ChemicalBook > CAS DataBase List > cis-1,2-Cyclohexanediol

cis-1,2-Cyclohexanediol

Synthesis

Product Name: cis-1,2-Cyclohexanediol
CAS No.: 1792-81-0
Chemical Name: cis-1,2-Cyclohexanediol
Synonyms: Grandidentol;TIMTEC-BB SBB007678;CIS-HEXAHYDROCATECHOL;CIS-1,2-CYCLOHEXANEDIOL;1,2-cis-cyclohexanediol;Adipic Acid Impurity 29;cis-Cyclohexane-1,2-diol;cis-2-Hydroxycyclohexanol;1,2-Cyclohexanediol, cis-;(1S)-1α,2α-Cyclohexanediol
CBNumber: CB8159715
Molecular Formula: C6H12O2
Formula Weight: 116.16
MOL File: 1792-81-0.mol

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cis-1,2-Cyclohexanediol Property

Melting point:: 97-101 °C (lit.)
Boiling point:: 116 °C / 13mmHg
Density: 1.0297
refractive index: 1.4270 (estimate)
storage temp.: Store at room temperature
solubility: soluble in Methanol
form: Crystalline Flakes or Powder
pka: 14.49±0.40(Predicted)
color: White to light beige
Water Solubility: slightly soluble
BRN: 1340578
CAS DataBase Reference: 1792-81-0(CAS DataBase Reference)
NIST Chemistry Reference: cis-1,2-Cyclohexanediol(1792-81-0)

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Safety

Safety Statements: 22-24/25
WGK Germany: 3
F: 3-10
HS Code: 29061990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 361267
Product name: cis-1,2-Cyclohexanediol
Purity: 99%
Packaging: 1g
Price: $58
Updated: 2025/07/31

TCI Chemical

Product number: C1802
Product name: cis-1,2-Cyclohexanediol
Purity: >98.0%(GC)
Packaging: 1g
Price: $51
Updated: 2025/07/31

TRC

Product number: C997755
Product name: cis-1,2-Cyclohexanediol
Packaging: 250mg
Price: $85
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC58748
Product name: cis-1,2-Cyclohexanediol
Packaging: 1g
Price: $90
Updated: 2021/12/16

AK Scientific

Product number: M185
Product name: cis-1,2-Cyclohexanediol
Packaging: 1g
Price: $94
Updated: 2021/12/16

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cis-1,2-Cyclohexanediol Chemical Properties,Usage,Production

Synthesis

To a mixture of N-methylmorpholine-N-oxide.2H2O (18.2 g, 155 mmol), water (50 mL), acetone (20 mL), and osmium tetroxide (80 mg) in t-butanol (8 mL) was added distilled cyclohexene (10.1 mL, 100 mmol). The reaction was slightly exothermic initially and was maintained at room temperature with a water bath. The reaction was complete after stirring overnight at room temperature under nitrogen. A slurry of 1 g of sodium hydrosulfifite, 12 g of magnesium silicate (magnesol), and 80 ml of water was added, and the magnesol was fifiltered. The fifiltrate was neutralized to pH 7 with 1 N H2SO4, the acetone was evaporated under vacuum, and the pH was further adjusted to pH 2. The solution was saturated with NaCl and extracted with EtOAc. The aqueous phase was concentrated by azeotroping with n-butanol and further extracted with ethyl acetate. The combined ethyl acetate layers were dried and evaporated, yielding 11.2 g (96.6%) of crystalline solid. Recrystallization from ether provided 10.6 g (91%) of cis-1,2-cyclohexanediol, mp 95–97°C.

Reference: Van Rheenen, V.; Kelly, R. C.; Cha, D. Y. Tetrahedron Lett. 1976, 17, 1973−1976.

Chemical Properties

White to light beige crystalline flakes or powder

Uses

cis-1,2-Cyclohexanediol is a reagent used in the synthesis of boronic esters of corannulene which are used to prepare icosahedral supramolecules.

Definition

ChEBI: A cyclohexane-1,2-diol with cis-configuration.

General Description

Core-shell-like silica nickel species nanoparticle catalyzed dehydrogenation of 1,2-cyclohexanediol to catechol is reported. Crystal structure of a Cr(V) complex with cis-1,2-cyclohexanediol is reported. Enzymatic oxidation of cis-1,2-cyclohexanediol by Gluconobacter oxydans (ATCC 621) is reported.

cis-1,2-Cyclohexanediol Preparation Products And Raw materials

Raw materials

Preparation Products

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1792-81-0, cis-1,2-CyclohexanediolRelated Search:

1,2-Cyclohexanediol 1,3-Propanediol TRANS-1,2-CYCLOHEXANEDIOL 2-Methyl-2,4-pentanediol 1,2-Cyclohexanedione 1,4-Butanediol 1,2-Hexanediol 1,4-Cyclohexanediol 2-Butene-1,4-diol Dimethyl maleate cis-(1S,2R)-2-Aminocyclopentanol hydrochloride cis-1,4-Dichloro-2-butene Inositol nicotinate Quinic acid MYO-INOSITOL 2-MONOPHOSPHATE DI(CYCLOHEXYLAMMONIUM) SALT Hydroxyecdysone Cevadine Chlorogenic acid

1,2-Cyclohexanediol, (1R,2S)-

cis-2-Hydroxycyclohexanol

meso-cis-1,2-Cyclohexanediol

(1R,2S)-1,2-Cyclohexanediol

(1S)-1α,2α-Cyclohexanediol

(1α,2α)-1,2-Cyclohexanediol

cis-1,2-Cyclohexanediol,99%

cis-1,2-Cyclohexanediol, 99% 1GR

cis-Cyclohexane-1,2-diol

cis-1,2-Cyclohexanediol 99%

<i>cis</i>-1,2-Cyclohexanediol

TIMTEC-BB SBB007678

1,2-Cyclohexanediol, cis-

Grandidentol

CIS-HEXAHYDROBRENZCATECHIN

CIS-HEXAHYDROCATECHOL

CIS-1,2-CYCLOHEXANEDIOL

CIS-1,2-DIHYDROXYCYCLOHEXANE

(1R,2S)-cyclohexane-1,2-diol

1,2-cis-Dihydroxycyclohexane

cis-hexahydrobrenzkatechin

rel-((1R,2S)-Cyclohexane-1,2-diol)

cis-1,2-Cyclohexanediol &gt

1,2-Cyclohexanediol, (1R,2S)-rel-

1,2-cis-cyclohexanediol

Adipic Acid Impurity 29

1792-81-0

1972-81-0

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