2H-INDOL-2-ONE, 6-AMINO-1,3-DIHYDRO-

Product Name: 2H-INDOL-2-ONE, 6-AMINO-1,3-DIHYDRO-
CAS No.: 150544-04-0
Chemical Name: 2H-INDOL-2-ONE, 6-AMINO-1,3-DIHYDRO-
Synonyms: 6-Aminooxindole;6-aminoindolin-2-one;6-amino-2-indolinone;6-Amino-2-oxoindoline;6-aMino-1,3-dihydro-indol-2-one;Indole-2-one, 2,3-dihydro-6-amino-;6-AMino-2,3-dihydro-1H-indol-2-one;2H-INDOL-2-ONE, 6-AMINO-1,3-DIHYDRO-;6-amino-1,3-dihydro-2H-indol-2-one 1HCl;2H-Indol-2-one,6-amino-1,3-dihydro-(9CI)
CBNumber: CB7847507
Molecular Formula: C8H8N2O
Formula Weight: 148.16
MOL File: 150544-04-0.mol

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2H-INDOL-2-ONE, 6-AMINO-1,3-DIHYDRO- Property

Melting point:: 200 °C (decomp)
Boiling point:: 394.3±42.0 °C(Predicted)
Density: 1.307±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
pka: 14.24±0.20(Predicted)
Appearance: Brown to black Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: A615683
Product name: 6-Aminoindolin-2-one
Packaging: 500mg
Price: $200
Updated: 2021/12/16

Matrix Scientific

Product number: 118950
Product name: 6-Aminoindolin-2-one
Purity: 95+%
Packaging: 250mg
Price: $252
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA132635
Product name: 6-Amino-1,3-dihydro-2H-indol-2-one hydrochloride
Packaging: 500mg
Price: $300
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA132635
Product name: 6-Amino-1,3-dihydro-2H-indol-2-one hydrochloride
Packaging: 100mg
Price: $87
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0373142
Product name: 6-AMINO-1,3-DIHYDRO-2H-INDOL-2-ONE
Purity: 95.00%
Packaging: 5MG
Price: $498.58
Updated: 2021/12/16

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2H-INDOL-2-ONE, 6-AMINO-1,3-DIHYDRO- Chemical Properties,Usage,Production

Synthesis

643-43-6

150544-04-0

General procedure for the synthesis of 6-aminoindolones from 2,4-dinitrophenylacetic acid: 2,4-dinitrophenylacetic acid (10 g, 44 mmol) was dissolved in ethanol (200 mL) and purged with nitrogen. 10% Pd/C catalyst (400 mg) was added and the reaction was hydrogenated at 45 psi hydrogen pressure for 2 hours. Upon completion of the reaction, the mixture was transferred to a round bottom flask, p-toluenesulfonic acid (150 mg) was added, and heated to reflux overnight. The reaction mixture was filtered through diatomaceous earth to remove the catalyst and the filtrate was subsequently concentrated. The product precipitated as brown crystals and 4.68 g (72% yield) was obtained by filtration. The product was characterized by 1H NMR (DMSO-d6, 400 MHz): δ 3.20 (s, 2H), 4.97 (br s, 2H), 6.07 (m, 2H), 6.76 (d, J = 8.7 Hz, 1H), 10.05 (s, 1H); HPLC retention time: 2.123 min; LRMS (M+) 148.7.

References

[1] Patent: US2005/256125, 2005, A1. Location in patent: Page/Page column 29
[2] Patent: WO2009/79767, 2009, A1. Location in patent: Page/Page column 87
[3] Journal of Organic Chemistry, 2015, vol. 80, # 21, p. 10939 - 10954
[4] ChemMedChem, 2012, vol. 7, # 5, p. 777 - 791
[5] Chemische Berichte, 1881, vol. 14, p. 830

2H-INDOL-2-ONE, 6-AMINO-1,3-DIHYDRO- Preparation Products And Raw materials

Raw materials

Preparation Products

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2H-INDOL-2-ONE, 6-AMINO-1,3-DIHYDRO- Suppliers

China 68 Europe 1 France 1 Germany 3 India 1 United Kingdom 1 United States 12 Global 87

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View Lastest Price from 2H-INDOL-2-ONE, 6-AMINO-1,3-DIHYDRO- manufacturers

Career Henan Chemical Co

Product: 2H-INDOL-2-ONE, 6-AMINO-1,3-DIHYDRO- 150544-04-0
Price: US $9.80/KG
Min. Order: 1g
Purity: ≥99%
Supply Ability: 100kg
Release date: 2020-01-14

150544-04-0, 2H-INDOL-2-ONE, 6-AMINO-1,3-DIHYDRO-Related Search:

6-Quinazolinemethanamine 6-Aminomethylquinoline 6-Aminoindole 2H-Indol-2-one, 3-amino-1,3-dihydro-3-methyl- 3H-Indol-3-one, 2-amino-1,2-dihydro-1-methyl- 2H-Indol-2-one, 3-amino-1,3-dihydro-1-methyl- 2H-INDOL-2-ONE, 5-AMINO-1,3-DIHYDRO- 4H-Pyrimido[4,5-b]indol-4-one, 2-amino-1,9-dihydro-6-hydroxy- (9CI) 7-Aminooxindole 4-Aminooxindole 6-AMINO-3,3-DIMETHYL-2-OXO-1,3-DIHYDRO-INDOLE N-(2-OXO-2,3-DIHYDRO-1H-INDOL-6-YL)-ACETAMIDE 7-methyl-6-nitro-2,3-dihydro-1H-indole-2,3-dione 2H-INDOL-2-ONE, 6-AMINO-1,3-DIHYDRO- 6-NITRO-1,3-DIHYDRO-INDOL-2-ONE

6-amino-1,3-dihydro-2H-indol-2-one hydrochloride

6-aMino-1,3-dihydro-indol-2-one

6-Amino-2-oxoindoline

6-amino-2-indolinone

Indole-2-one, 2,3-dihydro-6-amino-

2H-INDOL-2-ONE, 6-AMINO-1,3-DIHYDRO-

6-Aminooxindole

2H-Indol-2-one,6-amino-1,3-dihydro-(9CI)

6-aminoindolin-2-one

6-amino-1,3-dihydro-2H-indol-2-one(SALTDATA: HCl)

6-amino-1,3-dihydro-2H-indol-2-one 1HCl

6-AMino-2,3-dihydro-1H-indol-2-one

150544-04-0

AMINEPRIMARY