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2-Acetylbutyrolactone

Description Reference
Product Name
2-Acetylbutyrolactone
CAS No.
517-23-7
Chemical Name
2-Acetylbutyrolactone
Synonyms
ABL;3-acetyldihydrofuran-2(3H)-one;ABL1;ACETYLBUTYROLACTONE;2-Acetylbutyrolacton;-Acetyl-hydroxybutyricacid;2-Oxo-3-acetyltetrahydrofuran;JTK7;p190;bcr/abl
CBNumber
CB8101532
Molecular Formula
C6H8O3
Formula Weight
128.13
MOL File
517-23-7.mol
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2-Acetylbutyrolactone Property

Melting point:
<25 °C
Boiling point:
107-108 °C5 mm Hg(lit.)
Density 
1.19 g/mL at 25 °C(lit.)
vapor pressure 
0.131Pa at 20℃
refractive index 
n20/D 1.459(lit.)
Flash point:
>230 °F
storage temp. 
Keep in dark place,Sealed in dry,Room Temperature
solubility 
200g/l
pka
12.00±0.20(Predicted)
form 
Liquid
color 
Clear
Water Solubility 
310 g/L (20 ºC)
Merck 
14,83
BRN 
112676
Stability:
Stable. Incompatible with strong oxidizing agents, strong bases.
LogP
-0.43 at 22℃
CAS DataBase Reference
517-23-7(CAS DataBase Reference)
NIST Chemistry Reference
2(3H)-Furanone, 3-acetyldihydro-(517-23-7)
EPA Substance Registry System
2(3H)-Furanone, 3-acetyldihydro- (517-23-7)
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Safety

Hazard Codes 
Xi,T
Risk Statements 
36/37/38-61
Safety Statements 
26-36-37/39-45-53
WGK Germany 
1
RTECS 
LU3456000
TSCA 
Yes
HS Code 
29322980
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P202Do not handle until all safety precautions have been read and understood.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P308+P313IF exposed or concerned: Get medical advice/attention.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
A13409
Product name
α-Acetylbutyrolactone
Purity
≥99%
Packaging
100g
Price
$41.1
Updated
2024/03/01
Sigma-Aldrich
Product number
A13409
Product name
α-Acetylbutyrolactone
Purity
≥99%
Packaging
500g
Price
$45.4
Updated
2024/03/01
Sigma-Aldrich
Product number
A0608
Product name
ABL1 (27-end), active, His-tagged from mouse
Purity
PRECISIO? Kinase, recombinant, expressed in baculovirus infected Sf9 cells, ≥70% (SDS-PAGE), buffered aqueous glycerol solution
Packaging
10μG
Price
$522
Updated
2024/03/01
Sigma-Aldrich
Product number
SRP5279
Product name
ABL1, active, His tagged human
Purity
PRECISIO?, recombinant, expressed in baculovirus infected Sf9 cells, ≥70% (SDS-PAGE), buffered aqueous glycerol solution
Packaging
10μG
Price
$498
Updated
2023/06/20
TCI Chemical
Product number
A0681
Product name
alpha-Acetyl-gamma-butyrolactone
Purity
>99.0%(GC)
Packaging
25g
Price
$23
Updated
2024/03/01
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2-Acetylbutyrolactone Chemical Properties,Usage,Production

Description

It is an important intermediate involved in the synthesis of chemical and pharmaceutical products such as vitamin B, 3,4-substituted pyridine, 5-(2-Hydroxyethyl)-4-methylthiazole. In presence of 2-acetylbutyrolactone, reaction of tert-butyl isocyanide with dialkyl acetylenedicarboxylates leads to the formation of dialkyl (E)-2-{(tert-butylamino)[2-oxo-4,5-dihydro-3(2H)-furanylidene]methyl}-2-butenedioates.1 Moreover, reaction of 2-acetylbutyrolactone with thiosemicarbazide and 3-(2-bromo-acetyl)-chromen-2-one in anhydrous ethanol produced 3-{2-[5-hydroxyl-4-(2-hydroxyl-ethyl)-3-methyl-pyrazol-1-yl]-thiazol-4-yl}-chromen-2-one in good yields.2 In addition, 2-acetylbutyrolactone can also function as the raw material for synthesizing pilocarpine that is a leading therapeutic agent for the treatment of narrow and wide angle glaucoma.3 Besides, this chemical can also act as a fluorogenic reagent in the quantitative spectrofluorometric determination of primary amines, which has been demonstrated to be equally accurate and precise as the officially or other reported methods.4

