2-Bromo-4-iodoaniline
- Product Name
- 2-Bromo-4-iodoaniline
- CAS No.
- 29632-73-3
- Chemical Name
- 2-Bromo-4-iodoaniline
- Synonyms
- 2-Bromo-4-iodoanilin;2-Bromo-4-iodoaniline;2-Bromo-4-iodobenzenamine;Benzenamine, 2-bromo-4-iodo-
- CBNumber
- CB81091959
- Molecular Formula
- C6H5BrIN
- Formula Weight
- 297.92
- MOL File
- 29632-73-3.mol
2-Bromo-4-iodoaniline Property
- Melting point:
- 75-76 °C
- Boiling point:
- 307.6±32.0 °C(Predicted)
- Density
- 2.292
- storage temp.
- Keep in dark place,Inert atmosphere,2-8°C
- form
- tiny crystalline needles
- pka
- 1.74±0.10(Predicted)
- color
- Fawn/mauve
Safety
- HS Code
- 2921420090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B687548
- Product name
- 2-Bromo-4-iodoaniline
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- OR17657
- Product name
- 2-Bromo-4-iodoaniline
- Purity
- 98%
- Packaging
- 5g
- Price
- $60
- Updated
- 2021/12/16
- Product number
- FB139629
- Product name
- 2-Bromo-4-iodoaniline
- Packaging
- 500mg
- Price
- $70
- Updated
- 2021/12/16
- Product number
- OR17657
- Product name
- 2-Bromo-4-iodoaniline
- Purity
- 98%
- Packaging
- 1g
- Price
- $24
- Updated
- 2021/12/16
- Product number
- Z0488
- Product name
- 2-Bromo-4-iodoaniline
- Packaging
- 1g
- Price
- $84
- Updated
- 2021/12/16
2-Bromo-4-iodoaniline Chemical Properties,Usage,Production
Synthesis
615-36-1
29632-73-3
Part A. Synthesis of 2-bromo-4-iodoaniline The synthesis of this compound is based on a modified method of J. Chem. Soc., Perkin Trans. 1, 1970, 2106. The specific steps are as follows: 1. 1.61 g (9.36 mmol) of o-bromoaniline was mixed with 10 mL of water and 750 mg of sodium bicarbonate solid was added. 2. Mildly heat the mixture using a hot air gun to melt the aniline. 3. 2.58 g (10.2 mmol) of powdered iodine is added in batches over several minutes. 4. 4. Stir the reaction mixture for 2 hours at room temperature. 5. 5. The resulting dark solid product is collected by filtration, washed with water and dried over air to give a slightly wetted dark solid. 6. The product was purified directly by rapid column chromatography on silica gel, eluting first with hexane and subsequently with a hexane solution containing 5% ethyl acetate to afford 2.53 g (91% yield) of the target compound 2-bromo-4-iodoaniline as a pale pink solid.
References
[1] Bulletin of the Chemical Society of Ethiopia, 2015, vol. 29, # 1, p. 157 - 162
[2] Chemical Communications, 2012, vol. 48, # 48, p. 6052 - 6054
[3] Organic and Biomolecular Chemistry, 2011, vol. 9, # 8, p. 2987 - 2991
[4] Molecules, 2005, vol. 10, # 10, p. 1307 - 1317
[5] Molecules, 2004, vol. 9, # 7, p. 617 - 621
2-Bromo-4-iodoaniline Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-Bromo-4-iodoaniline manufacturers
- Product
- 2-Bromo-4-iodoaniline 29632-73-3
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 100KG
- Release date
- 2018-08-22