(4-METHYLPYRIDIN-3-YL)METHANOL
- Product Name
- (4-METHYLPYRIDIN-3-YL)METHANOL
- CAS No.
- 4664-27-1
- Chemical Name
- (4-METHYLPYRIDIN-3-YL)METHANOL
- Synonyms
- NSC30040;4-Picoline-3-methanol;4-Methyl-3-PyridineMethanol;(4-methyl-3-pyridyl)methanol;3-Pyridinemethanol, 4-methyl-;(4-METHYLPYRIDIN-3-YL)METHANOL;3-HydroxyMethyl-4-Methylpyridine;(4-Methylpyridin-3-yl)methanol?New
- CBNumber
- CB7849804
- Molecular Formula
- C7H9NO
- Formula Weight
- 123.16
- MOL File
- 4664-27-1.mol
(4-METHYLPYRIDIN-3-YL)METHANOL Property
- Melting point:
- 44-46℃
- Boiling point:
- 125-127℃ (1.5-2.0 Torr)
- Density
- 1.092±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 13.71±0.10(Predicted)
- Appearance
- White to yellow Solid
Safety
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- M327980
- Product name
- (4-methylpyridin-3-yl)methanol
- Packaging
- 500mg
- Price
- $330
- Updated
- 2021/12/16
- Product number
- CS-0053194
- Product name
- (4-Methylpyridin-3-yl)methanol
- Packaging
- 5g
- Price
- $429
- Updated
- 2021/12/16
- Product number
- 084204
- Product name
- (4-Methylpyridin-3-yl)methanol
- Purity
- 97%
- Packaging
- 1g
- Price
- $488
- Updated
- 2021/12/16
- Product number
- CS-0053194
- Product name
- (4-Methylpyridin-3-yl)methanol
- Packaging
- 10g
- Price
- $712
- Updated
- 2021/12/16
- Product number
- CS-0053194
- Product name
- (4-Methylpyridin-3-yl)methanol
- Packaging
- 1g
- Price
- $121
- Updated
- 2021/12/16
(4-METHYLPYRIDIN-3-YL)METHANOL Chemical Properties,Usage,Production
Synthesis
3222-50-2
4664-27-1
The general procedure for the synthesis of 3-hydroxymethyl-4-methylpyridine from 4-methylpyridine-3-carboxylic acid was as follows: a tetrahydrofuran solution (15 mL) of 1.0 mol/L borane-tetrahydrofuran complex was slowly added to a tetrahydrofuran solution (15 mL) containing 4-methylnicotinic acid (686 mg), followed by a heating and refluxing for 2 hours. Upon completion of the reaction, 2.0 mol/L hydrochloric acid solution (5 mL) was added dropwise to the reaction system and refluxing was continued for 0.5 hours. After the reaction mixture was cooled to room temperature, it was extracted with ethyl acetate. The organic phase was washed sequentially with aqueous sodium carbonate solution and saturated aqueous sodium chloride solution, followed by drying with anhydrous sodium sulfate. After the solvent was removed by distillation under reduced pressure, the resulting residue was purified by silica gel column chromatography (eluent ratio: ethyl acetate:methanol=1:0→9:1), and the target product (4-methylpyridin-3-yl)methanol (270 mg) was finally obtained as a white solid. Mass spectrum (ESI m/z): 124 (M+H). Retention time (min): 1.11.
References
[1] Patent: US2016/168139, 2016, A1. Location in patent: Paragraph 0958-0962
(4-METHYLPYRIDIN-3-YL)METHANOL Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from (4-METHYLPYRIDIN-3-YL)METHANOL manufacturers
- Product
- (4-Methylpyridin-3-yl)methanol 4664-27-1
- Price
- US $1.10-9.90/kg
- Min. Order
- 1kg
- Purity
- 99%min
- Supply Ability
- 100kg
- Release date
- 2025-08-18
- Product
- (4-Methylpyridin-3-yl)methanol 4664-27-1
- Price
- US $1.00-22.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100000KG
- Release date
- 2024-08-01
- Product
- (4-METHYLPYRIDIN-3-YL)METHANOL 4664-27-1
- Price
- US $0.00/g
- Min. Order
- 1g
- Purity
- 95%min
- Supply Ability
- 20kgs/month
- Release date
- 2019-11-18