Reference

  1. Asghari, S.; Mohammadi, L., Reaction of tert-butyl isocyanide and dialkyl acetylenedicarboxylates in the presence of 2-acetylbutyrolactone. Synthesis of functionalized alpha-methylene-gamma-butyrolactones. Tetrahedron Lett. 2006, 47, 4297-4299.
  2. Rao, V. R.; Kumar, P. V., Facile one-pot synthesis of 3-{25-hydroxy-4-(2-hydroxy-ethyl)-3-methyl-pyrazol-1-yl -thiazol-4-yl} -chromen-2-ones via a three-component reaction. Synth. Commun. 2006, 36, 2157-2161.
  3. Horne, D. A.; Fugmann, B.; Yakushijin, K.; Buchi, G., A SYNTHESIS OF PILOCARPINE. J. Org. Chem. 1993, 58, 62-64.
  4. Sabry, S. M., Application of 2-acetylbutyrolactone to spectrofluorinietry: Fluorescence properties of Schiff bases derived from 2-acetylbutyrolactone and spectrofluorimetric determination of primary amine-containing compounds. J. Pharm. Biomed. Anal. 2006, 40, 1057-1067.

Chemical Properties

Colorless to light yellow liqui

Uses

An intermediate in the synthesis of 2,4-disubstituted pyridines. A fluorogenic reagent for the spectrofluorimetric determination of primary amines.

Uses

In synthesis of 3,4-disubstituted pyridines; of 5-(b-hydroxethyl)-4-methylthiazole.

Definition

ChEBI: 3-Acetyldihydro-2(3H)-furanone is a gamma-lactone.

Flammability and Explosibility

Not classified

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2-Acetylbutyrolactone Suppliers

BLiT (Hefei)Chemical Co.,Ltd
Tel
0551-62622640 17720572443
Email
bright@blitchem.com
Country
China
ProdList
289
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58
Zhejiang Realsun Chemical Industry Co., Ltd
Tel
0576-88312588-8674
Fax
0576-88312598
Email
marketing@realsunchem.com
Country
China
ProdList
215
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58
Chemspon Bio-Tech Co., Ltd
Tel
0571-88937695 88937835 13606537248
Fax
0571-88933015 QQ:1423821043
Email
sales@chemspon.com
Country
China
ProdList
242
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58
Hefei TNJ Chemical Industry Co.,Ltd.
Tel
551-65418679 15837135945
Fax
0551-65418697
Email
info@tnjchem.com
Country
China
ProdList
1889
Advantage
62
Hangzhou Benoy Chemical Co., Ltd.
Tel
17342059697
Fax
QQ:2710089141
Email
sales@benoychem.com
Country
China
ProdList
391
Advantage
58
Xingyuan(Inner Mongolia)Advanced Material Technology Co.,Ltd,
Tel
13482203243
Email
3826038396@qq.com
Country
China
ProdList
10
Advantage
58
J & K SCIENTIFIC LTD.
Tel
010-82848833 400-666-7788
Fax
86-10-82849933
Email
jkinfo@jkchemical.com
Country
China
ProdList
96815
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76
Meryer (Shanghai) Chemical Technology Co., Ltd.
Tel
021-61259108 18621169109
Fax
86-21-61259102
Email
market03@meryer.com
Country
China
ProdList
40228
Advantage
62
INTATRADE GmbH
Tel
+49 3493/605464
Fax
+49 3493/605470
Email
sales@intatrade.de
Country
Germany
ProdList
3572
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66
future industrial shanghai co., ltd
Tel
400-0066400 13621662912
Fax
021-55660885
Email
sales@jonln.com
Country
China
ProdList
1995
Advantage
65
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View Lastest Price from 2-Acetylbutyrolactone manufacturers

Jinan Finer Chemical Co., Ltd
Product
2-Acetylbutyrolactone 517-23-7
Price
US $0.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
5000mt
Release date
2022-02-17
BLiT (Hefei)Chemical Co.,Ltd
Product
2-Acetylbutyrolactone 517-23-7
Price
US $0.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
1500 TONS
Release date
2024-03-29
Hebei Saisier Technology Co., LTD
Product
2-Acetylbutyrolactone 517-23-7
Price
US $6.00/KG
Min. Order
1KG
Purity
More than 99%
Supply Ability
500KG/Month
Release date
2024-09-18

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