ChemicalBook > CAS DataBase List > Tetrahydrothiopyran-4-one
Tetrahydrothiopyran-4-one
- Product Name
- Tetrahydrothiopyran-4-one
- CAS No.
- 1072-72-6
- Chemical Name
- Tetrahydrothiopyran-4-one
- Synonyms
- TETRAHYDRO-4H-THIOPYRAN-4-ONE;dihydro-2H-thiopyran-4(3H)-one;4H-Thiopyran-4-one, tetrahydro-;Penthianone;THIAN-4-ONE;4-OXOTHIANE;4-Oxothiane>THIAN-3-ONEOXIME;4-Thiacyclohexanon;4-thiacyclohexanone
- CBNumber
- CB8202200
- Molecular Formula
- C5H8OS
- Formula Weight
- 116.18
- MOL File
- 1072-72-6.mol
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Tetrahydrothiopyran-4-one Property
- Melting point:
- 60-64 °C (lit.)
- Boiling point:
- 140.82°C (estimate)
- Density
- 1.050 (estimate)
- refractive index
- 1.5100 (estimate)
- storage temp.
- Inert atmosphere,Room Temperature
- solubility
- Acetonitrile (Slightly), Chloroform (Slightly)
- form
- Crystalline Solid
- color
- White to pale yellow
- BRN
- 106464
- InChIKey
- OVRJVKCZJCNSOW-UHFFFAOYSA-N
- LogP
- 0.490 (est)
- CAS DataBase Reference
- 1072-72-6(CAS DataBase Reference)
- NIST Chemistry Reference
- 4H-Thiopyran-4-one, tetrahydro-(1072-72-6)
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Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P337+P313IF eye irritation persists: Get medical advice/attention.
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N-Bromosuccinimide Price
Sigma-Aldrich
- Product number
- 155160
- Product name
- Tetrahydro-4H-thiopyran-4-one
- Purity
- 99%
- Packaging
- 1g
- Price
- $43.3
- Updated
- 2024/03/01
Sigma-Aldrich
- Product number
- 155160
- Product name
- Tetrahydro-4H-thiopyran-4-one
- Purity
- 99%
- Packaging
- 5g
- Price
- $128
- Updated
- 2023/06/20
TCI Chemical
- Product number
- O0112
- Product name
- 4-Oxothiane
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $68
- Updated
- 2024/03/01
TCI Chemical
- Product number
- O0112
- Product name
- 4-Oxothiane
- Purity
- >98.0%(GC)
- Packaging
- 25g
- Price
- $218
- Updated
- 2024/03/01
Alfa Aesar
- Product number
- A15872
- Product name
- Tetrahydro-4H-thiopyran-4-one, 99%
- Packaging
- 1g
- Price
- $39.65
- Updated
- 2024/03/01
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Tetrahydrothiopyran-4-one Chemical Properties,Usage,Production
Chemical Properties
WHITE TO PALE YELLOW CRYSTALLINE SOLID
Uses
Tetrahydro-?4H-?thiopyran-?4-?one is a cyclic carbonyl compound used as a reactant in the stereoselective preparation of [aryl(nitro)ethyl] carbonyl compounds via asymmetric Michael addition to nitroolefins catalyzed by chiral pyrrolidine-pyridine conjugate bases.
General Description
The diastereoselectivity of the aldol reaction of tetrahydro-4H-thiopyran-4-one has been studied.
Purification Methods
Purify it by recrystallisation from diisopropyl ether or pet ether and dry it in air. If too impure, then dissolve it in Et2O, wash with aqueous NaHCO3, then H2O, dry (MgSO4), filter, evaporate and the residue is recrystallised as before. [Cardwell J Chem Soc 715 1949.] The oxime can be recrystallised from CHCl3/pet ether (at -20o) and has m 84-85o [Barkenbus et al. J Org Chem 20 871 1955]. The 2,4-dinitrophenylhydrazone has m 186o (from EtOAc) [Barkenbus et al. J Org Chem 16 232 1951]. The S-dioxide is recrystallised from AcOH, m 173-174o [Fehnel & Carmack J Am Chem Soc 70 1813 1948, Beilstein 17 II 287, 17 III/IV 4172, 17/1 V 21].
Tetrahydrothiopyran-4-one Preparation Products And Raw materials
Raw materials
Preparation Products
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Tetrahydrothiopyran-4-one Suppliers
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- 15995055116
- Fax
- 815229059
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- China
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- China
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- 24529
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View Lastest Price from Tetrahydrothiopyran-4-one manufacturers
Henan Aochuang Chemical Co.,Ltd.
- Product
- Tetrahydrothiopyran-4-one 1072-72-6
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 1Ton
- Release date
- 2022-10-08
Dideu Industries Group Limited
- Product
- Tetrahydrothiopyran-4-one 1072-72-6
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons Min
- Release date
- 2021-10-28
Career Henan Chemical Co
- Product
- Tetrahydrothiopyran-4-one 1072-72-6
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 20kg
- Release date
- 2018-08-14
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