ChemicalBook > CAS DataBase List > 2-AMINO-5-CHLORO-4-METHYL-3-NITROPYRIDINE

2-AMINO-5-CHLORO-4-METHYL-3-NITROPYRIDINE

Product Name
2-AMINO-5-CHLORO-4-METHYL-3-NITROPYRIDINE
CAS No.
148612-17-3
Chemical Name
2-AMINO-5-CHLORO-4-METHYL-3-NITROPYRIDINE
Synonyms
2-Amino-3-Nitro-5-Chloro-4-MP;2-AMINO-3-NITRO-5-CHLORO-4-PICOLINE;2-Amino-5-chloro-3-nitro-4-picoline;5-chloro-4-methyl-3-nitro-2-Pyridinamine;5-Chloro-4-Methyl-3-nitropyridin-2-aMine;2-Amino-3-nitro-4-methyl-5-chloropyridine;2-AMINO-5-CHLORO-4-METHYL-3-NITROPYRIDINE;2-PYRIDINAMINE, 5-CHLORO-4-METHYL-3-NITRO-;2-AMino-3-Nitro-5-Chloro-4-Methyl Pyridine;5-Chloro-4-methyl-3-nitro-pyridin-2-ylamine
CBNumber
CB8165811
Molecular Formula
C6H6ClN3O2
Formula Weight
187.58
MOL File
148612-17-3.mol
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2-AMINO-5-CHLORO-4-METHYL-3-NITROPYRIDINE Property

storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
Appearance
Yellow to brown Solid
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Safety

HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
A617413
Product name
2-Amino-5-chloro-4-methyl-3-nitropyridine
Packaging
50mg
Price
$45
Updated
2021/12/16
Apolloscientific
Product number
OR345260
Product name
2-Amino-5-chloro-4-methyl-3-nitropyridine
Purity
95+%
Packaging
5g
Price
$166
Updated
2021/12/16
SynQuest Laboratories
Product number
4H55-5-38
Product name
2-Amino-5-chloro-4-methyl-3-nitropyridine
Packaging
5G
Price
$183
Updated
2021/12/16
Apolloscientific
Product number
OR345260
Product name
2-Amino-5-chloro-4-methyl-3-nitropyridine
Purity
95+%
Packaging
10g
Price
$275
Updated
2021/12/16
SynQuest Laboratories
Product number
4H55-5-38
Product name
2-Amino-5-chloro-4-methyl-3-nitropyridine
Packaging
10g
Price
$303
Updated
2021/12/16
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2-AMINO-5-CHLORO-4-METHYL-3-NITROPYRIDINE Chemical Properties,Usage,Production

Synthesis

36936-27-3

148612-17-3

Example 108A Synthesis of 5-chloro-4-methyl-3-nitropyridin-2-amine: 2-amino-5-chloro-4-methylpyridine (30 g, 210 mmol) was dissolved in concentrated sulfuric acid (150 mL) and the solution was cooled to -10 °C. Nitric acid (36 mL, 806 mmol) was slowly added dropwise with stirring. After the dropwise addition was completed, the reaction mixture was warmed to 55°C and stirred continuously at this temperature for 3 hours. Upon completion of the reaction, the mixture was carefully poured into an ice/water mixture and the pH was adjusted to 8 by slow addition of 22% concentrated aqueous ammonium hydroxide solution.Subsequently, the suspension in the reaction mixture was filtered, the resulting solid was washed with water, and finally dried under vacuum to afford the target product 5-chloro-4-methyl-3-nitropyridin-2-amine (23 g, 123 mmol, 58.3% yield).

References

[1] Patent: US2014/275026, 2014, A1. Location in patent: Paragraph 1092

2-AMINO-5-CHLORO-4-METHYL-3-NITROPYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-AMINO-5-CHLORO-4-METHYL-3-NITROPYRIDINE Suppliers

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View Lastest Price from 2-AMINO-5-CHLORO-4-METHYL-3-NITROPYRIDINE manufacturers

Shaanxi Dideu Medichem Co. Ltd
Product
2-Amino-5-chloro-3-nitro-4-picoline 148612-17-3
Price
US $1.00-1.00/Kg/Drum
Min. Order
1g
Purity
98%
Supply Ability
50tons
Release date
2020-05-12
Dideu Industries Group Limited
Product
2-AMINO-5-CHLORO-4-METHYL-3-NITROPYRIDINE 148612-17-3
Price
US $1.10/g
Min. Order
1g
Purity
99.00%
Supply Ability
100 Tons min
Release date
2021-09-22
Career Henan Chemical Co
Product
2-AMINO-5-CHLORO-4-METHYL-3-NITROPYRIDINE 148612-17-3
Price
US $1.00/KG
Min. Order
1KG
Purity
97%-99.9%
Supply Ability
200kg
Release date
2020-03-05

148612-17-3, 2-AMINO-5-CHLORO-4-METHYL-3-NITROPYRIDINERelated Search:

2-Amino-5-bromo-4-methylpyridine 2-Amino-5-nitro-4-picoline 2-AMINO-3-NITRO-5-PICOLINE 2-Amino-5-bromo-4-methyl-3-nitropyridine 5-bromo-6-methyl-3-nitropyridin-2-amine 3,5-Dibromo-2-pyridylamine 2-Amino-6-methoxy-3-nitropyridine 2-Amino-6-methyl-5-nitropyridine 2-AMINO-3-BROMO-4-METHYL-5-NITROPYRIDINE 2-AMINO-3-CHLORO-5-NITRO-6-PICOLINE 2-Amino-5-chloro-3-nitro-6-picoline 2-AMINO-3-BROMO-5-NITRO-6-PICOLINE 4-METHYL-PYRIDINE-2,3-DIAMINE 5-CHLORO-2,3-DIAMINOPYRIDINE 2-Amino-5-chloro-3-nitropyridine 2-Amino-5-chloro-4-picoline 2-Amino-3-nitro-4-picoline 2-AMINO-5-CHLORO-4-METHYL-3-NITROPYRIDINE

  • 2-PYRIDINAMINE, 5-CHLORO-4-METHYL-3-NITRO-
  • 2-AMINO-5-CHLORO-4-METHYL-3-NITROPYRIDINE
  • 2-Amino-5-chloro-3-nitro-4-picoline
  • 2-AMINO-3-NITRO-5-CHLORO-4-PICOLINE
  • 2-AMino-3-Nitro-5-Chloro-4-Methyl Pyridine
  • 5-Chloro-4-Methyl-3-nitropyridin-2-aMine
  • 5-chloro-4-methyl-3-nitro-2-Pyridinamine
  • 5-Chloro-4-methyl-3-nitro-pyridin-2-ylamine
  • 2-Amino-5-chloro-4-methyl-3-nitropyridine 95+%
  • 2-Amino-3-nitro-4-methyl-5-chloropyridine
  • 2-AMINO-5-CHLORO-4-METHYL-3-NITROPYRIDINE ISO 9001：2015 REACH
  • 2-Amino-3-Nitro-5-Chloro-4-MP
  • 148612-17-3
  • Pyridine