2-Methoxy-5-Iodopyridine
- Product Name
- 2-Methoxy-5-Iodopyridine
- CAS No.
- 13472-61-2
- Chemical Name
- 2-Methoxy-5-Iodopyridine
- Synonyms
- 2-Methoxy-5-Iodopyridine;5-lodo-2-methoxypyridine;Pyridine, 5-iodo-2-methoxy-;5-Iodo-2-methoxypyridine>5-Iodo-2-methoxypyridine 98%
- CBNumber
- CB81033218
- Molecular Formula
- C6H6INO
- Formula Weight
- 235.02
- MOL File
- 13472-61-2.mol
2-Methoxy-5-Iodopyridine Property
- Boiling point:
- 237℃
- Density
- 1.825
- refractive index
- 1.6060 to 1.6100
- Flash point:
- 97℃
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- form
- Liquid
- pka
- 1.38±0.10(Predicted)
- color
- Clear colorless to pale yellow
- Sensitive
- Light Sensitive
Safety
- HS Code
- 29333990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- I0925
- Product name
- 5-Iodo-2-methoxypyridine
- Purity
- >98.0%(GC)
- Packaging
- 1g
- Price
- $38
- Updated
- 2025/07/31
- Product number
- I0925
- Product name
- 5-Iodo-2-methoxypyridine
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $119
- Updated
- 2025/07/31
- Product number
- I737150
- Product name
- 5-Iodo-2-methoxypyridine
- Packaging
- 100mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- 6238AA
- Product name
- 5-Iodo-2-methoxypyridine
- Packaging
- 1g
- Price
- $34
- Updated
- 2021/12/16
- Product number
- 4H56-H-33
- Product name
- 5-Iodo-2-methoxypyridine
- Packaging
- 5G
- Price
- $128
- Updated
- 2021/12/16
2-Methoxy-5-Iodopyridine Chemical Properties,Usage,Production
Synthesis
13472-85-0
13472-61-2
The general procedure for the synthesis of 5-bromo-2-methoxypyridine from 5-bromo-2-methoxypyridine was as follows: n-butyllithium (1.5 M in hexane solution, 4.98 mL, 7.47 mmol) was slowly added to a solution of isopropylmagnesium chloride (1.61 M in THF, 4.64 mL, 7.47 mmol) in THF (20 mL) under ice bath cooling conditions. The reaction mixture was stirred for 5 min to form a yellow solution after which 5-bromo-2-methoxypyridine (1.405 g, 0.98 mL, 7.10 mmol, 95%) was added. The resulting solution was continued to be stirred at 0 °C for 45 min. Molecular iodine (3.79 g, 14.94 mmol) was then added and the reaction mixture was stirred at 0°C for 30 minutes and then at room temperature for 1 hour. Upon completion of the reaction, the reaction was quenched by the addition of aqueous ammonium chloride (5 mL) and the organic and aqueous phases were separated. The aqueous phase was extracted with ethyl acetate (2 x 75 mL), and the combined organic layers were dried with magnesium sulfate, filtered and concentrated under reduced pressure. The crude product was purified by silica gel column chromatography (ethyl acetate-heptane, 5-80%) to afford the target product 5-iodo-2-methoxypyridine.
References
[1] Synthesis, 2012, vol. 44, # 5, p. 735 - 746
[2] Synthesis (Germany), 2015, vol. 47, # 20, p. 3231 - 3240
[3] Journal of the American Chemical Society, 2015, vol. 137, # 33, p. 10480 - 10483
2-Methoxy-5-Iodopyridine Preparation Products And Raw materials
Raw materials
Preparation Products
2-Methoxy-5-Iodopyridine Suppliers
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View Lastest Price from 2-Methoxy-5-Iodopyridine manufacturers
- Product
- 5-Iodo-2-methoxypyridine 13472-61-2
- Price
- US $10.00-50.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2025-06-18
- Product
- 5-Iodo-2-methoxypyridine 13472-61-2
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 98.7%
- Supply Ability
- 100 tons
- Release date
- 2022-01-25
- Product
- 2-Methoxy-5-Iodopyridine 13472-61-2
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99.0%
- Supply Ability
- 100kg
- Release date
- 2020-01-07