1-IODO-2-PHENOXY-BENZENE

Uses

Product Name: 1-IODO-2-PHENOXY-BENZENE
CAS No.: 34883-46-0
Chemical Name: 1-IODO-2-PHENOXY-BENZENE
Synonyms: 2-Iododiphenyl ether;-IODO-2-PHENOXY-BENZENE;1-IODO-2-PHENOXY-BENZENE;1-(2-iodophenoxy)benzene;2-Iodophenyl phenyl ether;Benzene, 1-iodo-2-phenoxy-;Benzaldehyde,3,4-dichloro-4-hydroxy-
CBNumber: CB7836138
Molecular Formula: C12H9IO
Formula Weight: 296.1
MOL File: 34883-46-0.mol

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1-IODO-2-PHENOXY-BENZENE Property

Melting point:: 56℃
Boiling point:: 198-202 °C
Density: 1.626±0.06 g/cm3(Predicted)
storage temp.: 2-8°C, protect from light
Appearance: White to off-white Solid
InChI: InChI=1S/C12H9IO/c13-11-8-4-5-9-12(11)14-10-6-2-1-3-7-10/h1-9H
InChIKey: AOZLGVLVAJRLPS-UHFFFAOYSA-N
SMILES: C1(I)=CC=CC=C1OC1=CC=CC=C1

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

ChemScene

Product number: CS-0060560
Product name: 1-Iodo-2-phenoxybenzene
Purity: 99.84%
Packaging: 250mg
Price: $55
Updated: 2021/12/16

ChemScene

Product number: CS-0060560
Product name: 1-Iodo-2-phenoxybenzene
Purity: 99.84%
Packaging: 1g
Price: $110
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0069372
Product name: 1-IODO-2-PHENOXY-BENZENE
Purity: 95.00%
Packaging: 5MG
Price: $495.15
Updated: 2021/12/16

Ambeed

Product number: A332174
Product name: 1-Iodo-2-phenoxybenzene
Purity: 98%
Packaging: 100mg
Price: $30
Updated: 2021/12/16

Ambeed

Product number: A332174
Product name: 1-Iodo-2-phenoxybenzene
Purity: 98%
Packaging: 250mg
Price: $47
Updated: 2021/12/16

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1-IODO-2-PHENOXY-BENZENE Chemical Properties,Usage,Production

Uses

2-Iododiphenyl ether is used as an organic intermediate.

Synthesis

2688-84-8

34883-46-0

The general procedure for the synthesis of 2-iododiphenyl ether from 2-aminodiphenyl ether is as follows: 1. the intermediate Bn-2 (1 eq.) and p-toluenesulfonic acid monohydrate (PTSA-H2O, 72.5 g, 3 eq.) were dissolved in acetonitrile (224 mL, 1.3 M) under ice-bath conditions and cooled to 5 °C. 2. A solution of sodium nitrite (NaNO2, 41.7 g, 2 eq.) dissolved in 240 mL of water was added dropwise. 3. After the dropwise addition was completed, the reaction mixture was kept at 5°C for 1 hour to produce the diazonium salt. 4. The resulting diazonium salt solution was slowly added to a solution of potassium iodide (KI, 100 g, 2 eq.) dissolved in 300 mL of water. 5. Upon completion of the reaction, the residue was extracted with ethyl acetate (EtOAc) and the organic layers were combined. 6. The combined organic layers were washed with 10% sodium sulfite (Na2SO3) solution and dried with anhydrous sodium sulfate (Na2SO4). 7. After filtration, the organic layer was concentrated under reduced pressure to obtain the crude product. 8. The crude product was purified by silica gel column chromatography to obtain the target compound 2-iododiphenyl ether.

References

[1] Chemistry - A European Journal, 2014, vol. 20, # 39, p. 12553 - 12558
[2] Journal of the Indian Chemical Society, 2013, vol. 90, # 10, p. 1537 - 1555
[3] Chemistry - A European Journal, 2012, vol. 18, # 11, p. 3286 - 3291
[4] Patent: US2018/155312, 2018, A1. Location in patent: Paragraph 0087; 0093-0095
[5] Journal of the American Chemical Society, 2015, vol. 137, # 11, p. 3775 - 3778

1-IODO-2-PHENOXY-BENZENE Preparation Products And Raw materials

Raw materials

Preparation Products

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1-IODO-2-PHENOXY-BENZENE Suppliers

China 58 India 1 United States 6 Global 65

Aladdin Scientific

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Synthonix Inc

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Combi-Blocks Inc.

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AlliChem, LLC

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APAC Pharmaceutical, LLC

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ChemPacific Corporation

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View Lastest Price from 1-IODO-2-PHENOXY-BENZENE manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 1-IODO-2-PHENOXY-BENZENE 34883-46-0
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 20T
Release date: 2024-07-31

Career Henan Chemical Co

Product: 1-iodo-2-phenoxybenzene 34883-46-0
Price: US $1.00/KG
Min. Order: 1KG
Purity: 98% HPLC
Supply Ability: 10 tons
Release date: 2020-02-14

34883-46-0, 1-IODO-2-PHENOXY-BENZENERelated Search:

Levothyroxine 3,3',5-TRIIODOTHYROPROPIONIC ACID ERYTHROSIN B 3,3',5-TRIIODOTHYROACETIC ACID Sodium levothyroxine Liothyronine sodium REVERSE T3 3,3',5,5'-TETRAIODOTHYRO-ACETIC ACID 3,5-DIIODO-4'-(4-HYDROXYPHENOXY)BENZOIC ACID ROSE BENGAL LACTONE 2,4-DICHLORO-1-(2-IODOPHENOXY)BENZENE 3,3',5'-Triiodo-D-thyronine TRIIODOFLUORESCEIN ERYTHROSIN B ISOTHIOCYANATE, ISOMER II 3,5-Diiodo-D-thyronine 3 5-DIIODOTHYROPROPIONIC ACID 3,5,3',5'-TETRAIODOTHYROFORMIC ACID DIIODODIMETHYLFLUORESCEIN

Benzene, 1-iodo-2-phenoxy-

1-IODO-2-PHENOXY-BENZENE

2-Iododiphenyl ether

2-Iodophenyl phenyl ether

1-(2-iodophenoxy)benzene

-IODO-2-PHENOXY-BENZENE

Benzaldehyde,3,4-dichloro-4-hydroxy-

34883-46-0