g
Price: $79
Updated: 2025/07/31

TCI Chemical

Product number: A1563
Product name: Methyl 3-Amino-2-methylbenzoate
Purity: >98.0%(GC)(T)
Packaging: 25g
Price: $228
Updated: 2025/07/31

TRC

Product number: M331018
Product name: Methyl 3-amino-2-methylbenzoate
Packaging: 250mg
Price: $45
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4658-1-Z6
Product name: Methyl 3-amino-2-methylbenzoate
Packaging: 25g
Price: $48
Updated: 2021/12/16

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Methyl 3-amino-2-methylbenzoate Chemical Properties,Usage,Production

Chemical Properties

off-white powder

Uses

Methyl 3-Amino-2-methylbenzoate can be used in petroleum recovery process.

Synthesis

52130-17-3

18583-89-6

A. General procedure for the synthesis of methyl 3-amino-2-methylbenzoate: 10 g (66.2 mmol) of 3-amino-2-methylbenzoic acid and 20 g of p-toluenesulfonic acid monohydrate were dissolved in 400 mL of methanol and the reaction was carried out at reflux overnight. After completion of the reaction, the reaction solution was diluted with a mixture of ethyl acetate and 1 M potassium carbonate solution. After cooling, the organic and aqueous layers were separated. The organic layer was washed sequentially with 1M potassium carbonate solution and saturated brine, dried over anhydrous sodium sulfate, filtered, and concentrated to give 9.23 g of an orange oily product in 85% yield. The product was characterized as follows: 1H NMR (CDCl3): δ 2.34 (s, 3H), 3.73 (br.s, 2H), 3.88 (s, 3H), 6.81 (d, J = 7.96 Hz, 1H), 7.05 (t, J = 7.78 Hz, 1H), 7.19-7.30 (m, 1H). IR (CHCl3): 3406, 3027, 3012, 2.30 (m). 3027, 3012, 2978, 2953, 1718, 1621, 1467, 1435, 1315, 1301, 1265, 1196, 1159, 1108, 1066, 1045, 810 cm-1. MS (FD): m/e 165 (M+, 100).

References

[1] Patent: US5952343, 1999, A
[2] Patent: US5461154, 1995, A
[3] Patent: US5484926, 1996, A
[4] Patent: US6555541, 2003, B1

Methyl 3-amino-2-methylbenzoate Preparation Products And Raw materials

Raw materials

Preparation Products

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Methyl 3-amino-2-methylbenzoate Suppliers

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View Lastest Price from Methyl 3-amino-2-methylbenzoate manufacturers

Shaanxi Dideu New Materials Co. Ltd

Product: Methyl 3-amino-2-methylbenzoate 18583-89-6
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 99.0%
Supply Ability: 10000KGS
Release date: 2025-05-12

Hebei Chuanghai Biotechnology Co., Ltd

Product: Methyl 3-amino-2-methylbenzoate 18583-89-6
Price: US $10.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 10 mt
Release date: 2025-03-10

Career Henan Chemical Co

Product: Methyl 3-amino-2-methylbenzoate 18583-89-6
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100kg
Release date: 2019-07-11

18583-89-6, Methyl 3-amino-2-methylbenzoateRelated Search:

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Methyl 3-amino-2-methylbenzoate 96%

Lenalidomide Impurity 27

Methyl 3-Amino-2-methylbenzoate &gt

Lenalidomide Impurity 98

Benzoic acid, 3-amino-2-methyl-, methyl ester (9CI, ACI)

3-amino-2-methyl-Benzoic acid methyl ester (9CI ACI)

Methyl3-Amino-2-Methylbenzoate/Methyl 2-Methyl-3-Aminobenzoate

3-aminotoluene methyl ester

18583-89-6

CH3C6H3NH2CO2CH3

ESTER

Organic Building Blocks

Esters

Building Blocks

C8 to C9

Carbonyl Compounds

Benzoic acid

C8 to C9

Carbonyl Compounds

Esters